Enrichment model and major controlling factors of below-source tight oil in Lower Cretaceous Fuyu reservoirs in northern Songliao Basin,NE China

Based on the geochemical,seismic,logging and drilling data,the Fuyu reservoirs of the Lower Cretaceous Quantou Formation in northern Songliao Basin are systematically studied in terms of the geological characteristics,the tight oil enrichment model and its major controlling factors.First,the Quantou Formation is overlaid by high-quality source rocks of the Upper Cretaceous Qingshankou Formation,with the development of nose structure around sag and the broad and continuous distribution of sand bodies.The reservoirs are tight on the whole.Second,the configuration of multiple elements,such as high-quality source rocks,reservoir rocks,fault,overpressure and structure,controls the tight oil enrichment in the Fuyu reservoirs.The source-reservoir combination controls the tight oil distribution pattern.The pressure difference between source and reservoir drives the charging of tight oil.The fault-sandbody transport system determines the migration and accumulation of oil and gas.The positive structure is the favorable place for tight oil enrichment,and the fault-horst zone is the key part of syncline area for tight oil exploration.Third,based on the source-reservoir relationship,transport mode,accumulation dynamics and other elements,three tight oil enrichment models are recognized in the Fuyu reservoirs:(1)vertical or lateral migration of hydrocarbon from source rocks to adjacent reservoir rocks,that is,driven by overpressure,hydrocarbon generated is migrated vertically or laterally to and accumulates in the adjacent reservoir rocks;(2)transport of hydrocarbon through faults between separated source and reservoirs,that is,driven by overpressure,hydrocarbon migrates downward through faults to the sandbodies that are separated from the source rocks;and(3)migration of hydrocarbon through faults and sandbodies between separated source and reservoirs,that is,driven by overpressure,hydrocarbon migrates downwards through faults to the reservoir rocks that are separated from the source rocks,and then migrates laterally through sandbodies.Fourth,the differences in oil source conditions,charging drive,fault distribution,sandbody and reservoir physical properties cause the differential enrichment of tight oil in the Fuyu reservoirs.Comprehensive analysis suggests that the Fuyu reservoir in the Qijia-Gulong Sag has good conditions for tight oil enrichment and has been less explored,and it is an important new zone for tight oil exploration in the future.

Subaqueous volcanic eruptive facies,facies model and its reservoir significance in a continental lacustrine basin:A case from the Cretaceous in Chaganhua area of southern Songliao Basin,NE China

The conventional lithofacies and facies model of subaerial and marine pyroclastic rocks cannot reflect the characteristics of subaqueous volcanic edifice in lacustrine basins.In order to solve this problem,the lithofacies of subaqueous eruptive pyroclastic rocks is discussed and the facies model is established by taking the tuff cone of Cretaceous Huoshiling Formation in the Chaganhua area of the Changling fault depression,Songliao Basin as the research object.The results indicate that the subaqueous eruptive pyroclastic rocks in the Songliao Basin can be divided into two facies and four subfacies.The two facies are the subaqueous explosive facies and the volcanic sedimentary facies that is formed during the eruption interval.The subaqueous explosive facies can be further divided into three subfacies:gas-supported hot pyroclastic flow subfacies,water-laid density current subfacies and subaqueous fallout subfacies.The volcanic sedimentary facies consists of pyroclastic sedimentary rocks containing terrigenous clast subfacies.A typical facies model of the tuff cone that is formed by subaqueous eruptions in the Songliao Basin was established.The tuff cone is generally composed of multiple subaqueous eruption depositional units and can be divided into two facies associations:near-source facies association and far-source facies association.The complete vertical succession of one depositional unit of the near-source facies association is composed of pyroclastic sedimentary rocks containing terrigenous clast subfacies,gas-supported hot pyroclastic flow subfacies,water-laid density current subfacies and subaqueous fallout subfacies from bottom to top.The depositional unit of the far-source facies association is dominated by the subaqueous fallout subfacies and contains several thin interlayered deposits of the water-laid density current subfacies.The gas-supported hot pyroclastic flow subfacies and the pyroclastic sedimentary rocks containing terrigenous clast subfacies are favorable subaqueous eruptive facies for reservoirs in continental lacustrine basins.

Petroleum exploration breakthrough and geological significance in Cretaceous Yingcheng and Denglouku formations of Shuangcheng area, northern Songliao Basin, NE China

Based on drilling geological,geochemical,geophysical and production test data,the characteristics of source rocks,reservoir rocks and caprocks,as well as the process of hydrocarbon generation,trap evolution and oil accumulation of the oil-bearing assemblage composed of the Cretaceous Yingcheng Formation(K1yc)and Denglouku Formation(K1d)in the Shuangcheng area,northern Songliao Basin,NE China,were analyzed by using the research methods for petroleum systems.The source rocks mainly exist in K1yc,with the organic matters mainly originated from lower aquatic organisms and algae,and reaching the grade of high-quality source rock in terms of organic abundance.The crude oil,which is characterized by low density,high freezing point and high wax content,is believed to have generated by the K1yc source rocks.The reservoir rocks include K1d sandstones and K1yc glutenites.The mudstone in the fourth member of K1d serves as the direct caprock of the oil reservoir.The oil was generated during the period between Yaojia Formation and Nenjiang Formation,and then accumulated during the periods of Nenjiang Formation and Paleogene–Neogene.The traps evolved in three stages:the late Yingcheng Formation,the late Quantou Formation and the late Nenjiang Formation,forming structural and structural-lithologic reservoirs.It is concluded that good source-reservoir-caprock assemblage,late hydrocarbon charging,short migration distance and stable tectonic setting are favorable factors for the formation of oil reservoirs.

Quantitative evaluation model of shale oil adsorption:A case study of the first member of Cretaceous Qingshankou Formation in northern Songliao Basin,NE China

A quantitative evaluation model that integrates kerogen adsorption and clay pore adsorption of shale oil was proposed,and the evaluation charts of adsorption-swelling capacity of kerogen(Mk)and adsorbed oil capacity of clay minerals(Mc)were established,taking the 1st member of Cretaceous Qingshankou Formation in the northern Songliao Basin as an example.The model and charts were derived from swelling oil experiments performed on naturally evolved kerogens and adsorbed oil experiments on clays(separated from shale core samples).They were constructed on the basis of clarifying the control law of kerogen maturity evolution on its adsorption-swelling capacity,and considering the effect of both the clay pore surface area that occupied by adsorbed oil and formation temperature.The results are obtained in four aspects:(1)For the Qing 1 Member shale,with the increase of maturity,Mk decreases.Given Ro of 0.83%–1.65%,Mk is about 50–250 mg/g.(2)The clay in shale adsorbs asphaltene.Mc is 0.63 mg/m^(2),and about 15%of the clay pore surface is occupied by adsorbed oil.(3)In the low to medium maturity stages,the shale oil adsorption is controlled by organic matter.When Ro>1.3%,the shale oil adsorption capacity is contributed by clay pores.(4)The oil adsorption capacity evaluated on the surface at room temperature is 8%–22%(avg.15%)higher than that is held in the formations.The proposed evaluation model reveals the occurrence mechanisms of shale oils with different maturities,and provides a new insight for estimating the reserves of shale oil under formation temperature conditions.

Identification, evolution and geological indications of solid bitumen in shales: A case study of the first member of Cretaceous Qingshankou Formation in Songliao Basin, NE China

On the basis of sorting out current understanding of solid bitumen (SB) in shales and taking organic-rich shales in the first member of the Cretaceous Qingshankou Formation in the Songliao Basin as an example, the definition, classification, occurrence and evolution path of SB are systemtically studied, and the indicative significance of SB reflectance (Rob) on maturity and its influence on the development of reservoir space are discussed and summarized. The results show that the difference of primary maceral types is primarily responsible for the different evolution paths of SB. Most of the pre-oil bitumen is in-situ SB with only a small amount being of migrated SB, while most of the post-oil bitumen and pyrobitumen are migrated SB. From the immature to early oil maturity stage, bituminite, vitrinite, and inertinite can be distinguished from SB based on their optical characteristics under reflected light, and alginite can be differentiated from SB by their fluorescence characteristics. Under scanning electron microscope, in-situ SB and migrated SB can be effectively identified. Rob increases linearly with increasing vitrinite reflectance (Ro), as a result of a decrease of aliphatic structure and the enhancement of aromatization of SB. Within the oil window three types of secondary pores may develop in SB, including modified mineral pores, devolatilization cracks and bubble holes. At a high maturity stage spongy pores may develop in pyrobitumen. Scanning electron microscopy combined with in-situ SEM-Raman spectroscopy can further reveal the structral information of different types of SB, thus providing crucial data for understanding for understanding OM migration paths, dynamics, and distances at micro-scale.

Gulong shale oil enrichment mechanism and orderly distribution of conventional–unconventional oils in the Cretaceous Qingshankou Formation,Songliao Basin,NE China

Through the study of organic matter enrichment,hydrocarbon generation and accumulation process of black shale of the Cretaceous Qingshankou Formation in the Songliao Basin,the enrichment mechanism of Gulong shale oil and the distribution of conventional–unconventional oil are revealed.The Songliao Basin is a huge interior lake basin formed in the Early Cretaceous under the control of the subduction and retreat of the western Pacific plate and the massive horizontal displacement of the Tanlu Fault Zone in Northeast China.During the deposition of the Qingshankou Formation,strong terrestrial hydrological cycle led to the lake level rise of the ancient Songliao Basin and the input of a large amount of nutrients,resulting in planktonic bacteria and algae flourish.Intermittent seawater intrusion events promoted the formation of salinization stratification and anoxic environment in the lake,which were beneficial to the enrichment of organic matters.Biomarkers analysis confirms that the biogenic organic matter of planktonic bacteria and algae modified by microorganisms plays an important role in the formation of high-quality source rocks with high oil generation capability.There are four favorable conditions for the enrichment of light shale oil in the Qingshankou Formation of the Gulong Sag,Songliao Basin:the moderate organic matter abundance and high oil potential provide sufficient material basis for oil enrichment;high degree of thermal evolution makes shale oil have high GOR and good mobility;low hydrocarbon expulsion efficiency leads to a high content of retained hydrocarbons in the source rock;and the confinement effect of intra-layer cement in the high maturity stage induces the efficient accumulation of light shale oil.The restoration of hydrocarbon accumulation process suggests that liquid hydrocarbons generated in the early(low–medium maturity)stage of the Qingshankou Formation source rocks accumulated in placanticline and slope after long-distance secondary migration,forming high-quality conventional and tight oil reservoirs.Light oil generated in the late(medium–high maturity)stage accumulated in situ,forming about 15 billion tons of Gulong shale oil resources,which finally enabled the orderly distribution of conventional–unconventional oils that are contiguous horizontally and superposed vertically within the basin,showing a complete pattern of“whole petroleum system”with conventional oil,tight oil and shale oil in sequence.

Ostracod Biostratigraphy of the Late Cretaceous Qingshankou Formation in the Songliao Basin

An ostracod biostratigraphic study was performed on 425 samples from the composite geological section constructed by using cores taken from five selected wells drilled in the Late Cretaceous Qingshankou Formation in the Songliao basin. A total of 19 ostracod zones are established in the formation, of which 3 are newly established and 3 are revised. The 19 ostracod zones are described in detail. This study provides a basis for the detailed stratigraphic division and correlation of the Qingshankou Formation and the Gaotaizi oil reservoir in the oilfield in the Songliao basin.

High-precision geochronology of the Early Cretaceous Yingcheng Formation and its stratigraphic implications for Songliao Basin,China

The Songliao Basin in Northeast Asia is the largest and longest-lived rift basin and preserves a nearcontinuous continental succession of the most of the Cretaceous period,providing great material to investigate the adaption of the terrestrial systems to the Cretaceous greenhouse climate and tectonic events.However,the paucity of precise and accurate radioisotopic ages from the Early Cretaceous strata of the Songliao Basin has greatly held back the temporal and causal correlation of the continental records to the global Early Cretaceous records.Three tuff layers intercalated in the Yingcheng Formation have been intercepted by the SK-2 borehole,which offer excellent materials for radioisotopic dating and calibration of the chronostratigraphy of the Lower Cretaceous sequence of Songliao Basin.Moreover,the Yingcheng Formation recorded the largest and the last of the two major volcanic events in Songliao Basin,which also represents a turning point in the basin evolution history of Songliao from syn-rift stage to post-rift stage.Here we report high-precision U–Pb zircon geochronology by the CA-ID-TIMS technique on three tuff samples from the Yingcheng Formation of the SK-2 borehole in the Songliao Basin to construct a greatly improved,absolute age framework for the Yingcheng Formation and provide crucial age constraints for the Songliao Lower Cretaceous Strata.The new CA-ID-TIMS geochronology constrained the Yingcheng Formation at 102.571+0.320/-2.346 Ma to ca.113 Ma,correlating to the Albian Stage.Combined with the previous published Songliao geochronology,the Quantou Formation is constrained to between 96.442+0.475/-0.086 Ma and 91.923+0.475/-0.086 Ma;the Denglouku Formation is constrained to between 102.571+0.320/-2.346 Ma and 96.442+0.475/-0.086 Ma;the age of the Shahezi Formation is estimated at ca.113 Ma to ca.118 Ma,which could extend to ca.125 Ma in some locations in Songliao Basin.The major unconformity between the Yingcheng Formation and the Denglouku Formation,which represents the transition of the basin from syn-rift to post-rift is thus confined to between 102.571+0.320/-2.346 Ma and 96.442+0.475/-0.086 Ma.This is roughly contemporaneous with the change in the direction of the paleo-Pacific plate motion from west-southwest to north or northwest in mid-Cretaceous,suggesting their possible connections.

Pore Characteristics and Factors Controlling Lacustrine Shales from the Upper Cretaceous Qingshankou Formation of the Songliao Basin,Northeast China:A Study Combining SEM,Low-temperature Gas Adsorption and MICP Experiments

To investigate pore characteristics and the factors controlling lacustrine shales,geochemical,mineralogical and petrophysical experiments were performed on 23 shale samples from the Qingshankou Formation of the Songliao Basin,China.A comparison of mercury injection capillary pressure(MICP)and low-temperature N2 adsorption pore-size distribution showed that MICP has a higher pore-size distribution(PSD)line in its overlapping pore diameter range,which may be elevated by the higher pressure of MICP.Therefore,in the overlapping range,low-temperature N2 adsorption data were preferred in pore characterization.Negative correlations were observed between pore volumes and TOC content,indicating organic matter pores are not well-developed in the studied samples.This may be related to their low grade of maturity and type I kerogens.There existed negative relationships between pore volumes and S1,which illustrated that liquid hydrocarbons occupied some pore space.Micropore volume had a better correlation with S1 than mesopore and macropore volumes,which suggests that liquid hydrocarbons preferentially occur in micropores.No obvious relationships between pore volumes and quartz or feldspar were observed,while pore volumes increased with the increasing clay mineral content.These relationships indicate that intraparticle pores in clay minerals represent the principal pore type.

Identification Marks of Cretaceous Shallow-Water Delta in the Songliao Basin,China

Shallow-water deltas are now a research focus of international sedimentology. Researchers have recently discovered that water depth is an important controlling factor for the development of shallow deltas, and that significant differences exist between shallow-water deltas and the traditional Gilbert deltas. The identification marks of shallow-water deltas are critical for better understanding sedimentary characteristics of these deltas. In continental basins, especially China＇s Mesozoic and Cenozoic continental basins, shallow-water deltas are widely developed. Thus, this work took the Songliao Basin as an example to analysis this kind of deltas.

Micropaleontology and palaeoclimate during the early Cretaceous in the Lishu depression,Songliao basin,Northeast China

Diverse and abundant microfossils, such as palynomorphs, algae and Ostracoda, were collected from lower Cretaceous strata of Lishu depression, located in southeastern Songliao basin, and were identified and classified in order to provide relevant, detailed records for paleoclimate research. The early Creta- ceous vegetation and climate of southeastern Songliao basin have been inferred from the analysis of palynomorph genera, algae and Ostracoda of the LSI and SW110 wells. The lower Cretaceous strata include, in ascending stratigraphic order, the Shahezi, Yingcheng and Denglouku formations. Palyno- logical assemblages for each formation, based on biostratigraphic and statistical analyses, provide an assessment of their longitudinal variations. During deposition of the Shahezi Formation, the climate was mid-subtropical. Vegetation consisted of coniferous forest and herbage. During deposition of the Ying- cheng Formation, the climate was south Asian tropical. Vegetation consisted mainly of coniferous forest and herbal shrub. In addition, fresh and saline non-marine water dominated the lacustrine setting during deposition of these formations. Deposition of the Denglouku Formation, however, occurred under a hot and dry tropical climate. The vegetation was mostly coniferous forest and lake waters became saline. Palaeoclimate variation is correlated by the lake level change and the development of sedimentary facies. Palaeoclimate contribute to the formation of hydrocarbon source rocks and reservoir.

Lacustrine high resolution sequence records from Upper Cretaceous Nenjiang Formation in Songliao Basin

The Nenjiang Formation was continuously cored in the SK-1 borehole(China Cretaceous Continental Scientific Drilling Project-SongKe1well).Over 95.7%recovery rate,the obtained continuous core is 827.6 m in length,covering the geological age ranges from late Santonian to middle Campanian.This is the most complete and continuous sedimentary deposits in the Songliao basin till now.Here we systematically presented the lithological results of the observation of the cores in 2--5 cm thickness scale at the drilling spot,and the analysis on lithofacies and sedimentary sequence,cyclic stratigraphy.13 types of sedimentary rocks deposited mainly in lacustrine,delta and fluvial environments were found in the Nenjiang Fromation,and they were subdivided into 19 microfacies including dolomite,marl,argillaceous limestone,turbidite,mudstone of still water,volcanic ash,channel-lag deposit,point bar,natural levee,crevasse splay,crevasse channel,floodplain,flood lake,distributary mouth bar,subaqueous distributary channels,subaqueous natural levee,subaqueous inter-distributary bay,distal bar and adjacent shore sand bar.The whole sedimentary column is composed of 630 sixth-order depositional cycles in the meter-scale,which can be further organized in 148 fifth-order depositional cycles,38 fourth-order depositional cycles and 5 third-order depositional cycles.Meticulous depiction(centimeter level)of the whole Formation provides an approach to study its sedimentary process with high precision.The centimeter-scale description of the sequent core presented some previously unidentified dolomite and volcanic ash layers.The cyclostratigraphy of the Nenjiang Formation was controlled by Milankovitch cycled,which is helpful to discover the climatic changes of the late Santonian to the middle Campanian in Songliao Basin.In addition,the detailed description of the sequent section is significant for the upcoming oil and gas exploration in the Songliao Basin if regarding the new type of oil/gas systems.

The Cretaceous Songliao Basin:Volcanogenic Succession,Sedimentary Sequence and Tectonic Evolution,NE China

The Songliao basin （SB） is a superposed basin with two different kinds of basin fills. The lower one is characterized by a fault-bounded volcanogenic succession comprising of intercalated volcanic, pyrodastic and epiclastic rocks. The volcanic rocks, dating from 110 Ma to 130 Ma, are of geochemically active continental margin type. Fast northward migration of the SB block occurred during the major episodes of the volcanism inferred from their paleomagnetic information. The upper one of the basin fill is dominated by non-marine sag-style sedimentary sequence of silicidastics and minor carbonates. The basin center shifted westwards from the early to late Cretaceous revealed by the GGT seismic velocity structure suggesting dynamic change in the basin evolution. Thus, a superposed basin model is proposed. Evolution of the SB involves three periods including （1） Alptian and pre- Aptian： a retroarc basin and range system of Andes type related to Mongolia-Okhotsk collisional belt （MOCB）; （2） Albian to Companian： a sag-like strike-slip basin under transtension related to oblique subduction of the Pacific plate along the eastern margin of the Eurasian plate; （3） since Maastrichtian： a tectonic inverse basin under compression related to normal subduction of the Pacific plate under the Eurasian plate, characterized by overthrust, westward migration of the depocenter and eastward uplifting of the basin margin.

Chronostratigraphy and Stratigraphic Classification of the Cretaceous of the Songliao Basin

Isotopic ages of synsedimentary clay minerals were directly determined with the ultrasonicscattering-settlement separation-K-Ar dilution technique. The apparent age of black mudstoneis 123 Ma for the Quantou Formation, 111.9-89.0 Ma for the Qingshankou Formation and77.6-76.8 Ma for the upper part of the Nenjiang Formation. The Rb-Sr isochrone age of themuddy limestone-mudstone sequence of the lower part of the Nenjiang Formation is 81 Ma andthat of the muddy evaporite of the middle part of the Quantou Formation is 122.2 Ma. On thebasis of the above isotopic ages, the authors propose a modified scheme of stratigraphic classifi-cation of the Cretaceous of the Songliao basin.

Characterizing the Micropores in Lacustrine Shales of the Late Cretaceous Qingshankou Formation of Southern Songliao Basin, NE China

Micropores of shale are significant to the gas content and production potential of shale, which has been verified in the research of marine shale gas; while, few studies have been conducted on lacustrine shales. This study collected 42 samples from three wells in the Late Cretaceous Qingshankou Formation of the southern Songliao Basin, NE China, and investigated these samples by the focused ion beam-scanning electron microscope(FIB–SEM) and nitrogen adsorption analysis techniques. Four types of micropores were identified in the samples, i.e., intergranular pore, intracellular pore, organic matter pore and microfracture. The pore structure type is characterized by open slit pores and "ink type" pores which are mainly 1.5–5 nm in diameter with mesopores as the main pores. The mesopores account for 74.01% of the pore volume and 54.68% of the pore surface area. Compared with the lacustrine shales from the Triassic Yanchang Formation in the Ordos Basin and Xujiahe Formation in the Sichuan Basin, the intergranular clay mineral interlayer pores are considered to be the main reservoir space for shale gas storage in the study area, followed by intraparticle pores, organic matter pores and microfractures. Maturity and micropore are the key controlling factors which affect the shale gas content of the Qingshankou Formation in southern Songliao Basin.

Lithofacies and Pore Structure of Fine-grained Sedimentary Rocks of Qing-1 Member of Cretaceous in the Southern Songliao Basin

Fine-grained sedimentary rocks often contain hydrocarbon and mineral resources.Compared with coarse-grained sedimentary rocks,fine-grained sedimentary rocks are less studied.To elucidate the lithofacies and pore structure of lacustrine fine-grained rocks,the 340.6 m continuous core of Cretaceous Qing-1 Member from five wells in the southern central depression of the Songliao Basin was analyzed using X-ray diffraction,Rock-Eval pyrolysis,low-temperature nitrogen adsorption,high-pressure mercury injection,argon ion polishing-field emission scanning electron microscopy,and laser scanning confocal microscopy.Based on mineral compositions,organic matter abundance and sedimentary structure,lacustrine fine-grained rocks in the study area were divided into ten lithofacies,with their spatial distributions mainly influenced by tectonic cycle,climate cycle and provenance.Furthermore,pore structure characteristics of different lithofacies are summarized.(1)The siliceous mudstone lithofacies with low TOC content and the laminated/layered claybearing siliceous mudstone lithofacies with medium TOC content have the highest proportion of first-class pores(diameter>100 nm),making it the most favourable lithofacies for the accumulation of shale oil and shale gas.(2)The massive claybearing siliceous mudstone lithofacies with low TOC content has the highest proportion of second-class pores(diameter ranges from 10 to 100 nm),making it a favourable lithofacies for the enrichment of shale gas.(3)The massive clay-bearing siliceous mudstone lithofacies with high TOC content has the highest proportion of third-class pores(diameter<10 nm),making it intermediate in gas storage and flow.Laser confocal oil analysis shows that the heavy component of oil is mainly distributed in the clay lamina,while the light part with higher mobility is mainly concentrated in the silty lamina.

Accumulation and exploration of continental shale gas resources of Cretaceous Shahezi Formation in Lishu fault depression,Songliao Basin,NE China

Distribution characteristics,organic matter development characteristics,gas-bearing characteristics,reservoir characteristics,and preservation conditions of the Shahezi Formation shale of Lower Cretaceous in the Lishu fault depression,Songliao Basin,NE China,are analyzed using organic geochemical,whole rock,and SEM analysis data,and CO_(2)and N_(2) adsorption and high-pressure mercury injection experiment data in combination with the tectonic and sedimentation evolution of the region to reveal the geological conditions for enrichment and resource potential of continental shale gas.The organic-rich shale in the Lower Cretaceous of the Lishu fault depression is mainly developed in the lower submember of the second member of the Shahezi Formation(K_(1)sh_(2)^(1) Fm.)and is thick and stable in distribution.The shale has high TOC,mainly types II_(1) and II_(2) organic matter,and is in the mature to the over-mature stage.The volcanic activity,salinization,and reduction of the water environment are conducive to the formation of the organic-rich shale.The shale reservoirs have mainly clay mineral intergranular pores,organic matter pores,carbonate mineral dissolution pores,and foliated microfractures as storage space.The pores are in the mesopore range of 10–50 nm,and the microfractures are mostly 5–10μm wide.Massive argillaceous rocks of lowland and highstand domains are deposited above and below the gas-bearing shale separately in the lower submember of the K_(1)sh_(2)^(1) Fm.,act as the natural roof and floor in the process of shale gas accumulation and preservation,and control the shale gas enrichment.Based on the above understandings,the first shale gas exploration well in Shahezi Formation was drilled in the Lishu fault depression of Songliao Basin.After fracturing,the well tested a daily gas production of 7.6×10^(4) m^(3),marking a breakthrough in continental shale gas exploration in the Shahezi Formation(K1 sh Fm.)of the Lishu fault depression in Songliao Basin.The exploration practice has reference significance for the exploration of continental shale gas in the Lower Cretaceous of Songliao Basin and its periphery.

Reservoir space and enrichment model of shale oil in the first member of Cretaceous Qingshankou Formation in the Changling Sag, southern Songliao Basin, NE China

The lithology, lithofacies, reservoir properties and shale oil enrichment model of the fine-grained sedimentary system in a lake basin with terrigenous clastics of large depression are studied taking the organic-rich shale in the first member of Cretaceous Qingshankou Formation(shortened as Qing 1 Member) in the Changling Sag, southern Songliao Basin as an example. A comprehensive analysis of mineralogy, thin section, test, log and drilling geologic data shows that lamellar shale with high TOC content of semi-deep lake to deep lake facies has higher hydrocarbon generation potential than the massive mudstone facies with medium TOC content, and has bedding-parallel fractures acting as effective reservoir space under over pressure. The sedimentary environments changing periodically and the undercurrent transport deposits in the outer delta front give rise to laminated shale area. The laminated shale with medium TOC content has higher hydrocarbon generation potential than the laminated shale with low TOC content, and the generated oil migrates a short distance to the sandy laminae to retain and accumulate in situ. Ultra-low permeability massive mudstone facies as the top and bottom seals, good preservation conditions, high pressure coefficient, and lamellar shale facies with high TOC are the conditions for "lamellation type" shale oil enrichment in some sequences and zones. The sequence and zone with laminated shale of medium TOC content in oil window and with micro-migration of expelled hydrocarbon are the condition for the enrichment of "lamination type" shale oil. The tight oil and "lamination type" shale oil are in contiguous distribution.

Enrichment and exploration of deep lacustrine shale oil in the first member of Cretaceous Qingshankou Formation, southern Songliao Basin, NE China

Pure shales in the first member of Qingshankou Formation(simplified as Qing 1 Member)in the southern Songliao Basin,i.e.,the semi-deep and deep lacustrine shales,are characterized by a high content of clay minerals and poor hydrocarbon mobility,making the development of shale oil difficult.According to the drilling and testing results,the shale of Qing 1 Member can be classified into 3 lithofacies,i.e.,bedded argillaceous shale,laminated diamictite shale,and interbedded felsic shale.The TOC and brittle minerals control the enrichment of shale oil,of them,TOC controls the total oil content,in other words,the total oil content increases with the increase of TOC;while the laminae made up of brittle minerals contain a large number of bigger intergranular pores which are favorable enrichment space for movable shale oil.In consideration of the origins of the 3 lithofacies,two shale oil enrichment models are classified,i.e.,the deep lacustrine high-TOC bedded argillaceous shale(Model-I)and the semi-deep lacustrine moderate-high-TOC laminated diamictite shale(Model-II).In the Model-I,the shale is characterized by high hydrocarbon generation ability,high total oil content,abundant horizontal bedding fractures,and vertical and high angle fractures locally;the complex fracture network formed by horizontal bedding fractures and vertical fractures improve the storage capacity and permeability of the shale reservoir,increase the enrichment space for movable oil.In the Model-II,the shale is characterized by good hydrocarbon generation ability and fairly high total oil content,and as the brittle laminae contain large intergranular pores,the shale has a higher movable oil content.Based on the two models,shale oil sweet-spot areas of 2880 km2 in the southern Songliao Basin are favorable for further exploration.Aimed at the difficulties in reservoir fracturing of the lacustrine shale with a high content of clay minerals,the composite fracturing technology with supercritical carbon dioxide was used in the shale oil reservoir for the first time,realizing large-scale volume fracturing in shale with a high content of clay minerals and strong heterogeneity,marking a breakthrough of oil exploration in continental shale with a high content of clay minerals in China.

A Floating Astronomical Time Scale for the Early Late Cretaceous Continental Strata in the Songliao Basin, Northeastern China

A continuous terrestrial succession was recovered from the Songke-2(SK-2)borehole in the Songliao Basin,Northeastern China.This borehole provides a unique material for further research on the continental paleoclimate during Cretaceous greenhouse period,following a series of achievements of the Songke-1(SK-1)core.In this study,thorium(Th)logging data were chosen as a paleoclimate proxy to conduct a detailed cyclostratigraphic analysis.The Th series varies quasi-periodically;power spectra and evolutionary fast Fourier transformation(FFT)analysis reveal significant cycles in the Quantou(K2 q),Qingshankou(K2 qn),Yaojia(K2 y)and Nenjiang(K2 n)formations.The ratio of cycle wavelengths in these stratigraphic units is approximately 20:5:2:1,corresponding to long orbital eccentricity(405 kyr),short orbital eccentricity(100 kyr),obliquity(37 kyr),and precession cycles(22.5 kyr and 18.4 kyr).The durations of the K2 n,K2 y,K2 qn and K2 q are estimated as 6.97,1.83,5.30 and 4.52 Myr,respectively,based on the constructed^18.62 Myr"floating"astronomical time scale(ATS).Comparison of the durations between the SK-1 s and SK-2 boreholes exhibits a slight difference of 0.06 Myr and 0.459 Myr for K2 qn and K2 y.Nevertheless,our ATS of K2 n supports the chronostratigraphic frame constructed by the CA-ID-TIMS data of the SK-1 s borehole.This new"floating"ATS provides precise numerical ages for stratigraphic boundaries,biozones and geological events in the Songliao Basin,and can serve as a basis for correlation of strata and events between marine and terrestrial systems.