t-Butyldimethylsilyl (TBDMS) ether can be cleaved upon refluxing in acetone/H2O (95 : 5) in the presence of a catalytic amount of copper (II) chloride dihydrate (5 mmol %).
基金Financial support by National Natural Science Foundation of China !(Grant No. 29972002) isgreatly acknowledged.
文摘t-Butyldimethylsilyl (TBDMS) ether can be cleaved upon refluxing in acetone/H2O (95 : 5) in the presence of a catalytic amount of copper (II) chloride dihydrate (5 mmol %).