Microstructure evolution and its effect on flow stress of TC17 alloy during deformation in α+β two-phase region

The microstructure evolution and its effect on flow stress of TC17 alloy during deformation in the α+β two-phase region were investigated via microstructure characterization and isothermal compression tests. Results showed that the spheroidized rate of α phase at 820 and 850℃ slightly increased with increasing strain. With increasing deformation temperature, the spheroidized rate of α phase showed a slight increasing trend, but the volume fraction of α phase significantly decreased. The flow stress at 780 ℃ and 1 s^-1 decreased continuously and steady state condition was not achieved up to strain of 1.2 due to dislocation annihilation and α lamellae rotation. Under this condition, the dynamic spheroidization was retarded. At the deformation temperatures of 820 and 850℃, and a strain rate of 1 s^-1, a steady state flow stress was observed at strains above 0.8 due to the balance between work hardening and dynamic softening. The dynamic softening was attributed to the α lamellae rotation, dynamic recovery and a little spheroidization.

Quantitative analysis of globularization and modeling of TC17 alloy with basketweave microstructure

The globularization behavior and mechanism of TC17 alloy with basketweave microstructure were investigated, and the models of dynamic and static globularization kinetics were established. The quantitative and metallographic results show that the globularization of α phase is sensitive to the parameters of deformation and heat treatment. By EBSD analysis, the formation and evolution mechanisms of intra-α boundaries are related to discontinuous dynamic recrystallization and continuous dynamic recrystallization, which can form α grains with high and low misorientations between neighbour grains after the heat treatment, respectively. Based on the globularization behavior and mechanism, two modified JMAK models are developed to predict the dynamic and static globularization kinetics, and the mean absolute relative errors(MARE) of 10.67% and 13.80% indicate the accuracy of the dynamic and static globularization kinetics models. The results of this work can provide guidance for controlling microstructure of titanium alloy.

Stress-strain characteristics of linear friction welding of TC11 and TC17 alloys

Abstract Transient stress and strain fields of dissimilar titanium alloys （TCll and TC17 ） joint during linear friction welding （ LFW） were investigated by a two-dimensional model with ABAQUS/Explicit. The results showed that in the X-axis, the maximum compressive stress of 850 MPa occurred in the center zone of friction interface , and the maximum tensile stress of 190 MPa distributed at the flash; in the Y-axis, the maximum compressive stress of 1 261 MPa located at the junction region between the welding fixture and edge of the specimen, and the maximum tensile stress of 320 MPa distributed in the connecting portion between the flash and edge of the specimen. In addition, areas of plastic strain increased gradually during welding process. In the X-axis, tensile strain mainly existed at the heads of the specimens; in the Y-axis, compressive strain mainly occurred at the heads of the specimens.

Influence of heat treatments on microstructure and mechanical properties of laser additive manufacturing Ti-5Al-2Sn-2Zr-4Mo-4Cr titanium alloy

The effect of heat treatments on laser additive manufacturing(LAM)Ti-5Al-2Sn-2Zr-4Mo-4Cr titanium alloy(TC17)was studied aiming to optimize its microstructure and mechanical properties.The as-deposited sample exhibits features of a mixed priorβgrain structure consisting of equiaxed and columnar grains,intragranular ultra-fineαlaths and numerous continuous grain boundaryα(αGB).After being pre-annealed inα+βregion(840°C)and standard solution and aging treated,the continuousαGB becomes coarser and the precipitate free zone(PFZ)nearby theαGB transforms into a zone filled with ultra-fine secondaryα(αS)but no primaryα(αP).When pre-annealed in singleβregion(910°C),allαphases transform intoβphase and the alloying elements distribute uniformly near the grain boundary.DiscontinuousαGB and uniform mixture ofαP andαS near grain boundary form after subsequent solution and aging treatment.The two heat treatments can improve the tensile mechanical properties of LAM TC17to satisfy the aviation standard for TC17.

Uncovering the hierarchical clusters in the heat-affected zone of an electron beam weldedα/βtitanium alloy joint

Using high-resolution transmission Kikuchi diffraction(TKD)and transmission electron microscopy(TEM),we examined the hierarchical clusters that form in situ in the heat-affected zone(HAZ),which are com-monly referred to as“ghost”structures,of bimodal titanium alloy Ti-5Al-2Sn-2Zr-4Mo-4Cr(wt%,TC17).The ghost structures are enriched with Al elements but poor in Mo and Cr compared to the surroundingβmatrix.TKD results show that the ghost structure in middle-HAZ mainly consists ofα_(L)laths with a high-angle grain boundary,which exhibits the classic Burgers orientation relationship(BOR)with the host matrix,while it encircles theα_(P)grains in far-HAZ.And the ghost structure is evidenced to form via in-complete martensitic transformation.TEM results further confirm that the ghost structure is composed ofαL and tinyβ_(L)laths with BOR,with the former being enriched with Al and poor with Cr and Mo,while the latter is the opposite.Interestingly,twoα_(L)variant clusters with a check-mark morphology are fre-quently observed viewed along[0001]_(αL)//[110]_(βL)directions,which are dominated by the crystallographic and geometrical relationships betweenαandβphases.Based on the microstructural characterization,it is hypothesized that the ghost structure is transformed from the initialα_(P)phase,due to the coupling ef-fect of high thermal stress(which induces the formation of a large number of dislocations)and element diffusion caused by sudden temperature increase and plunge cooling in the HAZ during the welding pro-cess.

High-temperature failure mechanism and defect sensitivity of TC17 titanium alloy in high cycle fatigue

Crack initiation is an essential stage of fatigue process due to its direct effect on fatigue failure.However,for titanium alloys in high-temperature high cycle fatigue(HCF),the crack initiation mechanisms remain unclear and the understanding for the defect sensitivity is also lacking.In this study,a series of fatigue tests and multi-scale microstructure characterizations were conducted to explore the high-temperature failure mechanism,and the coupled effect of temperature and defect on TC17 titanium alloy in HCF.It was found that an oxygen-rich layer(ORL)was produced at specimen surface at elevated temperatures,and brittle fracture of ORL at surface played a critical role for surface crack initiation in HCF.Besides,internal crack initiation with nanograins at high temperatures was a novel finding for the titanium alloy.Based on energy dispersive spectroscopy,electron backscatter diffraction and transmission electron microscope characterizations,the competition between surface and internal crack initiations at high temperatures was related to ORL at surface and dislocation resistance in inner microstructure.The fatigue strengths of smooth specimens decreased at elevated temperatures due to the lower dislocation resistance.While the fatigue strengths of the specimens with defect were not very sensitive to the temperatures.Finally,a fatigue strength model considering the coupled effect of temperature and defect was proposed for TC17titanium alloy.