In this research, the changing rules of billet forged Ti-22 Al-24 Nb alloy with various solution time were studied, and the mechanical properties of different microstructure were tested at the room temperature. The re...In this research, the changing rules of billet forged Ti-22 Al-24 Nb alloy with various solution time were studied, and the mechanical properties of different microstructure were tested at the room temperature. The results indicate that the(α2+O+B2) three-phase microstructure with equiaxed grains was acquired by Ti-22 Al-24 Nb alloy billet forging, and the average size of the grains was about 300 μm. With the increase of solution time, the primary lath-shaped O phase began to dissolve, and then the equiaxial α2 phase started to dissolve, but the undissolved α2/O phase began to be equiaxial and grow. The grains of original B2 phase recrystallized and grew. After the 2 h solution treatment, the recrystallization of grains was completed basically and the average size of the grains was about 100 μm. After the 2.5 h solution treatment, the strength of the alloy decreased, and the plasticity increased. However, when the solution treatment increased to 3 h, the plasticity decreased but the strength increased. The optimal solution parameters of Ti-22 Al-24 Nb alloy were the holding time of 2 h, the solution temperature of 1 000 ?C, and water cooling. Excellent comprehensive mechanical properties can be accquired under these parameters. The tensile strength, the yield strength, the elasticity modulus, the elongation, and the section shrinkage were 950 MPa, 915 MPa, 90 GPa, 15.69% and 42.28%, respectively.展开更多
The hot deformation behavior of Ti-22Al-25Nb alloy fabricated by hot compressed sintering was investigated under various conditions of compression tests in the deformation temperature range of 975-1075 °C with 20...The hot deformation behavior of Ti-22Al-25Nb alloy fabricated by hot compressed sintering was investigated under various conditions of compression tests in the deformation temperature range of 975-1075 °C with 20 °C intervals and the strain rate range of 0.001-1.0 s^-1. Based on the experimental data, a novel constitutive relation combining a series of models was developed, including Zener-Hollomon parameter (Z), DRX critical model and kinetics model. The results show that the hot-deformed activation energy Q is calculated to be 410.172 kJ/mol, the ratio of critical strain (εc) to peak strain (εp) is a constant value of about 0.67. The predicted stress obtained by the established constitutive equations matches well with the true stress from experimental data. Despite large errors occur at the stage where strain rate is 0.1 s^-1 and the values of true strain are less than 0.1, the stage of large strain should be more concerned during plastic forming. Furthermore, the predicting accuracy with the DRX kinetics model was testified by an electron back-scattered diffraction (EBSD) technique.展开更多
基金Funded by the National Natural Science Foundation of China(No.51464035)
文摘In this research, the changing rules of billet forged Ti-22 Al-24 Nb alloy with various solution time were studied, and the mechanical properties of different microstructure were tested at the room temperature. The results indicate that the(α2+O+B2) three-phase microstructure with equiaxed grains was acquired by Ti-22 Al-24 Nb alloy billet forging, and the average size of the grains was about 300 μm. With the increase of solution time, the primary lath-shaped O phase began to dissolve, and then the equiaxial α2 phase started to dissolve, but the undissolved α2/O phase began to be equiaxial and grow. The grains of original B2 phase recrystallized and grew. After the 2 h solution treatment, the recrystallization of grains was completed basically and the average size of the grains was about 100 μm. After the 2.5 h solution treatment, the strength of the alloy decreased, and the plasticity increased. However, when the solution treatment increased to 3 h, the plasticity decreased but the strength increased. The optimal solution parameters of Ti-22 Al-24 Nb alloy were the holding time of 2 h, the solution temperature of 1 000 ?C, and water cooling. Excellent comprehensive mechanical properties can be accquired under these parameters. The tensile strength, the yield strength, the elasticity modulus, the elongation, and the section shrinkage were 950 MPa, 915 MPa, 90 GPa, 15.69% and 42.28%, respectively.
基金Project(51405110) supported by the National Natural Science Foundation of ChinaProject(2014M551234) supported by the China Postdoctoral Science Foundation+2 种基金Project(20132302120002) supported by the Specialized Research Fund for the Doctoral Program of Higher Education,ChinaProject(HIT.NSRIF.2014006) supported by the Fundamental Research Funds for the Central Universities,ChinaProject(LBH-Z14096) supported by the Heilongjiang Province Postdoctoral Fund,China
文摘The hot deformation behavior of Ti-22Al-25Nb alloy fabricated by hot compressed sintering was investigated under various conditions of compression tests in the deformation temperature range of 975-1075 °C with 20 °C intervals and the strain rate range of 0.001-1.0 s^-1. Based on the experimental data, a novel constitutive relation combining a series of models was developed, including Zener-Hollomon parameter (Z), DRX critical model and kinetics model. The results show that the hot-deformed activation energy Q is calculated to be 410.172 kJ/mol, the ratio of critical strain (εc) to peak strain (εp) is a constant value of about 0.67. The predicted stress obtained by the established constitutive equations matches well with the true stress from experimental data. Despite large errors occur at the stage where strain rate is 0.1 s^-1 and the values of true strain are less than 0.1, the stage of large strain should be more concerned during plastic forming. Furthermore, the predicting accuracy with the DRX kinetics model was testified by an electron back-scattered diffraction (EBSD) technique.
