Superplastic properties and microstructural evolution of a Ti-24Al-14Nb-3V-0.5Mo (at. pct) intermetallic alloy were studied. Optimum superplastic properties were obtained for temperatures in the interval 960℃≤5 T≤5...Superplastic properties and microstructural evolution of a Ti-24Al-14Nb-3V-0.5Mo (at. pct) intermetallic alloy were studied. Optimum superplastic properties were obtained for temperatures in the interval 960℃≤5 T≤5980℃. The apparent activation energy in the superplastic regime was determined and the deformation mechanism was also discussed. Based on the studies, a curve panel with three sheets sandwich structure was fabricated successfully. The microstructures corresponding to different strain in the part were also studied.展开更多
The processing maps were used to identify the optimal forging parameters of Ti-24A1- 17Nb-0.5Mo alloy by evaluating the flow data according to the DMM model. The actual local strain rate and strain distribution in the...The processing maps were used to identify the optimal forging parameters of Ti-24A1- 17Nb-0.5Mo alloy by evaluating the flow data according to the DMM model. The actual local strain rate and strain distribution in the samples were obtained by finite element calculations. The local microstructures of the deformed samples were related to the local deformation parameters and correlated with the processing maps at 0.3, 0.4, 0.5 and 0.6 of logarithmic strain. Flow regimes predicted by DMM analysis were then correlated with the local microstructural observations. Five domains of efficient coefficient could be distinguished. Unstable regions were microstructurally related to shear band formation within the （~2~B2 phase deformation field, and to flow localiza- tion at grain boundaries of B2 phase in the near B2 phase deformation field. Stable flow regimes were shown to be associated with dynamic globularization of the plate- like a2 in the a2＋B2 phase deformation zone, and with dynamic recrystallization of B2 in the near B2 phase deformation zone.展开更多
In this work, hot isostatic pressing （HIPing） technique was used to densify the Ti2AINb pre-alloyed powder. The influence of HIPing loading route parameters （temperature and rates of heating and pressurizing） on m...In this work, hot isostatic pressing （HIPing） technique was used to densify the Ti2AINb pre-alloyed powder. The influence of HIPing loading route parameters （temperature and rates of heating and pressurizing） on microstructure and properties of PM Ti2AINb alloys was studied. The results showed that HIPing loading route parameters affected the densification process and mechanical properties （especially high temper- ature rupture lifetime） of PM Ti2AINb alloys in the present work. A finite element method （FEM） model for predicting the final densification was developed and was used to optimize the HIPing procedure.展开更多
Ti2 AlNb-based alloy powder metallurgy(PM)compacts were prepared via hot isostatic pressing(HIP)under relatively low temperature(920 and 980℃)and at certain pressure(130 MPa).The microstructure,composition and orient...Ti2 AlNb-based alloy powder metallurgy(PM)compacts were prepared via hot isostatic pressing(HIP)under relatively low temperature(920 and 980℃)and at certain pressure(130 MPa).The microstructure,composition and orientation of B2,α2 and O phases in the compacts were characterized and analyzed with an aim to investigate the effect of unsuitable HIPping parameters on the appearance of prior particle boundary(PPB),which seriously affects the mechanical properties of the alloy.The results show that moreα2 phase is the characteristics of the PPB in Ti2AlNb-based alloy when HIPped at relatively low temperature.Increasing HIPping temperature to the upper part of the two-phase region can effectively inhibit the formation of PPB.Electron backscatter diffraction measurements show the specific orientation relationship between phases,which helps us understand the origin of a2 and O phase and the corresponding transformation path.The HIPping at a higher temperature can weaken the micro-texture intensity of theα2 and O phase due to the increase of misorientation in B2 phase.Theα2 phase at cell wall keeps the Burgers orientation relationship(BOR)with the grain on one side,and does not satisfy the BOR with the other.It is found that some O phase variants inside the cell HIPped at 980℃can only maintainα2-O OR withα2 owing to theα2→O phase transformation forming the O phase,while these O variants deviate from B2-O OR with B2 phase.展开更多
Pre-alloyed powder of Ti-22Al-24Nb-0.5Mo（atomic fraction,%） was prepared by gas atomization.Powder metallurgy（PM） Ti 2AlNb alloys were prepared by a hot isostatic pressing（HIPing） route.The influence of experime...Pre-alloyed powder of Ti-22Al-24Nb-0.5Mo（atomic fraction,%） was prepared by gas atomization.Powder metallurgy（PM） Ti 2AlNb alloys were prepared by a hot isostatic pressing（HIPing） route.The influence of experimental variables including HIPing temperatures,solution and aging temperatures on microstructure and properties of PM Ti 2AlNb alloys was studied.The results showed that HIPing temperature affected the porosity distribution and mechanical properties of PM Ti 2AlNb alloys.The microstructure and mechanical properties of the PM Ti 2AlNb alloys changed obviously after various post heat treatments,and a good combination of tensile strength,ductility and rupture lifetime was obtained through an optimized heat treatment in the present work.展开更多
文摘Superplastic properties and microstructural evolution of a Ti-24Al-14Nb-3V-0.5Mo (at. pct) intermetallic alloy were studied. Optimum superplastic properties were obtained for temperatures in the interval 960℃≤5 T≤5980℃. The apparent activation energy in the superplastic regime was determined and the deformation mechanism was also discussed. Based on the studies, a curve panel with three sheets sandwich structure was fabricated successfully. The microstructures corresponding to different strain in the part were also studied.
文摘The processing maps were used to identify the optimal forging parameters of Ti-24A1- 17Nb-0.5Mo alloy by evaluating the flow data according to the DMM model. The actual local strain rate and strain distribution in the samples were obtained by finite element calculations. The local microstructures of the deformed samples were related to the local deformation parameters and correlated with the processing maps at 0.3, 0.4, 0.5 and 0.6 of logarithmic strain. Flow regimes predicted by DMM analysis were then correlated with the local microstructural observations. Five domains of efficient coefficient could be distinguished. Unstable regions were microstructurally related to shear band formation within the （~2~B2 phase deformation field, and to flow localiza- tion at grain boundaries of B2 phase in the near B2 phase deformation field. Stable flow regimes were shown to be associated with dynamic globularization of the plate- like a2 in the a2＋B2 phase deformation zone, and with dynamic recrystallization of B2 in the near B2 phase deformation zone.
文摘In this work, hot isostatic pressing （HIPing） technique was used to densify the Ti2AINb pre-alloyed powder. The influence of HIPing loading route parameters （temperature and rates of heating and pressurizing） on microstructure and properties of PM Ti2AINb alloys was studied. The results showed that HIPing loading route parameters affected the densification process and mechanical properties （especially high temper- ature rupture lifetime） of PM Ti2AINb alloys in the present work. A finite element method （FEM） model for predicting the final densification was developed and was used to optimize the HIPing procedure.
基金The supports from the National Key Research and Development Program of China (No.2016YFB0701304)the CAS Informatization Project (No.XXH13506-304)the Doctoral Scientific Research Foundation of Liaoning Province (No.20180540133)
文摘Ti2 AlNb-based alloy powder metallurgy(PM)compacts were prepared via hot isostatic pressing(HIP)under relatively low temperature(920 and 980℃)and at certain pressure(130 MPa).The microstructure,composition and orientation of B2,α2 and O phases in the compacts were characterized and analyzed with an aim to investigate the effect of unsuitable HIPping parameters on the appearance of prior particle boundary(PPB),which seriously affects the mechanical properties of the alloy.The results show that moreα2 phase is the characteristics of the PPB in Ti2AlNb-based alloy when HIPped at relatively low temperature.Increasing HIPping temperature to the upper part of the two-phase region can effectively inhibit the formation of PPB.Electron backscatter diffraction measurements show the specific orientation relationship between phases,which helps us understand the origin of a2 and O phase and the corresponding transformation path.The HIPping at a higher temperature can weaken the micro-texture intensity of theα2 and O phase due to the increase of misorientation in B2 phase.Theα2 phase at cell wall keeps the Burgers orientation relationship(BOR)with the grain on one side,and does not satisfy the BOR with the other.It is found that some O phase variants inside the cell HIPped at 980℃can only maintainα2-O OR withα2 owing to theα2→O phase transformation forming the O phase,while these O variants deviate from B2-O OR with B2 phase.
文摘Pre-alloyed powder of Ti-22Al-24Nb-0.5Mo（atomic fraction,%） was prepared by gas atomization.Powder metallurgy（PM） Ti 2AlNb alloys were prepared by a hot isostatic pressing（HIPing） route.The influence of experimental variables including HIPing temperatures,solution and aging temperatures on microstructure and properties of PM Ti 2AlNb alloys was studied.The results showed that HIPing temperature affected the porosity distribution and mechanical properties of PM Ti 2AlNb alloys.The microstructure and mechanical properties of the PM Ti 2AlNb alloys changed obviously after various post heat treatments,and a good combination of tensile strength,ductility and rupture lifetime was obtained through an optimized heat treatment in the present work.
