Titanium dioxide/ kaolinite nanocomposite was prepared by the sol-gel method, with layered kaolinite as a substrate and Ti （ OC4H9 ）4 as a precursor. The effects of hydrolysis, drying and calcination on the producti...Titanium dioxide/ kaolinite nanocomposite was prepared by the sol-gel method, with layered kaolinite as a substrate and Ti （ OC4H9 ）4 as a precursor. The effects of hydrolysis, drying and calcination on the production of nanometric titanium dioxide were discussed. The optimal conditions for preparation were＂ bbtained through experiments. The 1- 10 nrn thick monolayer anatase nano TiO2 crystal was produced under the conditions as follows： hydrolyzed at 37-42 ℃ for 4 h, dried at 70-80 ℃ for 1 h, and calcined at 550-650℃ for 3 h. The rate of degradation of 40 mg/ L azo dye and 20 mg/ L acid red dye can reuch 96% and 81.45%, respectively.展开更多
基金Funded by National "973" Plan Research Project ( No.2004CB619204) and Educational Ministry Scientific and Technologi-cal Research Key Project (No.02052)
文摘Titanium dioxide/ kaolinite nanocomposite was prepared by the sol-gel method, with layered kaolinite as a substrate and Ti （ OC4H9 ）4 as a precursor. The effects of hydrolysis, drying and calcination on the production of nanometric titanium dioxide were discussed. The optimal conditions for preparation were＂ bbtained through experiments. The 1- 10 nrn thick monolayer anatase nano TiO2 crystal was produced under the conditions as follows： hydrolyzed at 37-42 ℃ for 4 h, dried at 70-80 ℃ for 1 h, and calcined at 550-650℃ for 3 h. The rate of degradation of 40 mg/ L azo dye and 20 mg/ L acid red dye can reuch 96% and 81.45%, respectively.
