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Synthesis and Characterization of MgSb2O6 Trirutile-Type in Low Presence Concentrations of Ethylenediamine
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作者 H. Guillen-Bonilla J. Reyes-Gomez +4 位作者 A. Guillen-Bonilla D. Pozas-Zepeda J. T. Guillen-Bonilla L. Gildo Ortiz M. Flores Martinez 《Journal of Chemistry and Chemical Engineering》 2013年第5期395-401,共7页
The nanoparticles MgSb206 with trirutile-type structure were prepared by colloidal method using ethylanediamine (0.5 and 0.75 mL), following a calcination at 800 ℃. After, those powders were analyzed by x-ray obtai... The nanoparticles MgSb206 with trirutile-type structure were prepared by colloidal method using ethylanediamine (0.5 and 0.75 mL), following a calcination at 800 ℃. After, those powders were analyzed by x-ray obtaining a tetragonal structure with cell parameters, a = 4.64 A and c = 9.25 A and special group P42/mnm. Using a scanning electron microscopy were analyzed the powders calcined at 800 ℃, showing the formation of micro-plates, micro-rods, nanoparticles and morphology as rice grains. Employing a transmission electron microscopy, were found nanostructures hexagonal shaped with sizes of- 33.6 nm (0.5 mL) and 28.6 nm (0.75 mL). 展开更多
关键词 trirutile ETHYLENEDIAMINE morphology nanostructures.
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