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Effects of Ethanol Condensation Reflux Extraction and Ultrasound-assisted Extraction on the Content of Total Flavonoids of Pueraria edulis
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作者 Jun TANG Jianguang ZENG +1 位作者 Hao LI Chenzhong JIN 《Agricultural Biotechnology》 CAS 2023年第2期91-95,104,共6页
With Pueraria edulis from different habitats in Yunnan Province,Guangdong Province and Guangxi Zhuang autonomous region as materials,the medicinal materials of P.edulis were extracted by ethanol condensation reflux ex... With Pueraria edulis from different habitats in Yunnan Province,Guangdong Province and Guangxi Zhuang autonomous region as materials,the medicinal materials of P.edulis were extracted by ethanol condensation reflux extraction and ultrasound-assisted extraction,and the effects of different extraction methods the contents of total flavonoids in P.edulis from different areas were compared.The results showed that the best extraction time for P.edulis in Yunnan Province was 20 min,and that for Guangdong and Guangxi Zhuang Autonomous Region was 30 min.The yield of total flavonoids from P.edulis extracted by the condensation reflux extraction method was relatively better.The content of total flavonoids in P.edulis in Yunnan was the highest with an average content of 0.2557%,while the average content of total flavonoids in P.edulis in Guangdong was the lowest with an average content of 0.2108%. 展开更多
关键词 Pueraria edulis Total flavonoids Condensation reflux extraction method ultrasound-assisted extraction
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Optimization of Ultrasound-assisted Extraction Conditions for Polysaccharides from Pinus tabulaeformis Seed Shells
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作者 蒋龙 杨国庆 +2 位作者 杨鹏 刘伟 张大伟 《Agricultural Science & Technology》 CAS 2013年第12期1826-1829,共4页
[Objective] This study aimed to investigate the optimal technological condi- tions for ultrasouqd-assisted extraction of polysaccharides from Pinus tabulaeformis seed shells. [Melhod] Polysaccharides were extracted fr... [Objective] This study aimed to investigate the optimal technological condi- tions for ultrasouqd-assisted extraction of polysaccharides from Pinus tabulaeformis seed shells. [Melhod] Polysaccharides were extracted from P. tabulaeformis seed shells by ultrasound-assisted hot water extraction method and detected by phenol- concentrated sulfuric acid method. The effect of extraction temperature, extraction duration, solid-liquid ratio and extraction frequency on the extraction of polysaccha- rides was investigated using single-factor gradient experiment and the extraction conditions for polysaccharides from P. tabulaeformis seed shells were optimized us- ing L9(34) orthogonal design. [Result] The content of polysaccharides extracted twice at 60 ℃ for 25 min with solid-liquid ratio of 1:3.5 reached the maximum. The re- covery rate (n=-5) ranged from 97.71% to 100.67% and RSD was 1.56%, suggesting high stability. [Conclusion] A simple and efficient method for ultrasound-assisted ex- traction of polysaccharides from P. tabulaeformis seed shells was established in this study, which laid solid foundation for the development and utilization of abandoned pine nut shell resources. 展开更多
关键词 ultrasound-assisted extraction Spectrophotography Pinus tabulaeformis seed shells Polvsaccharides
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Optimized Ultrasound-assisted Extraction of Proacyanidins from Purple Cabbage 被引量:2
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作者 栾娜 刘行 《Agricultural Science & Technology》 CAS 2013年第3期512-515,519,共5页
[Objective] The paper was to optimize ultrasound-assisted extraction of proacyanidins from purple cabbage. [Method] The ultrasound-assisted extraction technology was used to study the extraction of proacyanidins from ... [Objective] The paper was to optimize ultrasound-assisted extraction of proacyanidins from purple cabbage. [Method] The ultrasound-assisted extraction technology was used to study the extraction of proacyanidins from purple cabbage. The effect of ethanol concentration, temperature, time, material-solution ratio and the power of ultrasound on extracting efficiency were studied by single-factor experiment. Based on this, L16(4%orthogonal test were conducted to determine the optimal condi- tion for extraction of proacyanidins from purple cabbage. [Result] The optimal condi- tion for extraction of proacyanidins from purple cabbage was as follows: ethanol concentration 50%, extraction temperature 50℃, extraction time 1 h, extraction power 540 W, material-liquid ratio 1:20. The extraction rate of procyanidins under this condition reached 104.8 mg/g. [Conclusion] The study provided a theoretical basis for scientific and reasonable utilization of procyanidins in purple cabbage. 展开更多
关键词 Purple cabbage Proacyanidins ULTRASOUND extraction
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Optimization of ultrasound-assisted extraction of camptothecin from Camptotheca acuminata seeds 被引量:2
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作者 JING Li-jia LI Si-yang CHANG Zui WANG Yang YAN Xiu-feng 《Journal of Forestry Research》 SCIE CAS CSCD 2011年第2期239-242,共4页
Naturally occurring camptothecin(CPT) is an important source of chemotherapeutic agents.The extraction from Camptotheca acuminata is still the main approach to obtain CPT compared with total synthesis.In the present... Naturally occurring camptothecin(CPT) is an important source of chemotherapeutic agents.The extraction from Camptotheca acuminata is still the main approach to obtain CPT compared with total synthesis.In the present study,ultrasound-assisted extractions(UAE) of CPT from C.acuminata seeds with alkaline solutions were investigated and CPT yield were determined by High Performance Liquid Chromatography.The conditions of alkaline species and concentrations,extraction time,extraction temperature and ultrasonic power were optimized.Results show that both Na3PO4 and Na2CO3 solutions gain good extraction yields,whereas Na3PO4 solution has stronger basicity and need higher concentration than Na2CO3 solution does,thus aqueous Na2CO3 is more beneficial for the extraction.The optimal condition was ultrasonically extracted with 0.5% aqueous Na2CO3 at 50°C and ultrasonic power of 400 W for 60 min.Comparing with UAE with ethanol,the extraction with 0.5% Na2CO3 solution achieves higher yield.Moreover,aqueous Na2CO3 as a solvent has various advantages including non-toxicity,inflammable,non-corrosive and low cost,which ensure this UAE method is a superior method with high utilizing prospect. 展开更多
关键词 CAMPTOTHECIN Camptotheca acuminata ultrasound-assistant extraction
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Study on the Technological Conditions of Ultrasound-assisted Extraction of Polysaccharides from Ajuga ciliata Bunge (Fujian) 被引量:1
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作者 Wenwen LU Ruonan HE +3 位作者 Zhongwei CHEN Chao YI Zhuangyu ZHANG Yanyan ZHENG 《Medicinal Plant》 CAS 2021年第1期51-55,共5页
[Objectives]To determine the optimum technological conditions of ultrasound-assisted extraction of polysaccharides from Ajuga ciliata Bunge.[Methods]In this study,Ajuga ciliata Bunge was used as raw material,and an or... [Objectives]To determine the optimum technological conditions of ultrasound-assisted extraction of polysaccharides from Ajuga ciliata Bunge.[Methods]In this study,Ajuga ciliata Bunge was used as raw material,and an orthogonal experiment was designed based on the single factor experiment to investigate the effects of ultrasonic time,solid-liquid ratio,ultrasonic temperature and ultrasonic power on the extraction rate of polysaccharides from A.ciliata Bunge(Fujian).Range analysis,variance analysis and SSR test of significant differences between groups were carried out with SPSS 20.0,and the test results were verified.[Results]Under the conditions of ultrasonic temperature of 85℃,ultrasonic time of 80 min,solid-liquid ratio of 1∶15 g/mL and ultrasonic power of 500 W,the yield of polysaccharides from A.ciliata Bunge(Fujian)was the best.[Conclusions]This study can provide theoretical basis for the application of A.ciliata Bunge(Fujian). 展开更多
关键词 Ajuga ciliata Bunge POLYSACCHARIDE Ultrasonic extraction Orthogonal test
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Effect of Ultrasound-Assisted Extraction of Phenolic Compounds on the Characteristics of Walnut Shells
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作者 Hannah Han Shusheng Wang +3 位作者 Milan Rakita Yanting Wang Qingyou Han Qin Xu 《Food and Nutrition Sciences》 2018年第8期1034-1045,共12页
Walnuts are one of nature’s more waste-heavy products. 67% of the nut is shell and husk, low value by-products that are rich in phenolic compounds. The phenolic compounds extracted from walnut shells are potentially ... Walnuts are one of nature’s more waste-heavy products. 67% of the nut is shell and husk, low value by-products that are rich in phenolic compounds. The phenolic compounds extracted from walnut shells are potentially good natural sources of antioxidants for the food and pharmaceutical industries. In this study, phenolic compounds were extracted using an ultrasonic bath, an ultrasonic probe and a standard shaking method. The extraction yield achieved with an ultrasonic probe was 51.2 mg GAE/g DW, two times higher than both the shaking method and the ultrasonic bath method which were 20.6 mg GAE/g DW and 25.8 mg GAE/g DW, respectively. Phenolic extraction was further improved by a size reduction of the walnut shells. The best extraction yield of 52.8 mg GAE/g DW was attained when the particle size was between 45 - 100 mesh. The ultrasonic probe treatment is the best method for extraction of phenolic compounds from walnut shells. Scanning electron microscopy (SEM) imaging indicated that the ultrasonic probe treatment could better rupture the hard structure of the cells, increasing the penetration of solvents and thus the extraction yield. 展开更多
关键词 WALNUT SHELL ultrasound-assisted extraction TOTAL PHENOLIC Content (TPC) Particle Size SEM Analysis
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Ultrasound-assisted extraction of antioxidant polyphenolic compounds from Nephelium lappaceum L.(Mexican variety) husk
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作者 Adriana Méndez-Flores Ayerim Hérnandez-Almanza +3 位作者 Aidé Sáenz-Galindo Jesús Morlett-Chávez Cristóbal N Aguilar Juan Ascacio-Valdés 《Asian Pacific Journal of Tropical Medicine》 SCIE CAS 2018年第12期676-681,共6页
Objective: To reach the recovery and identification of antioxidant polyphenolic compounds from Nephelium lappaceum L.(Mexican variety) husk using ultrasound-assisted extraction and liquid chromatography/mass spectrome... Objective: To reach the recovery and identification of antioxidant polyphenolic compounds from Nephelium lappaceum L.(Mexican variety) husk using ultrasound-assisted extraction and liquid chromatography/mass spectrometry as well as the in vitro antioxidant activity. Methods: Rambutan husk extracts were obtained by ultrasound-assisted extraction, mass/volume ratio, water/ethanol percentage and extraction time were evaluated. Once the best extraction condition of polyphenolic compounds was defined, a polyphenolic fraction was recovered using Ambetlite XAD-16. The total content of antioxidant polyphenolic compounds was determined by summation of the total hydrolysable polyphenol and total condensed polyphenol contents. Recovered compounds were identified by FTIR(ATR) spectroscopy and HPLC/ESI/MS. The antioxidant activity was carried out by ABTS, DPPH and lipid oxidation inhibition in vitro methods. Results: In Mexican variety rambutan husk, the total polyphenolic content was 487.67 mg/g, after ultrasound-assisted extraction. According to the HPLC/ESI/MS analysis 12 antioxidant polyphenolic compounds were identified, mostly ellagitannins such as geraniin, corilagin and ellagic acid. The antioxidant activity determined by ABTS, DPPH and lipid oxidation inhibition methods was demonstrated. The main functional groups of the identified compounds were determined by FTIR analysis. Conclusions: It was demonstrated that ultrasound-assisted extraction was effective and allowed the extraction and recovery of antioxidant polyphenolic compounds. Furthermore Mexican variety rambutan husk is an important source for recovering polyphenolic compounds with antioxidant activity, these compounds have potential application for the treatment/prevention of various diseases related to cancer and pathogenic microorganisms. 展开更多
关键词 MEXICAN VARIETY RAMBUTAN ULTRA-SOUND assisted extraction ANTIOXIDANT polyphenolic COMPOUNDS HPLC/ESI/MS
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Ultrasound-assisted extraction of bound phenolic compounds from the residue of Apocynum venetum tea and their antioxidant activities 被引量:2
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作者 Shengwei Sun Yiwen Zhao +10 位作者 Luyao Wang Yuzhi Tan Yaning Shi Rita-Cindy Aye-Ayire Sedjoah Yuting Shao Longxiang Li Mengxi Wang Jiashuai Wan Xia Fan Rong Guo Zhihong Xin 《Food Bioscience》 SCIE 2022年第3期502-511,共10页
Bound phenolic compounds from the residue of Apocynum venetum(A.venetum)tea were released by alkaline digestion with sonication,followed by extraction using ethyl acetate(EtOAc).The fragment ions of compounds in free ... Bound phenolic compounds from the residue of Apocynum venetum(A.venetum)tea were released by alkaline digestion with sonication,followed by extraction using ethyl acetate(EtOAc).The fragment ions of compounds in free and bound forms were identified by liquid chromatography electrospray ionization tandem mass spectrometry(LC-ESI-MS/MS)in both positive and negative modes.Further investigation of chemical constituents in the EtOAc extract led to the isolation of eleven individual compounds,and their chemical structures were identified as(−)-epicatechin(1),(−)-loliolide(2),(−)-syringaresinol-4-O-β-D-glucopyranoside(3),alloside of benzyl alcohol(4),3-[(6-O-hexopyranosylhexopyranosyl)oxy]-2-(palmitoyloxy)propyl(9Z,12Z,15Z)-9,12,15-octadecatrienoate(5),apocynoside I(6),quercetin-3-O-β-D-glucopyranoside(7),kaempferol-3-O-β-D-glucopyranoside(8),[1-acetyloxy-3-[3,4,5-trihydroxy-6-[[3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxymethyl]oxan-2-yl]oxypropan-2-yl]hexadecanoate(9),1-stearoyl-2-palmitoyl-sn-glycerol(10),and 3-hexene-l-O-β-D-glucoside(11)using a series of spectroscopic methods.Compounds 2–5 and 9–11 were isolated for the first time from A.venetum,while antioxidant experiments showed that compounds 1,7,and 8 displayed strong DPPH and ABTS+radical scavenging activities.This study represents the first investigation of bound phenolic compounds with potential health benefits in the residue of A.venetum tea. 展开更多
关键词 Apocynum venetum.L tea residue ultrasound-assisted extraction Bound phenolic compounds Structural characterization Antioxidant activity
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Evaluation of Oil Yield of Oil Shale by Infrared Spectrometry Coupled with Ultrasound-assisted Extraction 被引量:1
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作者 ZHAO Zhenying LIN Jun +2 位作者 YU Yong HOU Chuanbin SUN Yuyang 《Chemical Research in Chinese Universities》 SCIE CAS CSCD 2015年第3期352-356,共5页
The oil yield of oil shale was evaluated by Fourier transform infrared(FTIR) spectrometry coupled with ultrasound-assisted extraction. The extraction conditions, including the amount of sample, extraction time and e... The oil yield of oil shale was evaluated by Fourier transform infrared(FTIR) spectrometry coupled with ultrasound-assisted extraction. The extraction conditions, including the amount of sample, extraction time and extrac- tion temperature, were examined and optimized. Twenty-four oil shale samples were collected and divided into calibration set and prediction set randomly with a ratio of 2:1. The oil yields of all the samples were determined by the routine method(low-temperature retorting) for reference. The linear regression(LR) equations of oil yield vs. the total area of the spectrum peaks in a wavenumber range of 3100--2800 cm-1 as well as the sum of absorbance of three absorption peaks(2855, 2927 and 2955 cm-l), and the multiple linear regression(MLR) model of oil yield vs. the absorbances of the three absorption peaks were constructed with the samples in calibration set and applied to the evaluation of the oil yields of the samples in prediction set, respectively. The results show that the MLR model provides more accurate predictions than the other LR two equations. The determination coefficient(P2p ), the root- mean-square error of prediction(RMSEP) and the residual prediction deviation(RPD) of the MLR model are 0.9616, 0.6458 and 3.6, respectively. The present method is a rapid and effective alternative to the routine low-temperature retorting method. 展开更多
关键词 Oil shale Oil yield ultrasound-assisted extraction Infrared spectroscopy Multiple linear regression
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A Review on Sources,Extractions and Analysis Methods of a Sustainable Biomaterial:Tannins 被引量:2
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作者 Antonio Pizzi Marie-Pierre Laborie Zeki Candan 《Journal of Renewable Materials》 EI CAS 2024年第3期397-425,共29页
Condensed and hydrolysable tannins are non-toxic natural polyphenols that are a commercial commodity industrialized for tanning hides to obtain leather and for a growing number of other industrial applications mainly ... Condensed and hydrolysable tannins are non-toxic natural polyphenols that are a commercial commodity industrialized for tanning hides to obtain leather and for a growing number of other industrial applications mainly to substitute petroleum-based products.They are a definite class of sustainable materials of the forestry industry.They have been in operation for hundreds of years to manufacture leather and now for a growing number of applications in a variety of other industries,such as wood adhesives,metal coating,pharmaceutical/medical applications and several others.This review presents the main sources,either already or potentially commercial of this forestry by-materials,their industrial and laboratory extraction systems,their systems of analysis with their advantages and drawbacks,be these methods so simple to even appear primitive but nonetheless of proven effectiveness,or very modern and instrumental.It constitutes a basic but essential summary of what is necessary to know of these sustainable materials.In doing so,the review highlights some of the main challenges that remain to be addressed to deliver the quality and economics of tannin supply necessary to fulfill the industrial production requirements for some materials-based uses. 展开更多
关键词 TANNINS FLAVONOIDS SOURCES extraction methods analysis methods
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Feature extraction for machine learning-based intrusion detection in IoT networks 被引量:1
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作者 Mohanad Sarhan Siamak Layeghy +2 位作者 Nour Moustafa Marcus Gallagher Marius Portmann 《Digital Communications and Networks》 SCIE CSCD 2024年第1期205-216,共12页
A large number of network security breaches in IoT networks have demonstrated the unreliability of current Network Intrusion Detection Systems(NIDSs).Consequently,network interruptions and loss of sensitive data have ... A large number of network security breaches in IoT networks have demonstrated the unreliability of current Network Intrusion Detection Systems(NIDSs).Consequently,network interruptions and loss of sensitive data have occurred,which led to an active research area for improving NIDS technologies.In an analysis of related works,it was observed that most researchers aim to obtain better classification results by using a set of untried combinations of Feature Reduction(FR)and Machine Learning(ML)techniques on NIDS datasets.However,these datasets are different in feature sets,attack types,and network design.Therefore,this paper aims to discover whether these techniques can be generalised across various datasets.Six ML models are utilised:a Deep Feed Forward(DFF),Convolutional Neural Network(CNN),Recurrent Neural Network(RNN),Decision Tree(DT),Logistic Regression(LR),and Naive Bayes(NB).The accuracy of three Feature Extraction(FE)algorithms is detected;Principal Component Analysis(PCA),Auto-encoder(AE),and Linear Discriminant Analysis(LDA),are evaluated using three benchmark datasets:UNSW-NB15,ToN-IoT and CSE-CIC-IDS2018.Although PCA and AE algorithms have been widely used,the determination of their optimal number of extracted dimensions has been overlooked.The results indicate that no clear FE method or ML model can achieve the best scores for all datasets.The optimal number of extracted dimensions has been identified for each dataset,and LDA degrades the performance of the ML models on two datasets.The variance is used to analyse the extracted dimensions of LDA and PCA.Finally,this paper concludes that the choice of datasets significantly alters the performance of the applied techniques.We believe that a universal(benchmark)feature set is needed to facilitate further advancement and progress of research in this field. 展开更多
关键词 Feature extraction Machine learning Network intrusion detection system IOT
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Experimental investigation on coal pore-fracture variation and fractal characteristics synergistically affected by solvents for improving clean gas extraction 被引量:1
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作者 Feilin Han Sheng Xue +3 位作者 Chunshan Zheng Zhongwei Chen Guofu Li Bingyou Jiang 《International Journal of Mining Science and Technology》 SCIE EI CAS CSCD 2024年第3期413-425,共13页
Chemical solvents instead of pure water being as hydraulic fracturing fluid could effectively increase permeability and improve clean methane extraction efficiency.However,pore-fracture variation features of lean coal... Chemical solvents instead of pure water being as hydraulic fracturing fluid could effectively increase permeability and improve clean methane extraction efficiency.However,pore-fracture variation features of lean coal synergistically affected by solvents have not been fully understood.Ultrasonic testing,nuclear magnetic resonance analysis,liquid phase mass spectrometry was adopted to comprehensively analyze pore-fracture change characteristics of lean coal treated by combined solvent(NMP and CS_(2)).Meanwhile,quantitative characterization of above changing properties was conducted using geometric fractal theory.Relationship model between permeability,fractal dimension and porosity were established.Results indicate that the end face fractures of coal are well developed after CS2and combined solvent treatments,of which,end face box-counting fractal dimensions range from 1.1227 to 1.4767.Maximum decreases in ultrasonic longitudinal wave velocity of coal affected by NMP,CS_(2)and combined solvent are 2.700%,20.521%,22.454%,respectively.Solvent treatments could lead to increasing amount of both mesopores and macropores.Decrease ratio of fractal dimension Dsis 0.259%–2.159%,while permeability increases ratio of NMR ranges from 0.1904 to 6.4486.Meanwhile,combined solvent could dissolve coal polar and non-polar small molecules and expand flow space.Results could provide reference for solvent selection and parameter optimization of permeability-enhancement technology. 展开更多
关键词 Clean gas extraction Chemical solvent Experimental investigation Fractal characteristics Pore fracture
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Automatic Extraction Method of 3D Feature Guidelines for Complex Cultural Relic Surfaces Based on Point Cloud 被引量:1
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作者 GENG Yuxin ZHONG Ruofei +1 位作者 HUANG Yuqin SUN Haili 《Journal of Geodesy and Geoinformation Science》 CSCD 2024年第1期16-41,共26页
Cultural relics line graphic serves as a crucial form of traditional artifact information documentation,which is a simple and intuitive product with low cost of displaying compared with 3D models.Dimensionality reduct... Cultural relics line graphic serves as a crucial form of traditional artifact information documentation,which is a simple and intuitive product with low cost of displaying compared with 3D models.Dimensionality reduction is undoubtedly necessary for line drawings.However,most existing methods for artifact drawing rely on the principles of orthographic projection that always cannot avoid angle occlusion and data overlapping while the surface of cultural relics is complex.Therefore,conformal mapping was introduced as a dimensionality reduction way to compensate for the limitation of orthographic projection.Based on the given criteria for assessing surface complexity,this paper proposed a three-dimensional feature guideline extraction method for complex cultural relic surfaces.A 2D and 3D combined factor that measured the importance of points on describing surface features,vertex weight,was designed.Then the selection threshold for feature guideline extraction was determined based on the differences between vertex weight and shape index distributions.The feasibility and stability were verified through experiments conducted on real cultural relic surface data.Results demonstrated the ability of the method to address the challenges associated with the automatic generation of line drawings for complex surfaces.The extraction method and the obtained results will be useful for line graphic drawing,displaying and propaganda of cultural relics. 展开更多
关键词 point cloud conformal parameterization vertex weight surface mesh cultural relics feature extraction
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Preferentially selective extraction of lithium from spent LiCoO_(2)cathodes by medium-temperature carbon reduction roasting 被引量:1
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作者 Daixiang Wei Wei Wang +6 位作者 Longjin Jiang Zhidong Chang Hualei Zhou Bin Dong Dekun Gao Minghui Zhang Chaofan Wu 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2024年第2期315-322,共8页
Lithium recovery from spent lithium-ion batteries(LIBs)have attracted extensive attention due to the skyrocketing price of lithium.The medium-temperature carbon reduction roasting was proposed to preferential selectiv... Lithium recovery from spent lithium-ion batteries(LIBs)have attracted extensive attention due to the skyrocketing price of lithium.The medium-temperature carbon reduction roasting was proposed to preferential selective extraction of lithium from spent Li-CoO_(2)(LCO)cathodes to overcome the incomplete recovery and loss of lithium during the recycling process.The LCO layered structure was destroyed and lithium was completely converted into water-soluble Li2CO_(3)under a suitable temperature to control the reduced state of the cobalt oxide.The Co metal agglomerates generated during medium-temperature carbon reduction roasting were broken by wet grinding and ultrasonic crushing to release the entrained lithium.The results showed that 99.10%of the whole lithium could be recovered as Li2CO_(3)with a purity of 99.55%.This work provided a new perspective on the preferentially selective extraction of lithium from spent lithium batteries. 展开更多
关键词 spent LiCoO_(2)cathodes medium-temperature carbon reduction lithium extraction priority crystal transformation macro-scopic transport resistance
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Ultrasound-assisted Extraction of Kamebakaurin from Rabdosia excisa by Response Surface Methodology
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作者 TANG Jian MA Rui-li +4 位作者 LI Qian-qian JIANG Chun-bao CHEN Rui OUYANG Zhen CHEN Hai-sheng 《Chemical Research in Chinese Universities》 SCIE CAS CSCD 2013年第6期1072-1077,共6页
For the efficient extraction of kamebakaurin(KA), the ultrasound-assisted extraction(UAE) of KA from Rabdosia excisa(R, excisa) via response surface methodology(RSM) was investigated with high-performance liqu... For the efficient extraction of kamebakaurin(KA), the ultrasound-assisted extraction(UAE) of KA from Rabdosia excisa(R, excisa) via response surface methodology(RSM) was investigated with high-performance liquid chromatography(HPLC). Effects of the experimental parameters such as extraction solvent, ratio of liquid to plant material, extraction time and extraction temperature on the extracting efficiency of KA from R. excisa were evaluated, and the purity of KA in residual was calculated. The optimized conditions were 65.5%(volume fraction) acetone, 35 ℃, time of 24.6 min with ultrasound of 80 W/L, 40 kHz, ratio of liquid to plant material at 30:1(mL/g). The maximum yield of KA is 0.708 mg/kg, with mean purity of 6.09%, indicating that ultrasound-assisted extraction is a feasible and useful method for extracting KA from R. excisa. 展开更多
关键词 ultrasound-assisted extraction Kamebakaurin Rabdosia excisa Response surface methodology
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Effects of conductive agent type on lithium extraction from salt lake brine with LiFePO_(4) electrodes
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作者 Zhen Zhang Pan Luo +7 位作者 Yan Zhang Yuhan Wang Li Liao Bo Yu Mingshan Wang Junchen Chen Bingshu Guo Xing Li 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2024年第4期678-687,共10页
Electrochemical lithium extraction from salt lakes is an effective strategy for obtaining lithium at a low cost.Nevertheless,the elevated Mg:Li ratio and the presence of numerous coexisting ions in salt lake brines gi... Electrochemical lithium extraction from salt lakes is an effective strategy for obtaining lithium at a low cost.Nevertheless,the elevated Mg:Li ratio and the presence of numerous coexisting ions in salt lake brines give rise to challenges,such as prolonged lithium extraction periods,diminished lithium extraction efficiency,and considerable environmental pollution.In this work,Li FePO4(LFP)served as the electrode material for electrochemical lithium extraction.The conductive network in the LFP electrode was optimized by adjusting the type of conductive agent.This approach resulted in high lithium extraction efficiency and extended cycle life.When the single conductive agent of acetylene black(AB)or multiwalled carbon nanotubes(MWCNTs)was replaced with the mixed conductive agent of AB/MWCNTs,the average diffusion coefficient of Li+in the electrode increased from 2.35×10^(-9)or 1.77×10^(-9)to 4.21×10^(-9)cm^(2)·s^(-1).At the current density of 20 mA·g^(-1),the average lithium extraction capacity per gram of LFP electrode increased from 30.36 mg with the single conductive agent(AB)to 35.62 mg with the mixed conductive agent(AB/MWCNTs).When the mixed conductive agent was used,the capacity retention of the electrode after 30 cycles reached 82.9%,which was considerably higher than the capacity retention of 65.8%obtained when the single AB was utilized.Meanwhile,the electrode with mixed conductive agent of AB/MWCNTs provided good cycling performance.When the conductive agent content decreased or the loading capacity increased,the electrode containing the mixed conductive agent continued to show excellent electrochemical performance.Furthermore,a self-designed,highly efficient,continuous lithium extraction device was constructed.The electrode utilizing the AB/MWCNT mixed conductive agent maintained excellent adsorption capacity and cycling performance in this device.This work provides a new perspective for the electrochemical extraction of lithium using LFP electrodes. 展开更多
关键词 salt lake brine lithium extraction electrochemical lithium extraction conductive agent extraction efficiency adsorption capacity
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Influence of the Extraction Process on the Characteristics of Romanian Mountain Walnut Oil
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作者 Anne-Gaëlle Gambert Sabina Niţu +6 位作者 Andra Tămaș Maria Laura Fanani Justine Dupré Clara Delepine Ludovic Chaveriat Patrick Martin Lucian Rusnac 《American Journal of Plant Sciences》 CAS 2024年第10期940-967,共28页
The objective of this work is to extract walnut oil using various processes in order to compare the influence on the nature of the components extracted, and thus identify the areas of potential use. We carried out the... The objective of this work is to extract walnut oil using various processes in order to compare the influence on the nature of the components extracted, and thus identify the areas of potential use. We carried out the extractions by mechanical process, thanks to a press in reduced model provided with a worm. We obtained cold extracted oil whose characteristics slightly diverge from extra virgin oil found in shops in Romania, but its composition is similar. We were also able to extract by chemical process using two methods, Folch and Soxhlet. Commercially available table walnut oils are only cold extracted to avoid the presence of solvents. Those are difficult to remove and strongly oxidize the oil. Currently, consumers appreciate walnut oil for its taste and nutritional qualities. In nutrition, this oil is put forward for its composition rich in polyunsaturated fatty acids, which are needed for human body. Food supplements made from walnut oil are available today. For the moment, this is the only use of walnut oil. Indeed, there are some studies on other fields of application, but they remain in the field of research and nothing has yet been commercialized. In this present study, we compared the chemical and physical properties of cold-extracted oil with the solvent extraction of walnut kernel originating from the mountain region of Rumania. The cold extracted oil has a high content of polyunsaturated fatty acids (63%) and monounsaturated fatty acids (30%), a very low level of saturated fatty acid (7%) and no content of linolenic acid. The Soxhlet and Folch methods produced slightly different oils with increased amounts of minor components, which changes their characteristic. Even when solvent-extracted oils do not meet the standard criteria imposed by the Codex Alimentarius, they offer a possible use in the fields of food, cosmetics industries and biomedicine. 展开更多
关键词 Walnut Oil extraction COMPOSITION Romanian Mountain
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Development of a Simple Extraction Method for Tetracycline Analogues from Bovine Milk
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作者 Oscar Cordova Thien Le +4 位作者 Christopher Lambert Devin Brodie Stephany Ramirez Francis Sandoval Karno Ng 《Advances in Biological Chemistry》 CAS 2024年第4期111-120,共10页
Tetracycline and analogues are among the most used antibiotics in the dairy industry. Besides the therapeutic uses, tetracyclines are often incorporated into livestock feed as growth promoters. A considerable amount o... Tetracycline and analogues are among the most used antibiotics in the dairy industry. Besides the therapeutic uses, tetracyclines are often incorporated into livestock feed as growth promoters. A considerable amount of antibiotics is released unaltered through milk from dairy animals. The presence of antibiotic residues in milk and their subsequent consumption can lead to potential health impacts, including cancer, hypersensitivity reactions, and the development of antibiotic resistance. Thus, it is important to monitor residual levels of tetracyclines in milk. The purpose of this study is to develop a quick and simple method for simultaneously extracting five tetracycline analogues from bovine milk. Specifically, five tetracycline analogues: Chlortetracycline (CTC), demeclocycline (DEM), doxycycline (DC), minocycline (MC), and tetracycline (TC) were simultaneously extracted from milk using trifluoroacetic acid. Subsequently, the extracted analogues were separated by reverse-phase high-performance liquid chromatography (RP-HPLC) and detected at 355 nm using UV/Vis. Calibration curves for all five tetracycline analogues show excellent linearity (r2 value > 0.99). Percent recovery for MC, TC, DEM, CTC, and DC were: 31.88%, 96.91%, 151.29, 99.20%, and 85.58% respectively. The developed extraction method has good precision (RSD < 9.9% for 4 of the 5 analogues). The developed method with minimal sample preparation and pretreatment has the potential to serve as an initial screening test. 展开更多
关键词 ANTIBIOTICS TETRACYCLINES extraction MILK HPLC
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A comprehensive review of existing corpora and methods for creating annotated corpora for event extraction tasks
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作者 Mohd Hafizul Afifi Abdullah Norshakirah Aziz +3 位作者 Said Jadid Abdulkadir Kashif Hussain Hitham Alhussian Noureen Talpur 《Journal of Data and Information Science》 CSCD 2024年第4期196-238,共43页
Purpose:The purpose of this study is to serve as a comprehensive review of the existing annotated corpora.This review study aims to provide information on the existing annotated corpora for event extraction,which are ... Purpose:The purpose of this study is to serve as a comprehensive review of the existing annotated corpora.This review study aims to provide information on the existing annotated corpora for event extraction,which are limited but essential for training and improving the existing event extraction algorithms.In addition to the primary goal of this study,it provides guidelines for preparing an annotated corpus and suggests suitable tools for the annotation task.Design/methodology/approach:This study employs an analytical approach to examine available corpus that is suitable for event extraction tasks.It offers an in-depth analysis of existing event extraction corpora and provides systematic guidelines for researchers to develop accurate,high-quality corpora.This ensures the reliability of the created corpus and its suitability for training machine learning algorithms.Findings:Our exploration reveals a scarcity of annotated corpora for event extraction tasks.In particular,the English corpora are mainly focused on the biomedical and general domains.Despite the issue of annotated corpora scarcity,there are several high-quality corpora available and widely used as benchmark datasets.However,access to some of these corpora might be limited owing to closed-access policies or discontinued maintenance after being initially released,rendering them inaccessible owing to broken links.Therefore,this study documents the available corpora for event extraction tasks.Research limitations:Our study focuses only on well-known corpora available in English and Chinese.Nevertheless,this study places a strong emphasis on the English corpora due to its status as a global lingua franca,making it widely understood compared to other languages.Practical implications:We genuinely believe that this study provides valuable knowledge that can serve as a guiding framework for preparing and accurately annotating events from text corpora.It provides comprehensive guidelines for researchers to improve the quality of corpus annotations,especially for event extraction tasks across various domains.Originality/value:This study comprehensively compiled information on the existing annotated corpora for event extraction tasks and provided preparation guidelines. 展开更多
关键词 Information extraction Event extraction Text mining Large language model Natural language processing
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A Joint Entity Relation Extraction Model Based on Relation Semantic Template Automatically Constructed
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作者 Wei Liu Meijuan Yin +1 位作者 Jialong Zhang Lunchong Cui 《Computers, Materials & Continua》 SCIE EI 2024年第1期975-997,共23页
The joint entity relation extraction model which integrates the semantic information of relation is favored by relevant researchers because of its effectiveness in solving the overlapping of entities,and the method of... The joint entity relation extraction model which integrates the semantic information of relation is favored by relevant researchers because of its effectiveness in solving the overlapping of entities,and the method of defining the semantic template of relation manually is particularly prominent in the extraction effect because it can obtain the deep semantic information of relation.However,this method has some problems,such as relying on expert experience and poor portability.Inspired by the rule-based entity relation extraction method,this paper proposes a joint entity relation extraction model based on a relation semantic template automatically constructed,which is abbreviated as RSTAC.This model refines the extraction rules of relation semantic templates from relation corpus through dependency parsing and realizes the automatic construction of relation semantic templates.Based on the relation semantic template,the process of relation classification and triplet extraction is constrained,and finally,the entity relation triplet is obtained.The experimental results on the three major Chinese datasets of DuIE,SanWen,and FinRE showthat the RSTAC model successfully obtains rich deep semantics of relation,improves the extraction effect of entity relation triples,and the F1 scores are increased by an average of 0.96% compared with classical joint extraction models such as CasRel,TPLinker,and RFBFN. 展开更多
关键词 Natural language processing deep learning information extraction relation extraction relation semantic template
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