An NO2 photoacoustic sensor system with a high reflective mirror based on a low power blue diode laser is developed in this work. The excitation power is enhanced by increasing the number of reflections. Comparing wit...An NO2 photoacoustic sensor system with a high reflective mirror based on a low power blue diode laser is developed in this work. The excitation power is enhanced by increasing the number of reflections. Comparing with a traditional photoacoustic system, the pool constant is improved from 300.24(Pa·cm)/W to 1450.64(Pa·cm)/W, and the signal sensitivity of the photoacoustic sensor is increased from 0.016 μV/ppb to 0.2562 μV/ppb. The characteristics of temperature and humidity of the new photoacoustic sensor are also obtained, and the algorithm is adjusted to provide a quantitative response and drift of the resonance frequency. The results of this research provide a new method and concept for further developing the NO2 photoacoustic sensors.展开更多
Total reflection x-ray fluorescence analysis is applied to trace element detection in liquid for effective environmental monitoring.This analytical approach requires x-ray total reflection mirrors.In order to achieve ...Total reflection x-ray fluorescence analysis is applied to trace element detection in liquid for effective environmental monitoring.This analytical approach requires x-ray total reflection mirrors.In order to achieve high sensitivity element detection,the mirrors require high surface quality for high x-ray reflectivity.Surface finishing for x-ray mirrors is typically conducted through a series of abrasive processes,such as grinding and polishing,and is thus time consuming.The purpose of this study is to streamline and enhance the surface finishing process based on unique high quality grinding techniques for the production of x-ray total reflection mirrors.展开更多
First mirror(FM)cleaning,using radio frequency(RF)plasma,has been proposed to recover FM reflectivity in nuclear fusion reactors such as the International Thermonuclear Experimental Reactor(ITER).To investigate the in...First mirror(FM)cleaning,using radio frequency(RF)plasma,has been proposed to recover FM reflectivity in nuclear fusion reactors such as the International Thermonuclear Experimental Reactor(ITER).To investigate the influence of simultaneous cleaning of two mirrors on mirror cleaning efficiency and uniformity,experiments involving single-mirror cleaning and dual-mirror cleaning were conducted using RF capacitively coupled plasma in the laboratory.For the test and simultaneous cleaning of two mirrors,the FM and second mirror(SM),both measuring 110 mm×80 mm,were placed inside the first mirror unit(FMU).They were composed of 16 mirror samples,each with a dimension of 27.5 mm×20 mm.These mirror samples consist of a titanium-zirconium-molybdenum alloy substrate,a 500 nm Mo intermediate layer and a 30 nm Al_(2)O_(3) surface coating as a proxy for Be impurities.The cleaning of a single first mirror(SFM)and the simultaneous cleaning of the FM and SM(DFM and DSM)lasted for 9 h using Ar plasma at a pressure of 1 Pa.The total reflectivity of mirror samples on the DSM did not fully recover and varied with location,with a self-bias of−140 V.With a self-bias of−300 V,the total reflectivity of mirror samples on the SFM and DFM was fully recovered.The energy dispersive spectrometer results demonstrated that the Al_(2)O_(3) coating had been completely removed from these mirror samples.However,the mass loss of each mirror sample on the SFM and DFM before and after cleaning varied depending on its location,with higher mass loss observed for mirror samples located in the corners and lower loss for those in the center.Compared with SM cleaning,the simultaneous cleaning of two mirrors reduced the difference between the highest and lowest mass loss.Furthermore,this mass loss for the mirror samples of the DFM facing the DSM was increased.This indicated that mirror samples cleaned face to face in the FMU simultaneously could influence each other,highlighting the need for special attention in future studies.展开更多
We reported previously the idea to improve reflection-ability of a magnetic mirror by installing a cyclotron resonance space in the front part of the mirror. However, since the previous analysis was insufficient from ...We reported previously the idea to improve reflection-ability of a magnetic mirror by installing a cyclotron resonance space in the front part of the mirror. However, since the previous analysis was insufficient from the examination after that, we complement the following two things in this work: 1) A simpler procedure of design to make a supplemental magnetic mirror with the simplest magnetic configuration, compared with the procedure reported previously. 2) A peculiar characteristic arising only in reflection of a nonrelativistic charged particle (a deuteron ion).展开更多
Simulation approach includes such processes as photon emissions from X-ray tube with a spectral distribution, total reflection on the sample support, photoelectric effect in thin layer sample, as well as characteristi...Simulation approach includes such processes as photon emissions from X-ray tube with a spectral distribution, total reflection on the sample support, photoelectric effect in thin layer sample, as well as characteristic line absorption and detection. The calculation results are in agreement with experimental ones.展开更多
Multilayer interference mirrors play a pivotal role in spectroscopic diagnostic systems,which probe electron temperature and density during inertial confinement fusion processes.In this study,aperiodic Mo/B_(4)C multi...Multilayer interference mirrors play a pivotal role in spectroscopic diagnostic systems,which probe electron temperature and density during inertial confinement fusion processes.In this study,aperiodic Mo/B_(4)C multilayer mirrors of varied thick-nesses were investigated for X-ray plasma diagnostics at the 9.67-keV W-Lβline.The thickness distribution of the aperiodic multilayers was designed using the first Bragg diffraction condition and then optimized through a simplex algorithm to realize a narrow bandwidth and consistent spectral response.To enhance spectral accuracy,further refinements were undertaken by matching the grazing incidence X-ray reflectivity data with actual structural parameters.X-ray reflectivity measurements from the SSRF synchrotron radiation facility on the optimized sample showed a reflectivity of 29.7±2.6%,flat-band range of 1.3 keV,and bandwidth of 1.7 keV,making it suitable for high-temperature plasma diagnostics.The study explored the potential of predicting the 9.67 keV reflectivity spectrum using the fitting data from the grazing incidence X-ray reflectivity curves at 8.05 keV.Additionally,the short-term thermal stability of an aperiodic multilayer was assessed using temperature-dependent in situ X-ray measurements.Shifts in the reflectivity spectrum during annealing were attributed to interdiffusion and interfacial relaxation.The research team recommends the aperiodic Mo/B_(4)C multilayer mirror for operations below 300℃.展开更多
为了压缩总长度,红外热像仪普遍采用双反射镜折布局(U型)及箱式壳体,而现有传函仪仅能测量非折转布局(一字型)的光学系统的调制传递函数(Modulation Transfer Function,MTF),导致传函仪无法接到U型光学系统的像面,因此无法测量其MTF。...为了压缩总长度,红外热像仪普遍采用双反射镜折布局(U型)及箱式壳体,而现有传函仪仅能测量非折转布局(一字型)的光学系统的调制传递函数(Modulation Transfer Function,MTF),导致传函仪无法接到U型光学系统的像面,因此无法测量其MTF。为了解决该难题,本文采用光瞳衔接的方式,设计和加工一个中继镜组把U型光学系统的像面引出,通过测量组合系统的MTF,再计算出U型光学系统的MTF,从而解决其MTF测量的难题。然后使用6个同一个型号的红外热像仪对测量方法进行验证,在排除影响测量的干扰因素以后,通过测量组合系统MTF,再计算出U型光学系统的MTF。同时,在测量过程中发现5#、6#红外热像仪的U型光学系统的MTF下降较多,通过红外中心偏差测量仪的测量,发现第三、四镜片的中心偏差较大,故重新装调和控制,从而使U型光学系统的MTF有大幅提升。该方法为U型光学系统的MTF测量和性能提升提供了新的思路。展开更多
In order to meet the reflectivity measurement requirements of any incident angle at different points of the large size special high mirror,a rotating cavity ring-down spectroscopy high reflectivity measurement system ...In order to meet the reflectivity measurement requirements of any incident angle at different points of the large size special high mirror,a rotating cavity ring-down spectroscopy high reflectivity measurement system was built,in which the rotation function of the resonant cavity was set,and the lifting and parallel travelling mechanism of the measured mirror was added.Furthermore,the uncertainty of the measurement results was analyzed and calculated.The results showed that the reflectivity of a high reflective mirror measured by the system was 99.9795%,the measurement accuracy reached the order of 10-6,and the combined standard uncertainty of reflectivity measurement was 0.0028%.Collectively,these results provide a detection guarantee for the maintenance of the large size special high mirror,and provide ideas and methods for the uncertainty analysis of measurement results of similar equipment parameters.展开更多
Both long-term environmental durability and high reflectance of protected-Al mirrors are of great importance for developing the optical instruments in the vacuum ultraviolet(VUV) applications. In this paper, the depen...Both long-term environmental durability and high reflectance of protected-Al mirrors are of great importance for developing the optical instruments in the vacuum ultraviolet(VUV) applications. In this paper, the dependence of spectral property and environmental durability of MgF2 over-coated Al mirrors using a 3-step method on deposition temperature of the outermost MgF2 layer are investigated in detail. Optics(reflectance), structure(surface morphology and crystalline), and environmental durability(humidity test) are characterized and discussed. The results show that both optical and moistureresistant properties of MgF2 over-coated Al mirrors are dependent on MgF2 deposition temperature, and the optimal deposition temperature for the outermost MgF2 layer should be between 250℃ and 300℃ for MgF2 over-coated Al mirrors to have both reasonably high reflectance in the VUV spectral range and high moisture resistance for long lifetime applications.展开更多
The first mirror (FM) samples made of polycrystal (PC) stainless steel (SS), molybdenum (Mo) and tungsten (W) were mounted at different locations in HT-7 tokamak to investigate the surface modifications caus...The first mirror (FM) samples made of polycrystal (PC) stainless steel (SS), molybdenum (Mo) and tungsten (W) were mounted at different locations in HT-7 tokamak to investigate the surface modifications caused by erosion and deposition. The optical transmission characteristics of first mirror samples were measured by a spectrophotometer. It was found that different irradiation environment had different influences on the first mirror surfaces, especially with wave antenna nearby. In addition, the erosion made the reflectivity of FM degrade to some extents as a whole. But the deposition on the mirror influences more than erosion does. Comparing the mirrors of SS, W and Mo, irradiated in the same environment, the W-mirror had the least changes in reflectivity with regularity, while the SS-mirror had most serious changes.展开更多
We investigate the diffraction characteristics of an incident Gaussian beam cut by a straight edge bounding a semi-infinite opaque plane using Kirchhoff scalar wave theory in the Fresnel limit, and propose a new and s...We investigate the diffraction characteristics of an incident Gaussian beam cut by a straight edge bounding a semi-infinite opaque plane using Kirchhoff scalar wave theory in the Fresnel limit, and propose a new and simple mirror scheme to reflect atoms by using the intensity gradient induced by a blue-detuned semi-Gaussian laser beam. The optical potential of the diffracted light of the knife-cut semi-Gaussian beam for 85 Rb atom and its spontaneous emission probability are calculated and compared with the performance of the evanescent-wave mirror. Our study shows that the optical potential of the diffracted light of the semi-Gaussian beam is far higher than that of the evanescent light wave, and the maximum normal velocity of the incident atoms can be far greater than that of the evanescent light wave under the same parameters, so the blue-detuned semioGaussian beam, as a novel atomic mirror, can be used to efficiently reflect cold atoms with a normal velocity of greater than 1 m/s. However, the intensity gradient (force) of the diffracted light of the semi-Gaussian-beam is much smaller than that of the evanescent light wave, so its spontaneous emission probability is greater than that from the evanescent-wave when the normal velocity of incident atoms is greater.展开更多
Based on a femtosecond laser plasma-induced hard x-ray source with a high laser pulse energy(>100 mJ)at 10 Hz repetition rate,we present a time-resolved x-ray diffraction system on an ultrafast time scale.The laser...Based on a femtosecond laser plasma-induced hard x-ray source with a high laser pulse energy(>100 mJ)at 10 Hz repetition rate,we present a time-resolved x-ray diffraction system on an ultrafast time scale.The laser intensity is at relativistic regime(2×10^(19)W/cm^(2)),which is essential for effectively generating K_(α)source in high-Z metal material.The produced copper K_(α)radiation yield reaches to 2.5×10^(8)photons/sr/shot.The multilayer mirrors are optimized for monochromatizating and two-dimensional beam shaping of Kαemission.Our experiment exhibits its ability of monitoring the transient structural changes in a thin film SrCoO_(2.5)crystal.It is demonstrated that this facility is a powerful tool to perform dynamic studies on samples and adaptable to the specific needs for different particular applications with high flexibility.展开更多
The multilayer Laue lens(MLL) is a diffractive focusing optical element which can focus hard X-rays down to the nanometer scale. In this study, a WSi_(2)/Si multilayer structure consisting of 1736 layers, with a 7.2-n...The multilayer Laue lens(MLL) is a diffractive focusing optical element which can focus hard X-rays down to the nanometer scale. In this study, a WSi_(2)/Si multilayer structure consisting of 1736 layers, with a 7.2-nm-thick outermost layer and a total thickness of 17 μm, is prepared by DC magnetron sputtering. Regarding the thin film growth rate calibration, we correct the long-term growth rate drift from 2 to 0.6%, as measured by the grazing incidence X-ray reflectivity(GIXRR). A one-dimensional line focusing resolution of 64 nm was achieved,while the diffraction efficiency was 38% of the-1 order of the MLL Shanghai Synchrotron Radiation Facility(SSRF) with the BL15U beamline.展开更多
基金National Natural Science Foundation of China(Grant Nos.91644107,61575206,51904009,and 41905130)National Key Research and Development Program of China(Grant Nos.2017YFC0209401,2017YFC0209403,and 2017YFC0209902)the Outstanding Young Talents Program of Anhui University,China(Grant No.gxyq2019022).
文摘An NO2 photoacoustic sensor system with a high reflective mirror based on a low power blue diode laser is developed in this work. The excitation power is enhanced by increasing the number of reflections. Comparing with a traditional photoacoustic system, the pool constant is improved from 300.24(Pa·cm)/W to 1450.64(Pa·cm)/W, and the signal sensitivity of the photoacoustic sensor is increased from 0.016 μV/ppb to 0.2562 μV/ppb. The characteristics of temperature and humidity of the new photoacoustic sensor are also obtained, and the algorithm is adjusted to provide a quantitative response and drift of the resonance frequency. The results of this research provide a new method and concept for further developing the NO2 photoacoustic sensors.
文摘Total reflection x-ray fluorescence analysis is applied to trace element detection in liquid for effective environmental monitoring.This analytical approach requires x-ray total reflection mirrors.In order to achieve high sensitivity element detection,the mirrors require high surface quality for high x-ray reflectivity.Surface finishing for x-ray mirrors is typically conducted through a series of abrasive processes,such as grinding and polishing,and is thus time consuming.The purpose of this study is to streamline and enhance the surface finishing process based on unique high quality grinding techniques for the production of x-ray total reflection mirrors.
基金supported by the National Key R&D Project of China(No.2022YFE03030000)National Natural Science Foundation of China(Nos.11975269,12275306 and 12075279)+3 种基金the Youth Innovation Promotion Association of the Chinese Academy of Sciences(No.2022452)the Anhui Provincial Natural Science Foundation(No.2208085J40)the CASHIPS Director’s Fund(Nos.YZJJQY202302 and BJPY2023B03)the Comprehensive Research Facility for Fusion Technology Program of China(No.2018-000052-73-01-001228).
文摘First mirror(FM)cleaning,using radio frequency(RF)plasma,has been proposed to recover FM reflectivity in nuclear fusion reactors such as the International Thermonuclear Experimental Reactor(ITER).To investigate the influence of simultaneous cleaning of two mirrors on mirror cleaning efficiency and uniformity,experiments involving single-mirror cleaning and dual-mirror cleaning were conducted using RF capacitively coupled plasma in the laboratory.For the test and simultaneous cleaning of two mirrors,the FM and second mirror(SM),both measuring 110 mm×80 mm,were placed inside the first mirror unit(FMU).They were composed of 16 mirror samples,each with a dimension of 27.5 mm×20 mm.These mirror samples consist of a titanium-zirconium-molybdenum alloy substrate,a 500 nm Mo intermediate layer and a 30 nm Al_(2)O_(3) surface coating as a proxy for Be impurities.The cleaning of a single first mirror(SFM)and the simultaneous cleaning of the FM and SM(DFM and DSM)lasted for 9 h using Ar plasma at a pressure of 1 Pa.The total reflectivity of mirror samples on the DSM did not fully recover and varied with location,with a self-bias of−140 V.With a self-bias of−300 V,the total reflectivity of mirror samples on the SFM and DFM was fully recovered.The energy dispersive spectrometer results demonstrated that the Al_(2)O_(3) coating had been completely removed from these mirror samples.However,the mass loss of each mirror sample on the SFM and DFM before and after cleaning varied depending on its location,with higher mass loss observed for mirror samples located in the corners and lower loss for those in the center.Compared with SM cleaning,the simultaneous cleaning of two mirrors reduced the difference between the highest and lowest mass loss.Furthermore,this mass loss for the mirror samples of the DFM facing the DSM was increased.This indicated that mirror samples cleaned face to face in the FMU simultaneously could influence each other,highlighting the need for special attention in future studies.
文摘We reported previously the idea to improve reflection-ability of a magnetic mirror by installing a cyclotron resonance space in the front part of the mirror. However, since the previous analysis was insufficient from the examination after that, we complement the following two things in this work: 1) A simpler procedure of design to make a supplemental magnetic mirror with the simplest magnetic configuration, compared with the procedure reported previously. 2) A peculiar characteristic arising only in reflection of a nonrelativistic charged particle (a deuteron ion).
文摘Simulation approach includes such processes as photon emissions from X-ray tube with a spectral distribution, total reflection on the sample support, photoelectric effect in thin layer sample, as well as characteristic line absorption and detection. The calculation results are in agreement with experimental ones.
基金This work was supported by the National Natural Science Foundation of China(NSFC)(Nos.11875204 and U1932167)Fundamental Research Funds for the Central Universities(Nos.22120210446 and 22120180070)the Presidential Foundation of China Academy of Engineering Physics(No.YZJJLX2019011).
文摘Multilayer interference mirrors play a pivotal role in spectroscopic diagnostic systems,which probe electron temperature and density during inertial confinement fusion processes.In this study,aperiodic Mo/B_(4)C multilayer mirrors of varied thick-nesses were investigated for X-ray plasma diagnostics at the 9.67-keV W-Lβline.The thickness distribution of the aperiodic multilayers was designed using the first Bragg diffraction condition and then optimized through a simplex algorithm to realize a narrow bandwidth and consistent spectral response.To enhance spectral accuracy,further refinements were undertaken by matching the grazing incidence X-ray reflectivity data with actual structural parameters.X-ray reflectivity measurements from the SSRF synchrotron radiation facility on the optimized sample showed a reflectivity of 29.7±2.6%,flat-band range of 1.3 keV,and bandwidth of 1.7 keV,making it suitable for high-temperature plasma diagnostics.The study explored the potential of predicting the 9.67 keV reflectivity spectrum using the fitting data from the grazing incidence X-ray reflectivity curves at 8.05 keV.Additionally,the short-term thermal stability of an aperiodic multilayer was assessed using temperature-dependent in situ X-ray measurements.Shifts in the reflectivity spectrum during annealing were attributed to interdiffusion and interfacial relaxation.The research team recommends the aperiodic Mo/B_(4)C multilayer mirror for operations below 300℃.
文摘为了压缩总长度,红外热像仪普遍采用双反射镜折布局(U型)及箱式壳体,而现有传函仪仅能测量非折转布局(一字型)的光学系统的调制传递函数(Modulation Transfer Function,MTF),导致传函仪无法接到U型光学系统的像面,因此无法测量其MTF。为了解决该难题,本文采用光瞳衔接的方式,设计和加工一个中继镜组把U型光学系统的像面引出,通过测量组合系统的MTF,再计算出U型光学系统的MTF,从而解决其MTF测量的难题。然后使用6个同一个型号的红外热像仪对测量方法进行验证,在排除影响测量的干扰因素以后,通过测量组合系统MTF,再计算出U型光学系统的MTF。同时,在测量过程中发现5#、6#红外热像仪的U型光学系统的MTF下降较多,通过红外中心偏差测量仪的测量,发现第三、四镜片的中心偏差较大,故重新装调和控制,从而使U型光学系统的MTF有大幅提升。该方法为U型光学系统的MTF测量和性能提升提供了新的思路。
基金supported by the 2021 Annual Instructional Science and Technology Program of Yongzhou(No.2021-YZKJZD-009)the Outstanding Youth Foundation of Hunan Province(No.2020JJ2015)the Science Research Project of Hunan Institute of Science and Technology(No.21xky040).
文摘In order to meet the reflectivity measurement requirements of any incident angle at different points of the large size special high mirror,a rotating cavity ring-down spectroscopy high reflectivity measurement system was built,in which the rotation function of the resonant cavity was set,and the lifting and parallel travelling mechanism of the measured mirror was added.Furthermore,the uncertainty of the measurement results was analyzed and calculated.The results showed that the reflectivity of a high reflective mirror measured by the system was 99.9795%,the measurement accuracy reached the order of 10-6,and the combined standard uncertainty of reflectivity measurement was 0.0028%.Collectively,these results provide a detection guarantee for the maintenance of the large size special high mirror,and provide ideas and methods for the uncertainty analysis of measurement results of similar equipment parameters.
基金Project supported by the West Light Foundation of the Chinese Academy of Sciencesthe National Natural Science Foundation of China(Grant No.61805247)
文摘Both long-term environmental durability and high reflectance of protected-Al mirrors are of great importance for developing the optical instruments in the vacuum ultraviolet(VUV) applications. In this paper, the dependence of spectral property and environmental durability of MgF2 over-coated Al mirrors using a 3-step method on deposition temperature of the outermost MgF2 layer are investigated in detail. Optics(reflectance), structure(surface morphology and crystalline), and environmental durability(humidity test) are characterized and discussed. The results show that both optical and moistureresistant properties of MgF2 over-coated Al mirrors are dependent on MgF2 deposition temperature, and the optimal deposition temperature for the outermost MgF2 layer should be between 250℃ and 300℃ for MgF2 over-coated Al mirrors to have both reasonably high reflectance in the VUV spectral range and high moisture resistance for long lifetime applications.
基金National Natural Science Foundation of China(No.10775138)
文摘The first mirror (FM) samples made of polycrystal (PC) stainless steel (SS), molybdenum (Mo) and tungsten (W) were mounted at different locations in HT-7 tokamak to investigate the surface modifications caused by erosion and deposition. The optical transmission characteristics of first mirror samples were measured by a spectrophotometer. It was found that different irradiation environment had different influences on the first mirror surfaces, especially with wave antenna nearby. In addition, the erosion made the reflectivity of FM degrade to some extents as a whole. But the deposition on the mirror influences more than erosion does. Comparing the mirrors of SS, W and Mo, irradiated in the same environment, the W-mirror had the least changes in reflectivity with regularity, while the SS-mirror had most serious changes.
基金Project supported by the National Natural Science Foundation of China (Grant Nos 10174050 and 10374029), the Key Program of National Natural Science Foundation of China (Grant No 10434060), and by the Shanghai Priority Academic Discipline and the 211 Foundation of the Ministry of Education of China.
文摘We investigate the diffraction characteristics of an incident Gaussian beam cut by a straight edge bounding a semi-infinite opaque plane using Kirchhoff scalar wave theory in the Fresnel limit, and propose a new and simple mirror scheme to reflect atoms by using the intensity gradient induced by a blue-detuned semi-Gaussian laser beam. The optical potential of the diffracted light of the knife-cut semi-Gaussian beam for 85 Rb atom and its spontaneous emission probability are calculated and compared with the performance of the evanescent-wave mirror. Our study shows that the optical potential of the diffracted light of the semi-Gaussian beam is far higher than that of the evanescent light wave, and the maximum normal velocity of the incident atoms can be far greater than that of the evanescent light wave under the same parameters, so the blue-detuned semioGaussian beam, as a novel atomic mirror, can be used to efficiently reflect cold atoms with a normal velocity of greater than 1 m/s. However, the intensity gradient (force) of the diffracted light of the semi-Gaussian-beam is much smaller than that of the evanescent light wave, so its spontaneous emission probability is greater than that from the evanescent-wave when the normal velocity of incident atoms is greater.
基金Project supported by the National Key R&D Program of China(Grant No.2017YFA0403301)Science Challenge Project(Grant No.TZ2018005)+1 种基金the National Natural Science Foundation of China(Grant Nos.11991073,11721404,11805266,11905289,and 61975229)Key Program of Chinese Academy of Sciences(Grant Nos.XDA25030400 and XDB17030500).
文摘Based on a femtosecond laser plasma-induced hard x-ray source with a high laser pulse energy(>100 mJ)at 10 Hz repetition rate,we present a time-resolved x-ray diffraction system on an ultrafast time scale.The laser intensity is at relativistic regime(2×10^(19)W/cm^(2)),which is essential for effectively generating K_(α)source in high-Z metal material.The produced copper K_(α)radiation yield reaches to 2.5×10^(8)photons/sr/shot.The multilayer mirrors are optimized for monochromatizating and two-dimensional beam shaping of Kαemission.Our experiment exhibits its ability of monitoring the transient structural changes in a thin film SrCoO_(2.5)crystal.It is demonstrated that this facility is a powerful tool to perform dynamic studies on samples and adaptable to the specific needs for different particular applications with high flexibility.
基金the National Natural Science Foundation of China(Nos.12005250,U1932167,and U1432244).
文摘The multilayer Laue lens(MLL) is a diffractive focusing optical element which can focus hard X-rays down to the nanometer scale. In this study, a WSi_(2)/Si multilayer structure consisting of 1736 layers, with a 7.2-nm-thick outermost layer and a total thickness of 17 μm, is prepared by DC magnetron sputtering. Regarding the thin film growth rate calibration, we correct the long-term growth rate drift from 2 to 0.6%, as measured by the grazing incidence X-ray reflectivity(GIXRR). A one-dimensional line focusing resolution of 64 nm was achieved,while the diffraction efficiency was 38% of the-1 order of the MLL Shanghai Synchrotron Radiation Facility(SSRF) with the BL15U beamline.