A 980-nm semiconductor saturable absorber mirror(SESAM) mode-locked Yb-doped phosphate fiber laser is demonstrated by using an all-fiber linear cavity configuration. Two different kinds of cavity lengths are introdu...A 980-nm semiconductor saturable absorber mirror(SESAM) mode-locked Yb-doped phosphate fiber laser is demonstrated by using an all-fiber linear cavity configuration. Two different kinds of cavity lengths are introduced into the oscillator to obtain a robust and stable mode-locked seed source. When the cavity length is chosen to be 6 m, the oscillator generates an average output power of 3.5 m W and a pulse width of 76.27 ps with a repetition rate of 17.08 MHz. As the cavity length is optimized to short, 4.4-m W maximum output power and 61.15-ps pulse width are produced at a repetition rate of 20.96 MHz. The output spectrum is centered at 980 nm with a narrow spectral bandwidth of 0.13 nm. In the experiment, no undesired amplified spontaneous emission(ASE) nor harmful oscillation around 1030 nm is observed. Moreover,through a two-stage all-fiber-integrated amplifier, an output power of 740 m W is generated with a pulse width of 200 ps.展开更多
We report on a theoretical and experimental study of an all-normal-dispersion (ANDi) Yb-doped mode-locked fiber laser, in which nonlinear polarization rotation (NPR) is used to realize mode-locking without any dis...We report on a theoretical and experimental study of an all-normal-dispersion (ANDi) Yb-doped mode-locked fiber laser, in which nonlinear polarization rotation (NPR) is used to realize mode-locking without any dispersion compensation. Based on the coupled nonlinear Schr6dinger (CNLS) equation, a model simulating the mode-locked process of an all-normal-dispersion ring fiber laser is developed, which shows that the achievement of stable mode-locking depends on the alignment of the polarization controller (PC) along the fast-polarization axis of the fiber, the birefringence intensity, and the net cavity dispersion. According to the theoretical analysis, stable mode-locked pulses with pulse duration 300 ps and average output power 33.9 mW at repetition rate 36 MHz are obtained.展开更多
The stimulated Brillouin scattering (SBS) threshold enhancement factor in a pure white noise linewidth broad- ening Yb-doped fiber amplifier (YDFA) with a short large mode area fiber is theoretically and experimen...The stimulated Brillouin scattering (SBS) threshold enhancement factor in a pure white noise linewidth broad- ening Yb-doped fiber amplifier (YDFA) with a short large mode area fiber is theoretically and experimentally studied. We demonstrate a 1064.08nm, 11.6 GHz finewidth, 1.5 k W output power YDFA with an SBS threshold enhancement of -57 (26 W SBS threshold with single frequency seed). The output beam is near-diffraction lim- ited with a beam quality factor elM2 = 1.15 and a slope efficiency of up to 87%. No SBS or stimulated Raman scattering effects are observed in the whole power range. Further power sealing is limited by the available pump power in our system.展开更多
The wavelength-tunable and switchable narrow bandwidth mode-locking operation is demonstrated in an all fiber laser based on semiconductor-saturable absorber mirror (SESAM). Two narrow-band fiber Bragg gratings cent...The wavelength-tunable and switchable narrow bandwidth mode-locking operation is demonstrated in an all fiber laser based on semiconductor-saturable absorber mirror (SESAM). Two narrow-band fiber Bragg gratings centered at 1029.9nm and 1032nm respectively with a polarization controller inserted between them are used to realize the wavelength switchable between 1029.9nm and 1032nm. The laser delivers different pulse widths of 7.5ps for 1030nm and 20ps for 1032nm. The maximum output power for both could reach -6.5mW at single pulse operation. The output wavelength couM be tuned to about 0.gnm intervals ranging from 1030.2nm to 1031.1 nm and from 1032.15nm to 1033.7nm with the temperature change of the fiber Bragg grating, respectively.展开更多
We demonstrate a nonlinear polarization evolution mode-locked Yb-doped fiber oscillator with the broadband spectrum output operating in a dispersion-managed regime. Pumped by a 976 nm single-mode laser diode, stable m...We demonstrate a nonlinear polarization evolution mode-locked Yb-doped fiber oscillator with the broadband spectrum output operating in a dispersion-managed regime. Pumped by a 976 nm single-mode laser diode, stable mode-locked ultrashort pulses are emitted with an average power of 198mW at a repetition rate of 124MHz, corresponding to a pulse energy of 1.6nJ. The output spectrum spans from 950nm to ll50nm so that the transform-limited pulse duration is as short as 23 fs. Due to the imperfect dispersion compensation, we compress the pulses to 32 fs in this experiment.展开更多
We report on a wide-band and stable mode-locked all-polarization-maintaining fiber laser configuration using a nonlinear optical loop mirror. The central wavelength of the laser is 1080.14nm and the 3dB bandwidth is 2...We report on a wide-band and stable mode-locked all-polarization-maintaining fiber laser configuration using a nonlinear optical loop mirror. The central wavelength of the laser is 1080.14nm and the 3dB bandwidth is 20.29nm. The repetition rate of the pulse is 3.28 MHz and the pulse width is 848ps. By tuning the pump power, which is centered at 980nrn, from 300mW to 380mW, we obtain a linearly changed output power from 6row to 7.12roW. The all-polarization-mMntaining fiber configuration is fundamental to the stability of the output power.展开更多
Wavelength-tunable ultrashort pulse source with high energy is highly desired for a lot of applications. The wavelength-tunable all-normal-dispersion (ANDi) mode-locked fiber laser, which can be compressed easily an...Wavelength-tunable ultrashort pulse source with high energy is highly desired for a lot of applications. The wavelength-tunable all-normal-dispersion (ANDi) mode-locked fiber laser, which can be compressed easily and amplified by an all-fiber structure, is a promising seed of such a source with compact structures. The pulse compression and amplification at different center wavelengths (from 1026 to 1058nm) of the tunable ANDi Yb- doped mode-locked fiber lasers that we previously proposed are experimentally investigated in this work. It is found that, for different wavelengths, the duration and chirp of the direct output pulse from the oscillator vary considerably, however, the duration of compressed pulse fluctuates less. For the amplification process, due to the unf/at gain spectrum of Yb-doped fiber, the gain at a short wavelength is larger than that at a long wavelength. Consequently, the trends of spectrum distortions induced by the amplification process are different for different wavelengths. These results and analyses will be helpful for the design of a high-energy and wavelength-tunable ultrashort pulse source based on an ANDi seed.展开更多
A two-dimensional silver nanoplate is prepared with the seed-mediated growth method and is used for achieving pulse fiber laser operation. By controlling the dimension parameters of the silver nanoplate, the surface p...A two-dimensional silver nanoplate is prepared with the seed-mediated growth method and is used for achieving pulse fiber laser operation. By controlling the dimension parameters of the silver nanoplate, the surface plasmon resonance absorption peak of the material is successfully adjusted to 1068 nm. Based on the silver nanoplate as a saturable absorber, a passively Q-switched Yb-doped fiber laser operating at 1062 nm is demonstrated. The maximum average output power of 3.49mW is obtained with a minimum pulse width of 1.84#s at a pulse repetition rate of 65.TkHz, and the corresponding pulse energy and peak power are 53.1 nJ and 28.8mW, respectively.展开更多
An asymmetric heating method for fusion splicing of 1 060-XP silica fiber (1 060F) and phosphate glass fiber (PGF) using an electric arc splicer has been proposed. Double joints with the lowest splice loss of 0.6 ...An asymmetric heating method for fusion splicing of 1 060-XP silica fiber (1 060F) and phosphate glass fiber (PGF) using an electric arc splicer has been proposed. Double joints with the lowest splice loss of 0.6 dB and good bending-resist strength between 1 060 F and PGF has been obtained. The main reasons affecting fiber splice loss and strength have been analyzed.展开更多
To improve the crack-resistance of the mould for silica sol bonded quartz based ceramic mould casting,aluminum silicate fibers with the diameter ranging from 5 μm to 25 μm and the length about 1 mm were dispersed in...To improve the crack-resistance of the mould for silica sol bonded quartz based ceramic mould casting,aluminum silicate fibers with the diameter ranging from 5 μm to 25 μm and the length about 1 mm were dispersed in the ceramic mould.The effect of the aluminum silicate fibers on the tensile strength,shrinkage rate and the cracking trend of the ceramic mould were investigated.In the ceramic slurry,quartz sand was applied as ceramic aggregate,silica sol containing 30% silicon dioxide as bonder,and the weight ratio of quartz sand to silica sol was 2.69;the dispersed fibers changed from 0 to 0.24vol.%.The mould samples were formed after the slurry was poured and gelled at room temperature,and then sintered at different temperatures ranging from 100 to 800 ℃ to measure the tensile strength and shrinkage rate.The results show that,with the aluminum silicate fiber addition increasing from 0 to 0.24vol.%,the tensile strength increases linearly from 0.175 MPa to 0.236 MPa,and the shrinkage rate decreases linearly from 1.75% to 1.68% for the ceramic mould sintered at 400 ℃,from 1.37% to 1.31% for the ceramic mould at room temperature.As the sintering temperature was raised from 100 ℃ to 800 ℃,the tensile strength increases,and the shrinkage rate decreases at all temperatures,compared with those without fiber dispersion,but their variation patterns remain the same.Furthermore,the cracking trend of the mould and its decreasing proportion were defined and analyzed quantitatively considering both effects of the fiber dispersion on the strength and shrinkage.The cracking trend appears to decrease linearly with increasing fiber content and to reach the maximum reduction of 28.8% when 0.24vol.% fiber was dispersed.Therefore,the investigation proposes a new method to improve the crack-resistance of the ceramic mould,i.e.,inorganic fiber dispersion into the ceramic mould.展开更多
Uniform crystalline TiO2 thin films were coated on silica glass fibers by liquid phase deposition from aqueous solution of ammonium hexafluorotitanate at low temperature. TiO2 thin films and nanopowders were prepared ...Uniform crystalline TiO2 thin films were coated on silica glass fibers by liquid phase deposition from aqueous solution of ammonium hexafluorotitanate at low temperature. TiO2 thin films and nanopowders were prepared by adding H3BO3 into (NH4)2TiF6 solution supersaturated with anatase nano-crystalline TiO2 at 40 ℃. The effects of the deposition conditions on the surface morphology, section morphology, thickness of the deposited TiO2 thin films were investigated. The results indicate that the growth rate and particle size of the thin films were controlled by both the deposition conditions and the amount of anatase nano-crystalline TiO2.展开更多
We propose and demonstrate a Q-switched erbium-doped fiber laser (EDFL) using an erbium-doped zirconia-alumina silica glass-based fiber (Zr-EDF) as a saturable absorber. As a 16-cm-long Zr-EDF is incorporated into...We propose and demonstrate a Q-switched erbium-doped fiber laser (EDFL) using an erbium-doped zirconia-alumina silica glass-based fiber (Zr-EDF) as a saturable absorber. As a 16-cm-long Zr-EDF is incorporated into a ring EDFL cavity, a stable Q-switching pulse train operating at 1565?nm wavelength is successfully obtained. The repetition rate is tunable from 33.97?kHz to 71.23?kHz by increasing the pump power from the threshold of 26?mW to the maximum of 74?mW. The highest pulse energy of 26.67?nJ is obtained at the maximum pump power.展开更多
Three-dimensional silica fiber reinforced silicon nitride based composites were fabricated by preceramic polymer infiltration and pyrolysis method using perhydropolysilazane as a precursor. The effects of precoating a...Three-dimensional silica fiber reinforced silicon nitride based composites were fabricated by preceramic polymer infiltration and pyrolysis method using perhydropolysilazane as a precursor. The effects of precoating and high temperature calcination on the microstructures of the composites were investigated by scanning electron microscopy. For the composite without a precoating, the fracture surface is plain, and the fiber/matrix interfaces become very unclear after calcination at 1 600 ℃ due to intense interfacial reactions. The composite with a precoating shows tough fracture surface with distinct fiber pull-outs, and the fiber/matrix interfaces are still clear after calcination at 1 600 ℃. It is the appropriate precoating process that contributes to the good interfacial microstructures for the composite.展开更多
Two-dimension (2D) fused-silica fiber reinforced porous silicon nitride matrix composites were fabricated using slurry impregnation and cyclic infiltration with colloidal silica sol. The microstructure and fracture ...Two-dimension (2D) fused-silica fiber reinforced porous silicon nitride matrix composites were fabricated using slurry impregnation and cyclic infiltration with colloidal silica sol. The microstructure and fracture surface were characterized by SEM, the mechanical behavior was investigated by three-point bending test, and the dielectric constant was also measured by impedance analysis. The microstructure showed that the fiber and the matrix had a physical bonding, forming a clearance interface. The mechanical behavior suggested that the porous matrix acted as crack deflection, and the fracture surface had a lot of fiber pull-out. However, the interlaminar shear strength was not so good. The dielectric constant of the composites at room temperature was about 2.8-3.1. The relatively low dielectric constant and non-catastrophic failure indicated the potential application in the radome materials field. 2008 University of Science and Technology Beijing. All rights reserved.展开更多
A high capacity image-transmission silica fiber was prepared in North Jiaotong Universitysuccessfully.It is a result of cooperative development with Beijing Micro-technique Institute andBeijing Fabric No.605.This fibe...A high capacity image-transmission silica fiber was prepared in North Jiaotong Universitysuccessfully.It is a result of cooperative development with Beijing Micro-technique Institute andBeijing Fabric No.605.This fiber shows high-resolution,high-transmittance and high-qualitycolour-fidelity.展开更多
We report a comparative experimental study of the attenuation spectra transformations for a series of Yb doped alumino-germano silicate fibers with different contents of Yb3+ dopants, which arise as the result of irra...We report a comparative experimental study of the attenuation spectra transformations for a series of Yb doped alumino-germano silicate fibers with different contents of Yb3+ dopants, which arise as the result of irradiation either by a beam of high-energy electrons or by resonant (into the 977-nm absorption peak of YbYb3+ ions) optical pumping. The experimental data obtained reveal that in the two circumstances, substantial and complex but different in appearance changes occur within the resonant absorption band of YbYb3+ ions and in the off-resonance background loss of the fibers. Possible mechanisms responsible for these spectral changes are discussed.展开更多
Concrete, as an essential construction material in the construction industry, is the main component of solid waste. To improve the strength and durability of concrete, some additives can be added into concrete to repl...Concrete, as an essential construction material in the construction industry, is the main component of solid waste. To improve the strength and durability of concrete, some additives can be added into concrete to replace parts of cement. Carbon fiber and silica powder are the most common additives. Under a series of experiments, the effects of temperature, carbon fiber and silica powder on the mechanical properties of concrete were studied under normal circumstances. In this paper, a conclusion on the effects was drawn up mainly through some experimental analyses, so as to discuss the effect laws and provide a reference to manufacture the concrete of high strength and properties.展开更多
This paper reports how a hairy layer of carbon nano-fibers can be prepared on the macro-porous silica foam produced by the sphere templating method. Firstly, three-dimensional close-packed crystals of polystyrene sphe...This paper reports how a hairy layer of carbon nano-fibers can be prepared on the macro-porous silica foam produced by the sphere templating method. Firstly, three-dimensional close-packed crystals of polystyrene spheres are assembled on porous disk substrate by vacuum filtration or evaporation. The polystyrene template is annealed slightly above the glass transition temperature in order to strengthen the colloidal crystal and ensure inter- connection of the spheres so as to obtain porous materials with open structure. Following the treatment of hexde- cyltrimethylammonium bromide, the polystyrene template is filled with silica colloidal solution, which solidifies in the cavities. Then the polystyrene particles are removed by calcination at 843K, leaving behind porous silica foam. Scanning electron microscopy images demonstrate that silica foam has uniform and open structured pores. Nickel particles were deposited on porous silica foam layer by the dipping method and porous carbon nano-fiber washcoat was prepared by catalytic decomposition of ethene over small nickel particles.展开更多
A repeatable and simple thermal splicing method for low loss splice between fluoride and silica fibers is presented. The minimum splicing loss of 0.58 dB is achieved experimentally with this approach, Meanwhile, the p...A repeatable and simple thermal splicing method for low loss splice between fluoride and silica fibers is presented. The minimum splicing loss of 0.58 dB is achieved experimentally with this approach, Meanwhile, the power capacity of this splicing joint is also tested with a high power fiber laser. The maximum input power is up to 15 W, only limited by the available power of the laser source. To the best of our knowledge, this is the first report on thermal splicing between fluoride and silica fibers operating in a high power regime without any complicated ion-assisted deposition process.展开更多
The characteristics of the best known defect centers E' in silica optical fiber material irradiated with ray were investigated by ESR at room temperature.A mechanism model of production of the E' center defect...The characteristics of the best known defect centers E' in silica optical fiber material irradiated with ray were investigated by ESR at room temperature.A mechanism model of production of the E' center defect was established.The production of E' center includes two processes creation and activation.The strained bonds(or oxygen replacement) in silica networks lead to the creation of new defects whose concentration increases linearly with the dose.The pre-existing defects produce the activation,which tends to saturation.According to this model,the relation of E' center concentration changing with irradiation dose was obtained theoretically.The results are in good agreement with the experimental results.展开更多
基金supported by the National Natural Science Foundation of China(Grant No.61205047)
文摘A 980-nm semiconductor saturable absorber mirror(SESAM) mode-locked Yb-doped phosphate fiber laser is demonstrated by using an all-fiber linear cavity configuration. Two different kinds of cavity lengths are introduced into the oscillator to obtain a robust and stable mode-locked seed source. When the cavity length is chosen to be 6 m, the oscillator generates an average output power of 3.5 m W and a pulse width of 76.27 ps with a repetition rate of 17.08 MHz. As the cavity length is optimized to short, 4.4-m W maximum output power and 61.15-ps pulse width are produced at a repetition rate of 20.96 MHz. The output spectrum is centered at 980 nm with a narrow spectral bandwidth of 0.13 nm. In the experiment, no undesired amplified spontaneous emission(ASE) nor harmful oscillation around 1030 nm is observed. Moreover,through a two-stage all-fiber-integrated amplifier, an output power of 740 m W is generated with a pulse width of 200 ps.
文摘We report on a theoretical and experimental study of an all-normal-dispersion (ANDi) Yb-doped mode-locked fiber laser, in which nonlinear polarization rotation (NPR) is used to realize mode-locking without any dispersion compensation. Based on the coupled nonlinear Schr6dinger (CNLS) equation, a model simulating the mode-locked process of an all-normal-dispersion ring fiber laser is developed, which shows that the achievement of stable mode-locking depends on the alignment of the polarization controller (PC) along the fast-polarization axis of the fiber, the birefringence intensity, and the net cavity dispersion. According to the theoretical analysis, stable mode-locked pulses with pulse duration 300 ps and average output power 33.9 mW at repetition rate 36 MHz are obtained.
基金Supported by the National Natural Science Foundation of China under Grant Nos U1330134,61308024 and 11174305the National High-Technology Research and Development Program of China under Grant No 2014AA041901the Shanghai Natural Science Foundation under Grant No 11ZR1441400
文摘The stimulated Brillouin scattering (SBS) threshold enhancement factor in a pure white noise linewidth broad- ening Yb-doped fiber amplifier (YDFA) with a short large mode area fiber is theoretically and experimentally studied. We demonstrate a 1064.08nm, 11.6 GHz finewidth, 1.5 k W output power YDFA with an SBS threshold enhancement of -57 (26 W SBS threshold with single frequency seed). The output beam is near-diffraction lim- ited with a beam quality factor elM2 = 1.15 and a slope efficiency of up to 87%. No SBS or stimulated Raman scattering effects are observed in the whole power range. Further power sealing is limited by the available pump power in our system.
基金Supported by the National High Technology Research and Development Program of China under Grant No 2014AA041901NSAF Foundation of the National Natural Science Foundation of China under Grant No U1330134+1 种基金the Opening Project of Shanghai Key Laboratory of All Solid-State Laser and Applied Techniques under Grant No 2012ADL02the National Natural Science Foundation of China under Grant Nos 61308024 and 11174305
文摘The wavelength-tunable and switchable narrow bandwidth mode-locking operation is demonstrated in an all fiber laser based on semiconductor-saturable absorber mirror (SESAM). Two narrow-band fiber Bragg gratings centered at 1029.9nm and 1032nm respectively with a polarization controller inserted between them are used to realize the wavelength switchable between 1029.9nm and 1032nm. The laser delivers different pulse widths of 7.5ps for 1030nm and 20ps for 1032nm. The maximum output power for both could reach -6.5mW at single pulse operation. The output wavelength couM be tuned to about 0.gnm intervals ranging from 1030.2nm to 1031.1 nm and from 1032.15nm to 1033.7nm with the temperature change of the fiber Bragg grating, respectively.
基金Supported by the National Basic Research Program of China under Grant No 2012CB821304the National Natural Science Foundation of China under Grant No 61378040
文摘We demonstrate a nonlinear polarization evolution mode-locked Yb-doped fiber oscillator with the broadband spectrum output operating in a dispersion-managed regime. Pumped by a 976 nm single-mode laser diode, stable mode-locked ultrashort pulses are emitted with an average power of 198mW at a repetition rate of 124MHz, corresponding to a pulse energy of 1.6nJ. The output spectrum spans from 950nm to ll50nm so that the transform-limited pulse duration is as short as 23 fs. Due to the imperfect dispersion compensation, we compress the pulses to 32 fs in this experiment.
文摘We report on a wide-band and stable mode-locked all-polarization-maintaining fiber laser configuration using a nonlinear optical loop mirror. The central wavelength of the laser is 1080.14nm and the 3dB bandwidth is 20.29nm. The repetition rate of the pulse is 3.28 MHz and the pulse width is 848ps. By tuning the pump power, which is centered at 980nrn, from 300mW to 380mW, we obtain a linearly changed output power from 6row to 7.12roW. The all-polarization-mMntaining fiber configuration is fundamental to the stability of the output power.
基金Supported by the Initiative Scientific Research Program of Tsinghua University
文摘Wavelength-tunable ultrashort pulse source with high energy is highly desired for a lot of applications. The wavelength-tunable all-normal-dispersion (ANDi) mode-locked fiber laser, which can be compressed easily and amplified by an all-fiber structure, is a promising seed of such a source with compact structures. The pulse compression and amplification at different center wavelengths (from 1026 to 1058nm) of the tunable ANDi Yb- doped mode-locked fiber lasers that we previously proposed are experimentally investigated in this work. It is found that, for different wavelengths, the duration and chirp of the direct output pulse from the oscillator vary considerably, however, the duration of compressed pulse fluctuates less. For the amplification process, due to the unf/at gain spectrum of Yb-doped fiber, the gain at a short wavelength is larger than that at a long wavelength. Consequently, the trends of spectrum distortions induced by the amplification process are different for different wavelengths. These results and analyses will be helpful for the design of a high-energy and wavelength-tunable ultrashort pulse source based on an ANDi seed.
基金Supported by the Foundation of Shandong Province under Grant No J13LN28the National Natural Science Foundation of China under Grant No 11304184
文摘A two-dimensional silver nanoplate is prepared with the seed-mediated growth method and is used for achieving pulse fiber laser operation. By controlling the dimension parameters of the silver nanoplate, the surface plasmon resonance absorption peak of the material is successfully adjusted to 1068 nm. Based on the silver nanoplate as a saturable absorber, a passively Q-switched Yb-doped fiber laser operating at 1062 nm is demonstrated. The maximum average output power of 3.49mW is obtained with a minimum pulse width of 1.84#s at a pulse repetition rate of 65.TkHz, and the corresponding pulse energy and peak power are 53.1 nJ and 28.8mW, respectively.
基金Funded by the Guangdong Science and Technology Program (No.2005A10602001)the Guangzhou Science and Technology Program (No.2006Z2-D0161)the Program for New Century Excellent Talents (No.NCET-04-0821)
文摘An asymmetric heating method for fusion splicing of 1 060-XP silica fiber (1 060F) and phosphate glass fiber (PGF) using an electric arc splicer has been proposed. Double joints with the lowest splice loss of 0.6 dB and good bending-resist strength between 1 060 F and PGF has been obtained. The main reasons affecting fiber splice loss and strength have been analyzed.
文摘To improve the crack-resistance of the mould for silica sol bonded quartz based ceramic mould casting,aluminum silicate fibers with the diameter ranging from 5 μm to 25 μm and the length about 1 mm were dispersed in the ceramic mould.The effect of the aluminum silicate fibers on the tensile strength,shrinkage rate and the cracking trend of the ceramic mould were investigated.In the ceramic slurry,quartz sand was applied as ceramic aggregate,silica sol containing 30% silicon dioxide as bonder,and the weight ratio of quartz sand to silica sol was 2.69;the dispersed fibers changed from 0 to 0.24vol.%.The mould samples were formed after the slurry was poured and gelled at room temperature,and then sintered at different temperatures ranging from 100 to 800 ℃ to measure the tensile strength and shrinkage rate.The results show that,with the aluminum silicate fiber addition increasing from 0 to 0.24vol.%,the tensile strength increases linearly from 0.175 MPa to 0.236 MPa,and the shrinkage rate decreases linearly from 1.75% to 1.68% for the ceramic mould sintered at 400 ℃,from 1.37% to 1.31% for the ceramic mould at room temperature.As the sintering temperature was raised from 100 ℃ to 800 ℃,the tensile strength increases,and the shrinkage rate decreases at all temperatures,compared with those without fiber dispersion,but their variation patterns remain the same.Furthermore,the cracking trend of the mould and its decreasing proportion were defined and analyzed quantitatively considering both effects of the fiber dispersion on the strength and shrinkage.The cracking trend appears to decrease linearly with increasing fiber content and to reach the maximum reduction of 28.8% when 0.24vol.% fiber was dispersed.Therefore,the investigation proposes a new method to improve the crack-resistance of the ceramic mould,i.e.,inorganic fiber dispersion into the ceramic mould.
文摘Uniform crystalline TiO2 thin films were coated on silica glass fibers by liquid phase deposition from aqueous solution of ammonium hexafluorotitanate at low temperature. TiO2 thin films and nanopowders were prepared by adding H3BO3 into (NH4)2TiF6 solution supersaturated with anatase nano-crystalline TiO2 at 40 ℃. The effects of the deposition conditions on the surface morphology, section morphology, thickness of the deposited TiO2 thin films were investigated. The results indicate that the growth rate and particle size of the thin films were controlled by both the deposition conditions and the amount of anatase nano-crystalline TiO2.
基金Supported by the Postgraduate Research of Malaysia under Grant No PG098-2014Bthe CSIR of Government of India
文摘We propose and demonstrate a Q-switched erbium-doped fiber laser (EDFL) using an erbium-doped zirconia-alumina silica glass-based fiber (Zr-EDF) as a saturable absorber. As a 16-cm-long Zr-EDF is incorporated into a ring EDFL cavity, a stable Q-switching pulse train operating at 1565?nm wavelength is successfully obtained. The repetition rate is tunable from 33.97?kHz to 71.23?kHz by increasing the pump power from the threshold of 26?mW to the maximum of 74?mW. The highest pulse energy of 26.67?nJ is obtained at the maximum pump power.
文摘Three-dimensional silica fiber reinforced silicon nitride based composites were fabricated by preceramic polymer infiltration and pyrolysis method using perhydropolysilazane as a precursor. The effects of precoating and high temperature calcination on the microstructures of the composites were investigated by scanning electron microscopy. For the composite without a precoating, the fracture surface is plain, and the fiber/matrix interfaces become very unclear after calcination at 1 600 ℃ due to intense interfacial reactions. The composite with a precoating shows tough fracture surface with distinct fiber pull-outs, and the fiber/matrix interfaces are still clear after calcination at 1 600 ℃. It is the appropriate precoating process that contributes to the good interfacial microstructures for the composite.
基金the National Natural Science Foundation of China(No.90405015)the National Young Elitist Foundation(No.50425208).
文摘Two-dimension (2D) fused-silica fiber reinforced porous silicon nitride matrix composites were fabricated using slurry impregnation and cyclic infiltration with colloidal silica sol. The microstructure and fracture surface were characterized by SEM, the mechanical behavior was investigated by three-point bending test, and the dielectric constant was also measured by impedance analysis. The microstructure showed that the fiber and the matrix had a physical bonding, forming a clearance interface. The mechanical behavior suggested that the porous matrix acted as crack deflection, and the fracture surface had a lot of fiber pull-out. However, the interlaminar shear strength was not so good. The dielectric constant of the composites at room temperature was about 2.8-3.1. The relatively low dielectric constant and non-catastrophic failure indicated the potential application in the radome materials field. 2008 University of Science and Technology Beijing. All rights reserved.
文摘A high capacity image-transmission silica fiber was prepared in North Jiaotong Universitysuccessfully.It is a result of cooperative development with Beijing Micro-technique Institute andBeijing Fabric No.605.This fiber shows high-resolution,high-transmittance and high-qualitycolour-fidelity.
文摘We report a comparative experimental study of the attenuation spectra transformations for a series of Yb doped alumino-germano silicate fibers with different contents of Yb3+ dopants, which arise as the result of irradiation either by a beam of high-energy electrons or by resonant (into the 977-nm absorption peak of YbYb3+ ions) optical pumping. The experimental data obtained reveal that in the two circumstances, substantial and complex but different in appearance changes occur within the resonant absorption band of YbYb3+ ions and in the off-resonance background loss of the fibers. Possible mechanisms responsible for these spectral changes are discussed.
文摘Concrete, as an essential construction material in the construction industry, is the main component of solid waste. To improve the strength and durability of concrete, some additives can be added into concrete to replace parts of cement. Carbon fiber and silica powder are the most common additives. Under a series of experiments, the effects of temperature, carbon fiber and silica powder on the mechanical properties of concrete were studied under normal circumstances. In this paper, a conclusion on the effects was drawn up mainly through some experimental analyses, so as to discuss the effect laws and provide a reference to manufacture the concrete of high strength and properties.
基金NUFFIC, CSC and the Scientific Research Fund of Hunan Provincial Education Department (No.04B060).
文摘This paper reports how a hairy layer of carbon nano-fibers can be prepared on the macro-porous silica foam produced by the sphere templating method. Firstly, three-dimensional close-packed crystals of polystyrene spheres are assembled on porous disk substrate by vacuum filtration or evaporation. The polystyrene template is annealed slightly above the glass transition temperature in order to strengthen the colloidal crystal and ensure inter- connection of the spheres so as to obtain porous materials with open structure. Following the treatment of hexde- cyltrimethylammonium bromide, the polystyrene template is filled with silica colloidal solution, which solidifies in the cavities. Then the polystyrene particles are removed by calcination at 843K, leaving behind porous silica foam. Scanning electron microscopy images demonstrate that silica foam has uniform and open structured pores. Nickel particles were deposited on porous silica foam layer by the dipping method and porous carbon nano-fiber washcoat was prepared by catalytic decomposition of ethene over small nickel particles.
基金Supported by the National Natural Science Foundation of China under Grant No 61275144the Innovative Research and Development Project of Nanshan District under Grant No KC2013JSCX0013A+1 种基金the Shenzhen Science and Technology Innovation Projects under Grant No JCYJ20150324140036862the Funding from Shenzhen University under Grant No 00008355
文摘A repeatable and simple thermal splicing method for low loss splice between fluoride and silica fibers is presented. The minimum splicing loss of 0.58 dB is achieved experimentally with this approach, Meanwhile, the power capacity of this splicing joint is also tested with a high power fiber laser. The maximum input power is up to 15 W, only limited by the available power of the laser source. To the best of our knowledge, this is the first report on thermal splicing between fluoride and silica fibers operating in a high power regime without any complicated ion-assisted deposition process.
基金Supported by National Program on Key Basic Research Project(973 Program,No.2012CB723405)Natural Science Foundation of China(No.60937003,61077068,61275090,61275051,and 61027015)Shanghai Natural Science Foundation(No.12ZR1411200)
文摘The characteristics of the best known defect centers E' in silica optical fiber material irradiated with ray were investigated by ESR at room temperature.A mechanism model of production of the E' center defect was established.The production of E' center includes two processes creation and activation.The strained bonds(or oxygen replacement) in silica networks lead to the creation of new defects whose concentration increases linearly with the dose.The pre-existing defects produce the activation,which tends to saturation.According to this model,the relation of E' center concentration changing with irradiation dose was obtained theoretically.The results are in good agreement with the experimental results.