Objective:To evaluate the shear bond strength(SBS) between alumina-toughened zirconia (ATZ) cores and veneering ceramics,investigate the effect of aging in artificial saliva on SBS and compare it with that of yttria-s...Objective:To evaluate the shear bond strength(SBS) between alumina-toughened zirconia (ATZ) cores and veneering ceramics,investigate the effect of aging in artificial saliva on SBS and compare it with that of yttria-stabilized tetragonal zirconia polycrystals(Y-TZP).Methods:Bars of ATZ and Y-TZP were layered with veneering ceramics in accordance to the recommendation of the manufacturer.Half of each group(n = 10) was aged at 134℃.(under 2 bar pressure) in an autoclave for 48 h.Subsequently,all specimens were subjected to shear force in a universal testing machine.The interface and fractured surface of the specimens were evaluated using scanning electron microscopy and X-ray energy dispersive spectroscopy.Results:The initial mean SBS values in MPa±SD were 28.9±8.0 for ATZ and 26.2±7.6 for Y-TZP.After aging,the mean SBS values for ATZ and Y-TZP were 22.9±4.9 MPa and 22.8±6.9 MPa,respectively.Neither the differences between the SBS values of the ATZ and Y-TZP groups nor the influence of aging on all groups were statistically significant.Conclusions:The SBS between the ATZ core and the veneering ceramics was not affected by aging.The SBS of ATZ to veneering ceramics was not significantly different compared with that of Y-TZP.展开更多
Rock anchors are a common safety measure for stabilising large-scale infrastructure,such as bridge towers,retaining walls,rock slopes and windmills.There are four principal failure modes for rock anchors:(a)tensile fa...Rock anchors are a common safety measure for stabilising large-scale infrastructure,such as bridge towers,retaining walls,rock slopes and windmills.There are four principal failure modes for rock anchors:(a)tensile failure of the steel anchor,(b)anchor-grout interface failure,(c)grout-rock interface failure,and(d)rock mass uplift.Field tests were performed in a limestone quarry.These tests were designed to test failure modes B and C through pullout.In the tests of failure mode B,the shear stress on the anchor-grout interface is the largest at the top of the grout column and attenuates towards the distal end for small loads.The shear stress becomes uniformly distributed when the applied load is approximately 50%of the ultimate pullout load.The anchors designed to test failure mode C were installed with an endplate and had a higher toughness than the straight bar anchors.The shear stress on the grout-rock interface is the largest at the endplate and attenuates upward before slip starts along the interface.When the ultimate pullout load is reached,and the grout column starts to slip,the shear stress is approximately constant.The bond shear strength on the anchor-grout interface was approximately 20%of the uniaxial compressive strength of the grout,and the bond strength of the grout-rock interface was around 5%for that of the grout.The grout-rock interface is likely determined by whichever is weaker,the grout or the rock.展开更多
In rock engineering,the shear strength of the basalt-concrete bonding interface is a key factor affecting the shear performance of hydroelectric dam foundations,embedded rock piles and rock bolts.In this study,30 sets...In rock engineering,the shear strength of the basalt-concrete bonding interface is a key factor affecting the shear performance of hydroelectric dam foundations,embedded rock piles and rock bolts.In this study,30 sets of in-situ direct shear tests were conducted on the basalt-concrete bond interface in the Baihetan dam area to investigate the shear strength characteristics of the basalt-concrete bonding interface.The bonding interface contains two states,i.e.,the bonding interface is not sheared,termed as se(symbolic meaning see Table 1);the bonding interface is sheared with rupture surface,termed as si.The effects of lithology,Joints structure,rock type grade and concrete compressive strength on the shear strength of the concrete-basalt contact surface were investigated.The test results show that the shear strength of the bonding interface(s_(e)&s_(i))of columnar jointed basalt with concrete is greater than that of the bonding interface(s_(e)&s_(i))of non-columnar jointed one with the same rock type grade.When the rock type grade isⅢ_(2),fcol is 1.22 times higher than fncol and ccol is 1.13 times greater than cncol.The shear strength parameters of the basalt-concrete bonding interface differ significantly for different lithologies.The cohesion of the bonding interface(s_(i))of cryptocrystalline basalt with concrete is 2.05 times higher than that of the bonding interface(s_(i))of breccia lava with concrete under the same rock type grade condition.Rock type grade has a large influence on the shear strength of the non-columnar jointed basalt-concrete bonding interface(s_(e)&s_(i)).cnol increases by 33%when the grade of rock type rises fromⅢ_(1)toⅡ_(1).the rock type grade has a greater effect on bonding interface(s_(i))cohesion than the coefficient of friction.When the rock type grade is reduced fromⅢ_(2)toⅢ_(1),f_(ncol)′increases by 2%and c_(ncol)′improves by 44%.The shear strength of the non-columnar jointed basalt-concrete bonding interface(s_(e)&s_(i))increases with the increase of the compressive strength of concrete.When concrete compressive strength rises from 22.2 to 27.6 MPa,the cohesion increases by 94%.展开更多
3D concrete printing has the potential to replace shotcrete for construction of linings of tunnels in hard rock.The shear strength of the interface between rock and printed concrete is vital,especially at super-early ...3D concrete printing has the potential to replace shotcrete for construction of linings of tunnels in hard rock.The shear strength of the interface between rock and printed concrete is vital,especially at super-early ages.However,traditional methods for testing the shear strength of the interface,e.g.,the direct shear test,are time-consuming and result in a high variability for fast-hardening printed concrete.In this paper,a new fast bond shear test is proposed.Each test can be completed in 1 min,with another 2 min for preparing the next test.The influence of the matrix composition,the age of the printed matrices,and the interface roughness of the artificial rock substrate on the shear strength of the interface was experimentally studied.The tests were conducted at the age of the matrices at the 1st,the 4th,the 8th,the 16th,the 32nd,and the 64th min after its final setting.A dimensionless formula was established to calculate the shear strength,accounting for the age of the printed matrices,the interface roughness,and the shear failure modes.It was validated by comparing the calculated results and the experimental results of one group of samples.展开更多
目的:研究3种粘接剂对抛光及上釉锆瓷与正畸金属托槽粘接强度和耐久性的影响。方法:选用2种通用型粘接剂Single Bond Universal(SBU)和Prime&Bond Universal(PBU),以TransbondTMMIP(TM)为对照分别将抛光组、上釉组锆瓷与上颌中切牙...目的:研究3种粘接剂对抛光及上釉锆瓷与正畸金属托槽粘接强度和耐久性的影响。方法:选用2种通用型粘接剂Single Bond Universal(SBU)和Prime&Bond Universal(PBU),以TransbondTMMIP(TM)为对照分别将抛光组、上釉组锆瓷与上颌中切牙金属托槽粘接,试样共6组(n=20)。水浴或水浴+冷热循环储存后测试全部试件剪切粘接强度(SBS),分析断裂形态以及粘接剂残留指数(ARI)。结果:粘接剂(P<0.001)和储存条件(P<0.001)显著影响锆瓷与托槽的剪切粘接强度;抛光或上釉(P=0.09)组间无统计学差异。SBU在各组中都表现出较强的粘接强度和较低的ARI,3种粘接剂间的ARI分数存在显著差异(P<0.001)。结论:粘接金属托槽与抛光及上釉锆瓷时,SBU较PBU和TM有更好的粘接性能。展开更多
目的:评估第八代通用型粘结剂Single Bond Universal对玻璃陶瓷与树脂的粘结强度。方法:选用玻璃陶瓷块40个,经砂纸打磨,超声波清洁后,随机分成4组,每组10个,分别用不同的瓷表面处理方式:对照组不处理,硅烷偶联剂处理组,HF酸处理组,HF酸...目的:评估第八代通用型粘结剂Single Bond Universal对玻璃陶瓷与树脂的粘结强度。方法:选用玻璃陶瓷块40个,经砂纸打磨,超声波清洁后,随机分成4组,每组10个,分别用不同的瓷表面处理方式:对照组不处理,硅烷偶联剂处理组,HF酸处理组,HF酸+硅烷偶联剂处理组。各组经处理后于瓷块处理表面涂布Single Bond Universal粘结剂,粘结树脂制成试件。试件经冷热循环处理5000次后,将试件置于37℃蒸馏水中保存24 h取出,使用万能力学测试仪测试各试件的抗剪切强度,并用扫描电镜观察断裂面的断裂模式。结果:在试件的抗剪切强度方面,HF酸处理组(12.7851±0.8677)MPa、HF酸+硅烷偶联剂处理组(14.7292±0.8847)MPa明显高于硅烷偶联剂处理组(4.5890±1.1483)MPa和对照组(2.0637±0.2011)MPa,而HF酸处理组、HF酸+硅烷偶联剂处理组间差异无统计学意义。在断裂模式方面,HF酸处理组和HF酸+硅烷偶联剂处理组的断裂模式主要以内聚破坏和混合破坏为主。结论:当使用Single Bond Universal粘结剂粘结复合树脂与玻璃陶瓷时,不使用硅烷偶联剂即可达到较为理想的粘结效果,为临床使用Single Bond Universal粘结剂进行树脂修补玻璃陶瓷修复体缺损提供了理论依据。展开更多
Background: To date there is not a material considered ideal for the lased dentin. Objective: To compare the bond strength to human lased dentin of self-etch and etch-and-rinse adhesive systems, a self-adhesive resin ...Background: To date there is not a material considered ideal for the lased dentin. Objective: To compare the bond strength to human lased dentin of self-etch and etch-and-rinse adhesive systems, a self-adhesive resin composite and a glass-ionomer cement. Methods: Forty human molars were sectioned to obtain a 2 mm-thick slab of mid-coronal dentin. The occlusal surface of each slab was polished by SiC paper (P600) for 10 s. Then an half part of dentin slabs was randomly selected for receiving treatment with 2.94 μm Er:YAG laser (DEKA, Smart 2940D Plus) with 10 Hz at 100 mJ, pulse duration of 230 μs with contact tip. Dentin slabs were randomly divided into four groups (n = 10). Six conical frustum-shaped build-ups were constructed on the occlusal surface of each dentin slab using bonding agents (OptiBond Solo Plus Group 1;OptiBond All-in-one Group 2) combined with a resin composite (Premise Flow), self-adhesive resin composites (Vertise Flow Group 3) and a glass-ionomer cement (Ketac-Fil Group 4). Specimens were subjected to μSBS test. Data were analyzed by a mixed model and Tukey’s test. Results: Measured bond strengths were (mean ± standard deviation): 20.8 ± 5.5 MPa (laser treatment) and 15.6 ± 4.5 MPa (SiC paper) for Group 1, 18.9 ± 5.3 MPa (laser treatment) and 14.0 ± 4.3 MPa (SiC paper) for Group 2, 7.9 ± 2.8 MPa (laser treatment) and 4.3 ± 2.2 MPa (SiC paper) for Group 3, 4.7 ± 1.9 MPa (laser treatment) and 2.6 ± 1.2 MPa (SiC paper) for Group 4. The inferential analysis showed that the dentin laser treatment significantly affected the bond strength within each individual group. On dentin treated with laser the bond strengths recorded for build-ups constructed with etch and rinse and self-etch adhesive systems were significantly higher than those recorded for build-ups constructed with self-adhesive resin composite and glass-ionomer cement (p < 0.0001). Similarly, on dentin treated with SiC paper the bond strengths recorded for build-ups constructed with etch and rinse and self-etch adhesive systems were significantly higher than those recorded for build-ups constructed with self-adhesive resin composite and glass-ionomer cement (p < 0.0001). Conclusion: Er:YAG laser treatment has increased the shear bond strength of all the adhesive materials used.展开更多
基金supported by National High-Tech Research and Development Program of China(863 Program)(No.2006AA03Z440)
文摘Objective:To evaluate the shear bond strength(SBS) between alumina-toughened zirconia (ATZ) cores and veneering ceramics,investigate the effect of aging in artificial saliva on SBS and compare it with that of yttria-stabilized tetragonal zirconia polycrystals(Y-TZP).Methods:Bars of ATZ and Y-TZP were layered with veneering ceramics in accordance to the recommendation of the manufacturer.Half of each group(n = 10) was aged at 134℃.(under 2 bar pressure) in an autoclave for 48 h.Subsequently,all specimens were subjected to shear force in a universal testing machine.The interface and fractured surface of the specimens were evaluated using scanning electron microscopy and X-ray energy dispersive spectroscopy.Results:The initial mean SBS values in MPa±SD were 28.9±8.0 for ATZ and 26.2±7.6 for Y-TZP.After aging,the mean SBS values for ATZ and Y-TZP were 22.9±4.9 MPa and 22.8±6.9 MPa,respectively.Neither the differences between the SBS values of the ATZ and Y-TZP groups nor the influence of aging on all groups were statistically significant.Conclusions:The SBS between the ATZ core and the veneering ceramics was not affected by aging.The SBS of ATZ to veneering ceramics was not significantly different compared with that of Y-TZP.
文摘Rock anchors are a common safety measure for stabilising large-scale infrastructure,such as bridge towers,retaining walls,rock slopes and windmills.There are four principal failure modes for rock anchors:(a)tensile failure of the steel anchor,(b)anchor-grout interface failure,(c)grout-rock interface failure,and(d)rock mass uplift.Field tests were performed in a limestone quarry.These tests were designed to test failure modes B and C through pullout.In the tests of failure mode B,the shear stress on the anchor-grout interface is the largest at the top of the grout column and attenuates towards the distal end for small loads.The shear stress becomes uniformly distributed when the applied load is approximately 50%of the ultimate pullout load.The anchors designed to test failure mode C were installed with an endplate and had a higher toughness than the straight bar anchors.The shear stress on the grout-rock interface is the largest at the endplate and attenuates upward before slip starts along the interface.When the ultimate pullout load is reached,and the grout column starts to slip,the shear stress is approximately constant.The bond shear strength on the anchor-grout interface was approximately 20%of the uniaxial compressive strength of the grout,and the bond strength of the grout-rock interface was around 5%for that of the grout.The grout-rock interface is likely determined by whichever is weaker,the grout or the rock.
基金supported by the National Natural Science Foundation of China Key Projects of International Cooperation and Exchanges(No.42020104006)the National Natural Science Foundation of China(No.41630643)+1 种基金the Fundamental Research Funds for the Central Universities(No.CUGCJ1701)the Scientific Research Project of China Three Gorges Corporation LTD.
文摘In rock engineering,the shear strength of the basalt-concrete bonding interface is a key factor affecting the shear performance of hydroelectric dam foundations,embedded rock piles and rock bolts.In this study,30 sets of in-situ direct shear tests were conducted on the basalt-concrete bond interface in the Baihetan dam area to investigate the shear strength characteristics of the basalt-concrete bonding interface.The bonding interface contains two states,i.e.,the bonding interface is not sheared,termed as se(symbolic meaning see Table 1);the bonding interface is sheared with rupture surface,termed as si.The effects of lithology,Joints structure,rock type grade and concrete compressive strength on the shear strength of the concrete-basalt contact surface were investigated.The test results show that the shear strength of the bonding interface(s_(e)&s_(i))of columnar jointed basalt with concrete is greater than that of the bonding interface(s_(e)&s_(i))of non-columnar jointed one with the same rock type grade.When the rock type grade isⅢ_(2),fcol is 1.22 times higher than fncol and ccol is 1.13 times greater than cncol.The shear strength parameters of the basalt-concrete bonding interface differ significantly for different lithologies.The cohesion of the bonding interface(s_(i))of cryptocrystalline basalt with concrete is 2.05 times higher than that of the bonding interface(s_(i))of breccia lava with concrete under the same rock type grade condition.Rock type grade has a large influence on the shear strength of the non-columnar jointed basalt-concrete bonding interface(s_(e)&s_(i)).cnol increases by 33%when the grade of rock type rises fromⅢ_(1)toⅡ_(1).the rock type grade has a greater effect on bonding interface(s_(i))cohesion than the coefficient of friction.When the rock type grade is reduced fromⅢ_(2)toⅢ_(1),f_(ncol)′increases by 2%and c_(ncol)′improves by 44%.The shear strength of the non-columnar jointed basalt-concrete bonding interface(s_(e)&s_(i))increases with the increase of the compressive strength of concrete.When concrete compressive strength rises from 22.2 to 27.6 MPa,the cohesion increases by 94%.
基金Financial support by the Ministry of Science and Technology of China(No.2021YFE0114100)by the Federal Ministry of Education,Science and Research(BMBWF)of Austria(No.CN11/2021)+5 种基金jointly provided for the project‘Intense Upgrades of the New Austrian Tunnelling Method(NATM)and Demonstration of its Applicability to High-Quality Urban Development’,is gratefully acknowledgedsupported by the Science and Technology Commission of Shanghai Municipality(No.21DZ1203505)the National Natural Science Foundation of China(Grant Nos.51908424 and U1934210)Shanghai Rising-Star Program(No.22QB1405000)Jiangxi Province Department of Transportation Key Engineering Project(No.2021C0008)the financial support provided by the Chinese Scholarship Council(CSC,No.202006260198).
文摘3D concrete printing has the potential to replace shotcrete for construction of linings of tunnels in hard rock.The shear strength of the interface between rock and printed concrete is vital,especially at super-early ages.However,traditional methods for testing the shear strength of the interface,e.g.,the direct shear test,are time-consuming and result in a high variability for fast-hardening printed concrete.In this paper,a new fast bond shear test is proposed.Each test can be completed in 1 min,with another 2 min for preparing the next test.The influence of the matrix composition,the age of the printed matrices,and the interface roughness of the artificial rock substrate on the shear strength of the interface was experimentally studied.The tests were conducted at the age of the matrices at the 1st,the 4th,the 8th,the 16th,the 32nd,and the 64th min after its final setting.A dimensionless formula was established to calculate the shear strength,accounting for the age of the printed matrices,the interface roughness,and the shear failure modes.It was validated by comparing the calculated results and the experimental results of one group of samples.
文摘目的:研究3种粘接剂对抛光及上釉锆瓷与正畸金属托槽粘接强度和耐久性的影响。方法:选用2种通用型粘接剂Single Bond Universal(SBU)和Prime&Bond Universal(PBU),以TransbondTMMIP(TM)为对照分别将抛光组、上釉组锆瓷与上颌中切牙金属托槽粘接,试样共6组(n=20)。水浴或水浴+冷热循环储存后测试全部试件剪切粘接强度(SBS),分析断裂形态以及粘接剂残留指数(ARI)。结果:粘接剂(P<0.001)和储存条件(P<0.001)显著影响锆瓷与托槽的剪切粘接强度;抛光或上釉(P=0.09)组间无统计学差异。SBU在各组中都表现出较强的粘接强度和较低的ARI,3种粘接剂间的ARI分数存在显著差异(P<0.001)。结论:粘接金属托槽与抛光及上釉锆瓷时,SBU较PBU和TM有更好的粘接性能。
文摘目的:评估第八代通用型粘结剂Single Bond Universal对玻璃陶瓷与树脂的粘结强度。方法:选用玻璃陶瓷块40个,经砂纸打磨,超声波清洁后,随机分成4组,每组10个,分别用不同的瓷表面处理方式:对照组不处理,硅烷偶联剂处理组,HF酸处理组,HF酸+硅烷偶联剂处理组。各组经处理后于瓷块处理表面涂布Single Bond Universal粘结剂,粘结树脂制成试件。试件经冷热循环处理5000次后,将试件置于37℃蒸馏水中保存24 h取出,使用万能力学测试仪测试各试件的抗剪切强度,并用扫描电镜观察断裂面的断裂模式。结果:在试件的抗剪切强度方面,HF酸处理组(12.7851±0.8677)MPa、HF酸+硅烷偶联剂处理组(14.7292±0.8847)MPa明显高于硅烷偶联剂处理组(4.5890±1.1483)MPa和对照组(2.0637±0.2011)MPa,而HF酸处理组、HF酸+硅烷偶联剂处理组间差异无统计学意义。在断裂模式方面,HF酸处理组和HF酸+硅烷偶联剂处理组的断裂模式主要以内聚破坏和混合破坏为主。结论:当使用Single Bond Universal粘结剂粘结复合树脂与玻璃陶瓷时,不使用硅烷偶联剂即可达到较为理想的粘结效果,为临床使用Single Bond Universal粘结剂进行树脂修补玻璃陶瓷修复体缺损提供了理论依据。
文摘Background: To date there is not a material considered ideal for the lased dentin. Objective: To compare the bond strength to human lased dentin of self-etch and etch-and-rinse adhesive systems, a self-adhesive resin composite and a glass-ionomer cement. Methods: Forty human molars were sectioned to obtain a 2 mm-thick slab of mid-coronal dentin. The occlusal surface of each slab was polished by SiC paper (P600) for 10 s. Then an half part of dentin slabs was randomly selected for receiving treatment with 2.94 μm Er:YAG laser (DEKA, Smart 2940D Plus) with 10 Hz at 100 mJ, pulse duration of 230 μs with contact tip. Dentin slabs were randomly divided into four groups (n = 10). Six conical frustum-shaped build-ups were constructed on the occlusal surface of each dentin slab using bonding agents (OptiBond Solo Plus Group 1;OptiBond All-in-one Group 2) combined with a resin composite (Premise Flow), self-adhesive resin composites (Vertise Flow Group 3) and a glass-ionomer cement (Ketac-Fil Group 4). Specimens were subjected to μSBS test. Data were analyzed by a mixed model and Tukey’s test. Results: Measured bond strengths were (mean ± standard deviation): 20.8 ± 5.5 MPa (laser treatment) and 15.6 ± 4.5 MPa (SiC paper) for Group 1, 18.9 ± 5.3 MPa (laser treatment) and 14.0 ± 4.3 MPa (SiC paper) for Group 2, 7.9 ± 2.8 MPa (laser treatment) and 4.3 ± 2.2 MPa (SiC paper) for Group 3, 4.7 ± 1.9 MPa (laser treatment) and 2.6 ± 1.2 MPa (SiC paper) for Group 4. The inferential analysis showed that the dentin laser treatment significantly affected the bond strength within each individual group. On dentin treated with laser the bond strengths recorded for build-ups constructed with etch and rinse and self-etch adhesive systems were significantly higher than those recorded for build-ups constructed with self-adhesive resin composite and glass-ionomer cement (p < 0.0001). Similarly, on dentin treated with SiC paper the bond strengths recorded for build-ups constructed with etch and rinse and self-etch adhesive systems were significantly higher than those recorded for build-ups constructed with self-adhesive resin composite and glass-ionomer cement (p < 0.0001). Conclusion: Er:YAG laser treatment has increased the shear bond strength of all the adhesive materials used.