Propagation of Iamb waves in adhesively bonded multilayered media

The effect of introducing attenuation on Lamb wave dispersion curves is studied in this paper. Attenuation is introduced to a three-layered composite plate by an adhesive bond layer with viscous behavior. No changes are required to the transfer matrix formulation for the propagation of elastic waves. By introduction of a complex wavenumber, the model can be used to the propagation of attenuative Lamb waves. Numerical examples for a three-layered aluminium-epoxy-aluminium plate show that attenuation values of each mode in plates are related not only to attenuation, but also to the thickness of the bonded layer, which is in agreement with practical situations.

The dynamic stress intensity factor analysis of adhesively bonded material interface crack with damage under shear loading

This paper studies the dynamic stress intensity factor （DSIF） at the interface in an adhesive joint under shear loading. Material damage is considered. By introducing the dislocation density function and using the integral transform, the problem is reduced to algebraic equations and can be solved with the collocation dots method in the Laplace domain. Time response of DSIF is calculated with the inverse Laplace integral transform. The results show that the mode Ⅱ DSIF increases with the shear relaxation parameter, shear module and Poisson ratio, while decreases with the swell relaxation parameter. Damage shielding only occurs at the initial stage of crack propagation. The singular index of crack tip is -0.5 and independent on the material parameters, damage conditions of materials, and time. The oscillatory index is controlled by viscoelastic material parameters.

Determination of key parameters of Al–Li alloy adhesively bonded joints using cohesive zone model

The key parameters of the adhesive layer of a reinforcing patch are of great significance and affect the ability to suppress crack propagation in an Al–Li alloy patch-reinforced structure.This paper proposes a method to determine the key parameters of the adhesive layer of adhesively bonded joints in the Al–Li alloy patch-reinforced structure.A zero-thickness cohesive zone model(CZM)was selected to simulate the adhesive layer’s fracture process,and an orthogonal simulation was designed to compare against the test results.A three-dimensional progressive damage model of an Al–Li alloy patch-reinforced structure with single-lap adhesively bonded joints was developed.The simulation’s results closely agree with the test results,demonstrating that this method of determining the key parameters is likely accurate.The results also verify the correctness of the cohesive strength and fracture energy,the two key parameters of the cohesive zone model.The model can accurately predict the strength and fracture process of adhesively bonded joints,and can be used in research to suppress crack propagation in Al–Li alloy patch-reinforced structures.

Damage Failure Analysis of Z-Pins Reinforced Composite Adhesively Bonded Single-Lap Joint

In order to study themechanical properties of Z-pins reinforced laminated composite single-lap adhesively bonded joint under un-directional static tensile load,damage failure analysis of the joint was carried out bymeans of test and numerical simulation.The failure mode and mechanism of the joint were analyzed by tensile failure experiments.According to the experimental results,the joint exhibits mixed failure,and the ultimate failure is Z-pins pulling out of the adherend.In order to study the failure mechanism of the joint,the finite element method is used to predict the failure strength.The numerical results are in good agreement with the experimental results,and the error is 6.0%,which proves the validity of the numerical model.Through progressive damage failure analysis,it is found that matrix tensile failure of laminate at the edge of Z-pins occurs first,then adhesive layer failure-proceeds at the edge of Z-pins,and finally matrix-fiber shear failure of the laminate takes place.With the increase of load,the matrix-fiber shear failure expands gradually in the X direction,and at the same time,the matrix tensile failure at the hole edge gradually extends in different directions,which is consistent with the experimental results.

An Experimental and Numerical Study of Effect of Textured Surface by Arc Discharge on Strength of Adhesively Bonded Joints

Aluminum alloys are being increasingly applied in the automotive industry as a means to reduce mass. Their application to the vehicle structure is typically via a combination of either mechanical or fusion joining with adhesive bonding. Correspondingly, there has been a large effort in improving the adhesive bonding characteristics by changing the surface properties using different surface treatment techniques. One such method is the atmospheric arc discharge process which develops a specific surface roughness which can be leveraged to improve adhesive bonding. In this paper the effect of a textured surface by arc discharge on the failure mode and strength of adhesively bonded aluminum alloy sheets is investigated. A single-lap joint configuration is used for simulation and experimental analysis. A two-dimensional （2D） finite element method （FEM） involving the morphology of treated surfaces and using interfacial elements based on a cohesive zone model （CZM） are used to predict the joint strength which is an enabler for faster product development cycles. The influence of arc process parameters： the arc current and the torch scanning speed, on the surface morphology and joint strength are explored in this study. Specifically, the present study shows that the surface treatment of aluminum alloys by arc discharge can strongly enhance adhesive bond strength. Additionally, arc treatment not only increases the joint strength but also improves the quality of bond along the interface （transition toward cohesive failure mode）. The current FE simulation of adhesive joint using the elastic and elasto-plastic （non-linear） material properties for adherend and adhesive, respectively, and cohesive zone elements for interface shows an accurate prediction of the resulting joint strength. By inclusion of non-linear multi-scale geometry model via considering the surface topographical changes after surface treatment the FE joint strength prediction can be successfully implemented.

Influence of adhesive layer properties on laser-generated ultrasonic waves in thin bonded plates

This paper studies quantitatively the generation of Lamb waves in thin bonded plates subjected to laser illumination, after considering the viscoelasticity of the adhesive layer. The displacements of such plates have been calculated in the frequency domain by using the finite element method, and the time domain response has been reconstructed by applying an inverse fast Fourier transform. Numerical results are presented showing the normal surface displacement for several configurations： a single aluminum plate, a three-layer bonded plate, and a two-layer plate. The characteristics of the laser-generated Lamb waves for each particular case have been investigated. In addition, the sensitivity of the transient responses to variations of material properties （elastic modulus, viscoelastic modulus, and thickness） of the adhesive layer has been studied in detail.

Effect of hot-humid exposure on static strength of adhesive-bonded aluminum alloys

The effect of hot-humid exposure(i.e., 40 C and 98% R.H.) on the quasi-static strength of the adhesive-bonded aluminum alloys was studied. Test results show that the hot-humid exposure leads to the significant decrease in the joint strength and the change of the failure mode from a mixed cohesive and adhesive failure with cohesive failure being dominant to adhesive failure being dominant. Careful analyses of the results reveal that the physical bond is likely responsible for the bond adhesion between L adhesive and aluminum substrates. The reduction in joint strength and the change of the failure mode resulted from the degradation in bond adhesion, which was primarily attributed to the corrosion of aluminum substrate. In addition, the elevated temperature exposure significantly accelerated the corrosion reaction of aluminum, which accelerated the degradation in joint strength.

Dynamic fracture analysis of adhesive bonded material under normal loading

Dynamic fracture behavior of a Griffith crack along the interface of an adhesive bonded material under normal loading is studied. The singular integral equations are obtained by employing integral transformation and introducing dislocation density functions. By adopting Gauss-Jacobi integration formula, the problem is reduced to the solution of algebraic equations, and by collocation dots method. their solutions can be obtained Based on the parametric discussions presented in the paper, the following conclusions can be drawn： （1） Mode I dynamic stress intensity factor （DSIF） increases with increasing initial crack length and decreasing visco-elastic layer thickness, revealing distinct size effect; （2） The influence of the visco-elastic adhesive relaxation time on the DSIF should not be ignored.

Effect of Multiple Coatings of One-step Self-etching Adhesive on Microtensile Bond Strength to Primary Dentin

Objective To investigate the effect of multiple coatings of the one-step self-etching adhesive on immediate microtensile bond strength to primary dentin.Methods Twelve caries-free human primary molars were randomly divided into 2 groups with 6 teeth each.In group 1,each tooth was hemisected into two halves.One half was assigned to control subgroup 1,which was bonded with a single-step self-etching adhesive according to the manufacturer's instructions;the other half was assigned to experimental subgroup 1 in which the adhesive was applied three times before light curing.In group 2,the teeth were also hemisected into two halves.One half was assigned to control subgroup 2,which was bonded with the single-step self-etching adhesive according to the manufacturer's instructions;the other half was assigned to experimental subgroup 2 in which three layers of adhesive were applied with light curing each successive layer.Microtensile bond strength was immediately tested after specimen preparation.Results When the adhesive was applied three times before light curing,the bond strength of the experimental subgroup 1(n=33,57.49±11.61 MPa) was higher than that of the control subgroup 1(n=31,49.71±11.43 MPa,P<0.05).When using the technique of applying multiple layers of adhesive with light curing each successive layer,no difference of immediate bond strength was observed between the control subgroup 2 and the experimental subgroup 2(P>0.05).Conclusion Multiple coatings of one-step self-etching adhesive can increase the immediate bond strength to primary dentin when using the technique of light-curing after applying three layers of adhesive.

Diffusive-stochastic-viscoelastic model on specific adhesion of viscoelastic solids via molecular bonds

A diffusive-stochastic-viscoelastic model is proposed for the specific adhesion of viscoelastic solids via stochastically formed molecular bonds. In this model, we assumed that molecular level behaviours, including the diffusion of mobile adhesion molecules and stochastic reaction between adhesion molecules and binding sites, obey the Markovian stochastic processes, while mesoscopic deformations of the viscoelastic media are governed by continuum mechanics. Through Monte Carlo simulations of this model, we systematically investigated how the competition between time scales of molecular diffusion, reaction, and deformation creep of the solids may influence the lifetime and dynamic strength of the adhesion. We revealed that there exists an optimal characteristic time of molecule diffusion corresponding to the longest lifetime and largest adhesion strength, which is in good agreement with experimental observed characteristic time scales of molecular diffusion in cell membranes. In addition, we identified that the media viscosity can significantly increase the lifetime and dynamic strength, since the deformation creep and stress relaxation can effectively reduce the concentration of interfacial stress and increases the rebinding probability of molecular bonds.

Adhesive Bonding and Self-Curing Characteristics of α-Starch Based Composite Binder for Green Sand Mould/Core

Interactions between different components in α-starch based composite binder for green sand mould/core were investigated by using XRD, IR spectra, 1H NMR spectra and SEM. Several adhesive hardening structures and theories of the binder at room temperature were proposed according to the interactions between various compositions. Thus, the reasons for the binder to have excellent combination properties and unique adhesive bonding and self-curing characteristics were explained by these theories successfully. And the theories are of great directive importance to design and development of composite binder for green sand mould/core.

Experimental study about the influence of adhesive stiffness to the bonding strengths of adhesives for ceramic/metal targets

The aim of the investigations presented here was to understand how the stiffness of the adhesive affects the failure of ceramic tiles adhered to metallic backings. The working hypothesis was that varying the adhesive stiffness could have the same effect on the ballistic performance as a variation of the adhesive thickness.Two different projectile/target combinations were utilized for ballistic tests in order to generate extremely different loading conditions. With targets consisting of 6 mm aluminum oxide ceramic and 6 mm aluminum backing, complete penetration occurred in each test with 7.62 mm tungsten carbide core AP ammunition at an impact velocity of 940 m/s. In contrast, with ceramic tiles of 20 mm thickness on 13 mm steel backing,no penetration of the ceramic occurred at the impact of a 7.62 mm ball round at 840 m/s.Four different types of adhesive(high-strength till high-flexible) were tested in both configurations. The elongation of the adhesive layer, the deformation of the metallic backing and the failure of the ceramics were observed by means of a high-speed camera during the projectile/target interaction.The results of the ballistic tests showed that a higher fracture strain caused a larger deformation of the backing compared to adhesives, which exhibit a high tensile strength and low fracture strains.The experimental results indicate that the damage behavior of the ceramic/metal composites depends on the absolute elongation of the adhesive layer. This can be controlled either by the thickness or the stiffness of the bonding layer.

Effect of Self-adhesive Resin Cement and Tribochemical Treatment on Bond Strength to Zirconia

Aim To evaluate the interactive effects of different self- adhesive resin cements and tribochemical treatment on bond strength to zirconia. Methodology The following self-adhesive resin cements for bonding two zirconia blocks were evaluated： Maxcem （MA）, Smartcem （SM）, Rely X Unicem Aplicap （UN）, Breeze （BR）, Biscem （BI）, Set （SE）, and Clearfil SA luting （CL）. The specimens were grouped according to conditioning as follows： Group 1, polishing with 600 grit polishing paper; Group 2, silica coating with 110 μm Al2O3 particles which modified with silica; and, Group 3, tribochemical treatment - silica coating ＋ silanization. Specimens were stored in distilled water at 37℃ for 24 hours before testing shear bond strength. Results Silica coating and tribochemical treatment significantly increased the bond strength of the MA, UN, BR, B1, SE and CL to zirconia compared to #600 polishing. For both #600 polished and silica coating treatments, MDP- containing self-adhesive resin cement CL had the highest bond strengths to zirconia. Conclusion Applying silica coating and tribochemical treatment improved the bond strength of self-adhesive resin cement to zirconia, especially for CL.

Influence of Phosphoric Acid Etching on the Bond Strength of a Universal Adhesive System to Caries-Affected Dentin

The purpose of this study was to evaluate the influence of acid etching on the bond strength of a universal adhesive system (Single Bond Universal, 3M) to caries-affected dentin. Forty permanent third molars were selected and carious lesions were induced by the microbiological method with?S. mutans?ATCC25175. Teeth were allocated randomly across four experimental designs (n?=?10): PA-I: phosphoric acid etching and application of the adhesive system, followed by immediate microtensile bond strength testing;PA-CC: phosphoric acid etching and application of the adhesive system, followed by microtensile bond strength testing after a 14-day cariogenic challenge;NPA-I: application of the adhesive system without acid etching, followed by immediate bond strength testing and NPA-CC: application of the adhesive system without acid etching followed by bond strength testing after 14-day cariogenic challenge. For microtensile bond strength testing,?a restoration with Charisma composite resin was made and each specimen was sectioned with a cross-sectional area of 1 mm2. Only adhesive and mixed fractures were considered for bond strength calculation. Results were evaluated by the Kruskal-Wallis and Friedman tests. The highest bond strengths were observed in the phosphoric acid etching groups (p??0.05). Cariogenic challenge did not affect bond strength (p?>?0.05). The predominant fracture type was adhesive. We conclude that phosphoric acid increased the bond strength of the Single Bond Universal system to caries-affected dentin, and that cariogenic challenge did not interfere with this bond strength.

An in Vitro Comparison of Bonding Effectiveness of Different Adhesive Strategies on Erbium:Yttrium-Alluminum-Garnet Laser Irradiated Dentin

Background: To date there is not a material considered ideal for the lased dentin. Objective: To compare the bond strength to human lased dentin of self-etch and etch-and-rinse adhesive systems, a self-adhesive resin composite and a glass-ionomer cement. Methods: Forty human molars were sectioned to obtain a 2 mm-thick slab of mid-coronal dentin. The occlusal surface of each slab was polished by SiC paper (P600) for 10 s. Then an half part of dentin slabs was randomly selected for receiving treatment with 2.94 μm Er:YAG laser (DEKA, Smart 2940D Plus) with 10 Hz at 100 mJ, pulse duration of 230 μs with contact tip. Dentin slabs were randomly divided into four groups (n = 10). Six conical frustum-shaped build-ups were constructed on the occlusal surface of each dentin slab using bonding agents (OptiBond Solo Plus Group 1;OptiBond All-in-one Group 2) combined with a resin composite (Premise Flow), self-adhesive resin composites (Vertise Flow Group 3) and a glass-ionomer cement (Ketac-Fil Group 4). Specimens were subjected to μSBS test. Data were analyzed by a mixed model and Tukey’s test. Results: Measured bond strengths were (mean ± standard deviation): 20.8 ± 5.5 MPa (laser treatment) and 15.6 ± 4.5 MPa (SiC paper) for Group 1, 18.9 ± 5.3 MPa (laser treatment) and 14.0 ± 4.3 MPa (SiC paper) for Group 2, 7.9 ± 2.8 MPa (laser treatment) and 4.3 ± 2.2 MPa (SiC paper) for Group 3, 4.7 ± 1.9 MPa (laser treatment) and 2.6 ± 1.2 MPa (SiC paper) for Group 4. The inferential analysis showed that the dentin laser treatment significantly affected the bond strength within each individual group. On dentin treated with laser the bond strengths recorded for build-ups constructed with etch and rinse and self-etch adhesive systems were significantly higher than those recorded for build-ups constructed with self-adhesive resin composite and glass-ionomer cement (p < 0.0001). Similarly, on dentin treated with SiC paper the bond strengths recorded for build-ups constructed with etch and rinse and self-etch adhesive systems were significantly higher than those recorded for build-ups constructed with self-adhesive resin composite and glass-ionomer cement (p < 0.0001). Conclusion: Er:YAG laser treatment has increased the shear bond strength of all the adhesive materials used.

BONDING OF MINIATURE PARTS WITH ADHESIVES AND VISION BASED PROCEDURE INSPECTION

Bonding with adhesives is an important technique for building up hybridmicrosystems. Some adhesives are tested with capillary dispensing system for microassembly, andvolume of droplets less than 10 nl with good repeatability can be acquired. 1-part UV curingadhesive hardens rapidly and is suitable for bonding of transparent microparts. Light-activatedadhesive starts the curing process in an adjustable short period of time after the radiation ofvisible light, and thus suits bonding of non-transparent microparts. A method is proposed forbonding the guides of a miniature linear motor being developed by collaborate research center 516(SFB516) in Germany. With the method high assembly accuracy in the vertical direction can beguaranteed. By making small grooves on the stator for containing adhesive, the deterioration of theaccuracy due to the thickness of adhesive layer can be avoided. The criteria on deciding the size ofthe groove are given and analyzed. Vision based inspection method is introduced for automaticassembly of the guides. The dispensing volume and position of dispensed adhesive droplets can bedetected for ensuring the bonding quality.

Push-out Bond Strength of Self-adhesive Methacrylate Resin-based Sealers to Root Dentin

This study examined the adhesive strength of two self-adhesive methacrylate resin-based sealers（MetaSEAL and RealSeal SE） to root dentin and compared them with RealSeal and AH Plus in properties. A total of 48 extracted human single-rooted teeth were used to prepare the 0.9-mm thick longitudinal tooth slice（each per tooth）. Standardized simulated canal spaces of uniform dimensions were prepared in the middle of radicular dentin. After treated with 5.25% sodium hypochlorite（NaOCl） and 17% EDTA, tooth slices were allocated randomly to four groups（n=12） in terms of different sealers used： MetaSEAL, RealSeal SE, RealSeal, and AH plus groups. The simulated canal spaces were obturated with different sealers in each group. There were 10 slabs with 20 simulated canal spaces（n=20） used in each group for push-out testing. The failure modes and the ultrastructures of fractured sealer-dentin interfaces were examined. The remaining 2 slabs in each group underwent partial demineralization for observation of the ultrastructure of resin tags. The results showed that the push-out bond strength was 12.01±4.66 MPa in MetaSEAL group, significantly higher than that in the other three groups（P0.05）. Moreover, no statistically significant differences were noted in the push-out bond strength between RealSeal SE（5.43±3.68 MPa） and AH Plus（7.34±2.83 MPa） groups and between RealSeal SE and RealSeal（2.93±1.76 MPa） groups（P0.05）. Mixed failures were predominant in the fractured sealer-dentin interfaces in MetaSEAL and AH Plus groups, while adhesive failures were frequently seen in RealSeal SE and RealSeal groups. In conclusion, after complete removal of the smear layer, MetaSEAL showed superior bond ability to root dentin. The RealSeal SE is applicable in clinical practice, with its adhesive strength similar to that of AH Plus. The self-adhesive methacrylate resin-based sealer holds promise for use in endodontic treatment.

Effect of operating temperature on aged single lap bonded joints

In recent decades,designers have increasingly focused on the stability of assemblies in composite materials over time,particularly when used in structural applications.The use of structural adhesives allows for realising assemblies without mechanical fasteners.In fact,bonding is an assembly technique that prevent corrosion,ensures uniform stresses in the joint,and grows the specific resistance of the assembly.The knowledge of the behaviour of bonded joint is necessary to ensure the reliability of this technique over time,especially in aggressive environments.The aim of this wo rk consists in investigating the combined effect of hydrothermal ageing and temperature test on the lap shear strength of single lap joints realised in CFRP.The results showed a higher influence of the ageing on paste adhesive compared to film adhesive.However,the ageing,combined with the operating temperature,played a fundamental role on the shear strength of the bonded joints.

Characterization of Curing and Bonding of Wood with Adhesive Mixtures of Liquefied Wood and Hexamethylenediamine

Various crosslinking agents can be added to the formulations of natural-based adhesives for wood bonding in order to achieve better durability and higher strength of the formed joints.In the present study,the effect of hexamethylenediamine(HMDA)addition on the performance of liquefied wood(LW)adhesive for wood bonding is investigated.Differential scanning calorimetry showed the improved thermal stability and crosslinking of the LW adhesive with HMDA.The intensified presence of amide linkages(C–N bonds)was found in LW+HMDA with attenuated total reflection Fourier transform infrared spectroscopy.Analysis of the bonded joints using an automated bonding evaluation system showed that a higher press temperature resulted in stronger bonds for both types of adhesives.Moreover,the addition of HMDA to LW adhesive improved the bond strength of the joints and accelerated the crosslinking of the adhesive.However,with a tensile shear strength of(6.76±2.16)N×mm^(−2)(for LW)and(6.89±2.10)N×mm^(−2)(for LW+HMDA),both adhesives were found to be unsuitable for interior non-structural use.In addition,the acidity of LW resulted in relatively high wood failure(70%)in the adhesive joints tested.Improved crosslinking of LW with HMDA was reflected in improved resistance of LW+HMDA adhesive joints to water degradation.In conclusion,HMDA is a promising additive for improving the adhesive performance of LW adhesives.

Multiple Coatings can Improve the Bond Durability of One-step Self-etching Adhesive to Primary Dentin

Objective To investigate whether multiple coatings can improve the bond durability of one-step self-etching adhesive to primary dentin. Methods Twelve caries-free human primary molars were randomly divided into 2 groups. In group 1, each tooth was hemisected into 2 halves. One half was assigned to the control subgroup 1, which was bonded with a commercially available one-step self-etching adhesive according to the manufacturer＇s instruc- tions; the other half was assigned to experimental subgroup 1, in which the adhesive was applied three times before light curing. In group 2, one split half tooth was bonded with a commercially available one-step self-etching adhesive according to the manufacturer＇s instructions; for the other half, three layers of adhesive were applied with each successive layer of light curing. Specimens were stored in 0.9% NaC1 containing 0.02% sodium azide at 37℃ for 18 months and then were subjected to microtensile bond strength test and the fracture mode analysis. Results When the adhesive was applied three times before light curing, the bond strength of the ex- perimental subgroup 1 was significantly higher than that of the control subgroup 1 （47.46__＋13.91 vs. 38.12＋11.21 MPa, P〈O.05）. When using the technique of applying multiple layers of adhesive with each successive layer of light curing, no difference was observed in bond strength between the control subgroup and the experimental subgroup （39.40＋8.87 vs. 40.87-＋9.33 MPa, P〉O.05）. Conclusion Multiple coatings can improve the bond durability of one-step self-etching adhesive to primary dentin when using the technique of light-curing after applying 3 layers of adhesive.