Wollastonite, a mineral of wide industrial applications was synthesised from rice husk ash silica and limestone. A number of raw batches consisting of these starting materials, in 1:1 molar ratio, were heat treated to...Wollastonite, a mineral of wide industrial applications was synthesised from rice husk ash silica and limestone. A number of raw batches consisting of these starting materials, in 1:1 molar ratio, were heat treated to produce it through solid state reaction from 900℃ to 1300℃. The conducted reaction was monitored by XRD step by step. Amount of Wollastonite formed at every temperature was also studied to some extent. Analyses of the obtained data indicated that the target mineral formation was quite effective and almost proportional to a rise in temperature up to 1200℃. The results from both, XRD and chemical analysis were found in fair agreement with one another展开更多
In order to solve the high-price and short-lifetime problems of the cutter of agricultural machinery,and improve the wear resistance of the cutter, the TiCN/Fe metal ceramic composite coating was prepared on the subst...In order to solve the high-price and short-lifetime problems of the cutter of agricultural machinery,and improve the wear resistance of the cutter, the TiCN/Fe metal ceramic composite coating was prepared on the substrate of Q235 steel by reaction nitrogen arc cladding technique. The mixture powder of titanium and graphite was preplaced on the Q235 steel surface after intensive mixing by planetary ball mill and gluing with starch binder. The microstructure and phase of the coatings, interface behavior between coatings and the substrate were investigated by scanning electronic microscope and X-ray diffractometer. The micro-hardness distribution of the coating section was tested by micro-hardness tester. Friction coefficient and wear weight loss were measured by abrasion machine. Wearing surface morphology was investigated by scanning electronic microscope. The results show that an excellent bonding between the coatings and the Q235 steel substrate is ensured by the strong metallurgical interface and phase of the coatings. The coatings are mainly composed of TiCN. The highest micro- hardness of the coatings reaches 1 089 HV0. 2, while the micro-hardness of Q235 steel substrate is only about 286 HV0. 2. The anti-abrasive test results show that the wear resistance of the cladding coating is better than that of quenched and tempered 65 Mn steel which is often used as cutter of agricultural machinery. The field test results show that the TiCN/ Fe metal ceramic composite coating prepared by reaction nitrogen arc cladding is feasible to the manufacture and remanufacture of the cutter of agricultural machinery.展开更多
文摘Wollastonite, a mineral of wide industrial applications was synthesised from rice husk ash silica and limestone. A number of raw batches consisting of these starting materials, in 1:1 molar ratio, were heat treated to produce it through solid state reaction from 900℃ to 1300℃. The conducted reaction was monitored by XRD step by step. Amount of Wollastonite formed at every temperature was also studied to some extent. Analyses of the obtained data indicated that the target mineral formation was quite effective and almost proportional to a rise in temperature up to 1200℃. The results from both, XRD and chemical analysis were found in fair agreement with one another
基金financially supported by the Natural Science Foundation of Hebei Province for Distinguished Young Scientists(No.E2011204036)the Natural Science Foundation of Hebei Province(No.E2014204028)the Youth Fund of Hebei Education Department(No.QN2014100)
文摘In order to solve the high-price and short-lifetime problems of the cutter of agricultural machinery,and improve the wear resistance of the cutter, the TiCN/Fe metal ceramic composite coating was prepared on the substrate of Q235 steel by reaction nitrogen arc cladding technique. The mixture powder of titanium and graphite was preplaced on the Q235 steel surface after intensive mixing by planetary ball mill and gluing with starch binder. The microstructure and phase of the coatings, interface behavior between coatings and the substrate were investigated by scanning electronic microscope and X-ray diffractometer. The micro-hardness distribution of the coating section was tested by micro-hardness tester. Friction coefficient and wear weight loss were measured by abrasion machine. Wearing surface morphology was investigated by scanning electronic microscope. The results show that an excellent bonding between the coatings and the Q235 steel substrate is ensured by the strong metallurgical interface and phase of the coatings. The coatings are mainly composed of TiCN. The highest micro- hardness of the coatings reaches 1 089 HV0. 2, while the micro-hardness of Q235 steel substrate is only about 286 HV0. 2. The anti-abrasive test results show that the wear resistance of the cladding coating is better than that of quenched and tempered 65 Mn steel which is often used as cutter of agricultural machinery. The field test results show that the TiCN/ Fe metal ceramic composite coating prepared by reaction nitrogen arc cladding is feasible to the manufacture and remanufacture of the cutter of agricultural machinery.
