The arc characteristics of submerged arc welding (SAW) with stainless steel wire were studied by using Analysator Hannover (AH). The tests were carded out under the same preset arc voltage combined with different ...The arc characteristics of submerged arc welding (SAW) with stainless steel wire were studied by using Analysator Hannover (AH). The tests were carded out under the same preset arc voltage combined with different welding currents. By comparing the probability density distribution (PDD) curves of arc voltage and welding current, the changes were analyzed, the metal transfer mode in SAW was deduced, and the characteristics of a stable arc were summarized. The analysis results show that, with an increase of welding parameters, the short-circuiting peak in the PDD curves of arc voltage decreases gradually until it disappears, and the dominant metal transfer mode changes from flux-wall guided transfer to projected transfer and then to streaming transfer. Moreover, when the PDD curves of arc voltage are both unimodal and generally symmetrical, the greater the peak probability and the smaller the peak span, the more stable the arc becomes.展开更多
This present study applied gas tungsten arc welding in order to join AISI 304 and AISI 201 stainless steels.The objective was to find the optimum welding condition that gave a weld bead in accordance with DIN EN ISO 2...This present study applied gas tungsten arc welding in order to join AISI 304 and AISI 201 stainless steels.The objective was to find the optimum welding condition that gave a weld bead in accordance with DIN EN ISO 25817 quality level B, pitting corrosion potential of the weld metal of not less than that of the AISI304 base metal and a ratio of delta-ferrite in austenite matrix of the weld metal of not lower than 3%.Such a ratio is a criterion widely accepted to protect the weld metal from solidification cracking. At the welding current of 75 A and by using pure argon as a shielding gas 0 to 8 vol.% and applying a welding speed in the range of 2-3.5 mm·s^(-1) was found to give a complete weld bead with an increased depthper-width ratio(promote weldability). For welding speed in the range of 3 and 3.5 mm·s^(-1)(promote corrosion resistance). Increasing the welding speed in such a range decreased the amount of delta-ferrite in the austenite matrix, and increased the pitting corrosion potential of the weld metal to be 302 mV_(SCE).This value was still lower than the pitting corrosion potential of the AISI 304 base metal. Mixing nitrogen in argon shielding gas increased the nitrogen content in the weld. The optimum condition was found when using a welding speed of 3 mm· s^(-1) and mixing 1 vol.% of nitrogen in the argon shielding gas(promote weldability and corrosion resistance). Pitted areas after potentiodynamic test were observed in the austenite in which its Cr content was relatively low.展开更多
A typical 321 stainless steel/aluminum composite coating (321/Al coating) was prepared by high velocity arc spraying technique (HVAS) with 321 stainless steel wire as the anode and aluminum wire as the cathode. The tr...A typical 321 stainless steel/aluminum composite coating (321/Al coating) was prepared by high velocity arc spraying technique (HVAS) with 321 stainless steel wire as the anode and aluminum wire as the cathode. The traditional 321 stainless steel coating was also prepared for comparison. Tribological properties of the coatings were evaluated with the ring-block wear tester under different conditions. The structure and worn surface of the coatings were analyzed by scanning electron microscopy(SEM), X-ray diffractometry(XRD) and energy dispersion spectroscopy(EDS). The results show that, except for aluminum phase addition in the 321/Al coating, no other phases are created compared with the 321 coating. However, due to the addition of aluminum, the 321/Al coating forms a type of "ductile/hard phases inter-deposited" structure and performs quite different tribological behavior. Under the dry sliding condition, the anti-wear property of 321/Al coating is about 42% lower than that of 321 coating. But under the oil lubricated conditions with or without 32 h oil-dipping pretreatment, the anti-wear property of 321/Al coating is about 9% and 5% higher than that of 321 coating, respectively. The anti-wear mechanism of the composite coating is mainly relevant to the decrease of oxide impurities and the strengthening action resulted from the "ductile/hard phases inter-deposited" coating structure.展开更多
The present study is concerned with the effect of filler metals such as austenitic stainless steel, ferritic stainless steel and duplex stainless steel on tensile and impact properties of the ferritic stainless steel ...The present study is concerned with the effect of filler metals such as austenitic stainless steel, ferritic stainless steel and duplex stainless steel on tensile and impact properties of the ferritic stainless steel conforming to AISI 409M grade. Rolled plates of 4 mm thickness were used as the base material for preparing single pass butt welded joints. Tensile and impact properties, microhardness, microstructure and fracture surface morphology of the joints fabricated by austenitic stainless steel, ferritic stainless steel and duplex stainless steel filler metals were evaluated and the results were reported. From this investigation, it is found that the joints fabricated by duplex stainless steel filler metal showed higher tensile strength and hardness compared to the joints fabricated by austenitic and ferritic stainless steel filler metals. Joints fabricated by austenitic stainless steel filler metal exhibited higher ductility and impact toughness compared with the joints fabricated by ferritic stainless steel and duplex stainless steel filler metals.展开更多
Double-sided arc welding with a single power source can effectively increase the weld penetration, diminish distortion, improve welding speed and save energy. Compared to conventional arc welding processes, double-sid...Double-sided arc welding with a single power source can effectively increase the weld penetration, diminish distortion, improve welding speed and save energy. Compared to conventional arc welding processes, double-sided arc welding can generate a penetrating electromaguetic field to help to form fine dendritic microstrueture in the weld due to the symmetry of heating. Type 1Cr1SNi9Ti aastenitic stainless steel was bead-on-plate welded with double-sided arc welding and conventional plasma arc welding processes, respectively, and microstructure in the weld, heat-affected zone and base metal were examined. After analyzing the black carbon-enriched band in the weld during plasma arc welding with electron probe microanalyzer ( EPMA ) and X-ray diffraction (XRD) technology, it was found that the black band was shaped from the aggregation of ferrite in the fasion boundary. Hardness measurement showed that this black band does not apparently affect the microhardncss distribution in the weld.展开更多
AISI 304 stainless steel was ion implanted with Co, and the tribological property on the surface of the stainless steelwas investigated. The Co ion implantation was carried out using a metal vapor vacuum arc (Mevva) b...AISI 304 stainless steel was ion implanted with Co, and the tribological property on the surface of the stainless steelwas investigated. The Co ion implantation was carried out using a metal vapor vacuum arc (Mevva) broad-beam ionsource with an extraction voltage of 40 kV, implantation doses of 3×10^(17)/cm^2 and 5×10^(17)/cm^2, and ion currentdensities of 13, 22 and 32μA/cm^2. The results showed that the near-surface hardness of Co-implanted stainless steelsample was increased by 50% or more, and it increased with increasing ion current density at first and then declined.The friction coefficient decreased from 0.74 to 0.20 after Co implantation. The wear rate after Co implantationreduced by 25% or more as compared to the unimplanted sample. The wear rate initially decreased with increasingion current density and then an increase was observed. Within the range of experimental parameters, there existsa critical ion current density for the Co-implanted stainless steel, at which the wear rate decreased with increasingretained dose, going through a minimum and then increased. The critical ion current density in this paper is about22μA/cm^2.展开更多
Arc ion plating (AIP) is applied to form Ti/(Ti,Cr)N/CrN multilayer coating on the surface of 316L stainless steel (SS316L) as bipolar plates for proton exchange membrane fuel cells (PEMFCs). The characterizations of ...Arc ion plating (AIP) is applied to form Ti/(Ti,Cr)N/CrN multilayer coating on the surface of 316L stainless steel (SS316L) as bipolar plates for proton exchange membrane fuel cells (PEMFCs). The characterizations of the coating are analyzed by scanning electron microscopy (SEM) and X-ray diffraction (XRD). Interfacial contact resistance (ICR) between the coated sample and carbon paper is 4.9 m Omega cm(2) under 150 N/cm(2), which is much lower than that of the SS316L substrate. Potentiodynamic and potentiostatic tests are performed in the simulated PEMFC working conditions to investigate the corrosion behaviors of the coated sample. Superior anticorrosion performance is observed for the coated sample, whose corrosion current density is 0.12 mu A/cm(2). Surface morphology results after corrosion tests indicate that the substrate is well protected by the multilayer coating. Performances of the single cell with the multilayer coated SS316L bipolar plate are improved significantly compared with that of the cell with the uncoated SS316L bipolar plate, presenting a great potential for PEMFC application. (C) 2016 Science Press and Dalian Institute of Chemical Physics, Chinese Academy of Sciences. Published by Elsevier B.V. and Science Press. All rights reserved.展开更多
The present work is aimed at studying the microstructure and pitting corrosion behaviour of shielded metal arc welded high nitrogen steel made of Cromang-N electrode. Basis for selecting this electrode is to increase ...The present work is aimed at studying the microstructure and pitting corrosion behaviour of shielded metal arc welded high nitrogen steel made of Cromang-N electrode. Basis for selecting this electrode is to increase the solubility of nitrogen in weld metal due to high chromium and manganese content. Microscopic studies were carried out using optical microscopy(OM) and field emission scanning electron microscopy(FESEM). Energy back scattered diffraction(EBSD) method was used to determine the phase analysis, grain size and orientation image mapping. Potentio-dynamic polarization testing was carried out to study the pitting corrosion resistance in aerated 3.5% NaCl environment using a GillAC electrochemical system. The investigation results showed that the selected Cr-Mn-N type electrode resulted in a maximum reduction in delta-ferrite and improvement in pitting corrosion resistance of the weld zone was attributed to the coarse austenite grains owing to the reduction in active sites of the austenite/delta ferrite interface and the decrease in galvanic interaction between austenite and delta-ferrite.展开更多
To study the influence laws of welding parameters on weld porosity, underwater wet flux-cored arc welding ( FCAW) duplex stainless steel S32101 was carried out in a hyperbaric chamber, and the second-order multiple ...To study the influence laws of welding parameters on weld porosity, underwater wet flux-cored arc welding ( FCAW) duplex stainless steel S32101 was carried out in a hyperbaric chamber, and the second-order multiple regression equation was established. The interactive effects of welding parameters on the porosity were analyzed by the three dimensional response surfaces and the contour plots. The results present that the interaction effect between water depth and voltage on the porosity is the most significant. Theoretically, a non-pores weld bead can be gained by reasonably matching these parameters with water depth less than 10 m. Always, the weld porosity reaches its peak value with a 7 mm/s welding speed.展开更多
Pulsed current Micro Plasma Arc Welding is used to joint thin sheets of AISI 304L sheets, which are used in manufacturing of metallic bellows and diaphragms. In this article the effects of pulsing current parameters o...Pulsed current Micro Plasma Arc Welding is used to joint thin sheets of AISI 304L sheets, which are used in manufacturing of metallic bellows and diaphragms. In this article the effects of pulsing current parameters on weld pool geometry namely front width, back width, front height and back height of pulsed current micro plasma arc welded AISI 304L stainless steel sheets was analyzed. Four factors, five levels, central composite design was used to develop mathematical models, incorporating pulsed current parameters and weld pool geometry. The mathematical models have been developed by Response Surface Method. The adequacy of the models was checked by ANOVA technique. Variation of output responses with input process variables are discussed. By using the developed mathematical models, weld pool geometry parameters can be predicted.展开更多
The 2205 duplex stainless + DH36 clad steel plate was welded by gas metal arc welding(GMAW), and the welding performance of the clad steel plate was investigated. The results show that the adaptability of the weldi...The 2205 duplex stainless + DH36 clad steel plate was welded by gas metal arc welding(GMAW), and the welding performance of the clad steel plate was investigated. The results show that the adaptability of the welding procedure for the base metal of carbon steel, the transition layer, and the cladding material is excellent. The test results indicate that the phase proportion and component dilution of the GMAW-welded joints of clad steel plate can be effectively controlled to yield joints with good mechanical properties and corrosion resistance.展开更多
An attempt is made to develop the tools that are capable enough to withstand the shear, impact and thermal forces that occur during friction stir welding of stainless steels. The atmospheric plasma spray and plasma tr...An attempt is made to develop the tools that are capable enough to withstand the shear, impact and thermal forces that occur during friction stir welding of stainless steels. The atmospheric plasma spray and plasma transferred arc hardfacing processes are employed to deposit refractory ceramic based composite coatings on the Inconel 738 alloy. Five different combinations of self-fluxing alloy powder and 60% ceramic reinforcement particulate mixtures are used for coating. The best friction stir welding tool selected based on tool wear analysis is used to fabricate the austenitic stainless steel joints.展开更多
The fatigue behaviors of 48MnV steel, both uncoated and coated with different thicknesses of 3Cr13 deposits using twin arc spraying, were investigated. The fatigue properties of the 48MnV steel, determined under axial...The fatigue behaviors of 48MnV steel, both uncoated and coated with different thicknesses of 3Cr13 deposits using twin arc spraying, were investigated. The fatigue properties of the 48MnV steel, determined under axial loading conditions, can be substantially decreased by coating 3Cr13 films, deposited by twin arc spraying. And the fatigue behavior of the thinner coatings is better than that of the thicker ones, of which the fatigue limits decrease by 9%[CD*2]14%. The decrease in fatigue life attributes to the less mechanical properties of the coatings in comparison with those of the substrate, their relative bad bonding strength and trapped oxide or Al2O3 particles retain in the matrix after blasting responsible for the initiation of fatigue cracks.展开更多
High nitrogen stainless steel(HNS) is a nickel free austenitic stainless steel that is used as a structural component in defence applications for manufacturing battle tanks as a replacement of the existing armour grad...High nitrogen stainless steel(HNS) is a nickel free austenitic stainless steel that is used as a structural component in defence applications for manufacturing battle tanks as a replacement of the existing armour grade steel owing to its low cost, excellent mechanical properties and better corrosion resistance.Conventional fusion welding causes problems like nitrogen desorption, solidification cracking in weld zone, liquation cracking in heat affected zone, nitrogen induced porosity and poor mechanical properties.The above problems can be overcome by proper selection and procedure of joining process. In the present work, an attempt has been made to correlate the microstructural changes with mechanical properties of fusion and solid state welds of high nitrogen steel. Shielded metal arc welding(SMAW), gas tungsten arc welding(GTAW), electron beam welding(EBW) and friction stir welding(FSW) processes were used in the present work. Optical microscopy, scanning electron microscopy and electron backscatter diffraction were used to characterize microstructural changes. Hardness, tensile and bend tests were performed to evaluate the mechanical properties of welds. The results of the present investigation established that fully austenitic dendritic structure was found in welds of SMAW. Reverted austenite pools in the martensite matrix in weld zone and unmixed zones near the fusion boundary were observed in GTA welds. Discontinuous ferrite network in austenite matrix was observed in electron beam welds.Fine recrystallized austenite grain structure was observed in the nugget zone of friction stir welds.Improved mechanical properties are obtained in friction stir welds when compared to fusion welds. This is attributed to the refined microstructure consisting of equiaxed and homogenous austenite grains.展开更多
The microstracture, mechanical and corrosion resistance properties of 445J2 ultra pure ferritic stainless steel thin plate joints conducted by the pulsed current gas tungsten arc welding (PCGTAW) were discussed in t...The microstracture, mechanical and corrosion resistance properties of 445J2 ultra pure ferritic stainless steel thin plate joints conducted by the pulsed current gas tungsten arc welding (PCGTAW) were discussed in this paper. In order to avoid weld defects, the appropriate welding process was adjusted. The joints were subjected to optical microscopy, transverse static tensile, plastic deformation, intergranular corrosion and electrochemistry corrosion tests. The results indicated that the weld zone (WZ) is characterized with columnar grains and equiaxed grains and the heat-affected zone (HAZ) shows coarse ferrite grains due to the rapid solidification of thin plate welding. The PCGTAW joint exhibited acceptable mechanical properties and equivalent corrosion resistance properties as the base metal.展开更多
The foaming slag practice can effectively solve the problems existing in EAF smelting of stainless steel, such as high electrical consumption ,high refractory consumption and long tap to tap time. In this paper, theor...The foaming slag practice can effectively solve the problems existing in EAF smelting of stainless steel, such as high electrical consumption ,high refractory consumption and long tap to tap time. In this paper, theoretical analyses were made on the technical difficulties and development feasibility of the technology. Slag foaming experiments were performed in a 10t EAF where crude stainless steel with a Cr content of 13% - 15% and a carbon content of 1.5% - 2.5% was smelted and special foaming pellets were added to release additional gas for better foaming. Good foaming slag was observed with the electric arc fully covered by the foam when the content of Cr2O3 is between 7% - 12%. The industrial scale experiments were performed in a 110 t EAF by the use of the same foaming pellets. Compared with the traditional operation, these experiments resulted in better foaming effects.展开更多
2205 duplex stainless steels ( DSSs) are welded in gas tungsten arc welding (GTAW) with the addition of N2 to argon, and the desirable microstructure and properties of the joints are obtained by altering the nitro...2205 duplex stainless steels ( DSSs) are welded in gas tungsten arc welding (GTAW) with the addition of N2 to argon, and the desirable microstructure and properties of the joints are obtained by altering the nitrogen percentage in the shielding gas mixture. The mechanical properties of joints are tested with tensile and microhardness machine, and the joint micrustructure is analyzed with scanning electron microscope (SEM) and optical microscope ( OM ) , and detrimental phase precipitate is investigated with X-ray diffraction (XRD), respectively. Finally, the corrosion behaviour of joint is also evaluated. Results show that the favorable joint strength and corrosion resistance can be obtained with appropriate shielding gas mixture in GTA W. No detrimental phase precipitates in the weldment, and the joint tensile fracture obviously presents the characteristic of ductile fracture.展开更多
This study reports a hybrid method which allows the formation of biocomposites on stainless steel implants. The main idea of the method is to create multilayer coatings consisting of titanium primer layer and a microa...This study reports a hybrid method which allows the formation of biocomposites on stainless steel implants. The main idea of the method is to create multilayer coatings consisting of titanium primer layer and a microarc calcium-phosphate coating. The titanium layer is deposited from plasma of continuous vacuum-arc discharge, and calcium-phosphate coating is formed by the microarc oxidation technique. The purpose of the hybrid method is to combine the properties of good strength stainless steel with high bioactivity of calcium-phosphate coating. This paper describes the chemical composition, morphology characteristics, adhesion and the ability of the formed biocomposites to stimulate the processes of osteoinduction. It is expedient to use such biocomposites for implants which carry heavy loads and are intended for long-term use, e.g. total knee endoprosthesis.展开更多
FSW and TIG were conducted on 316L stainless steel.Variation during microstructure and properties in joints obtained by different welding methods was studied.The results show that the effect of severe mechanical stirr...FSW and TIG were conducted on 316L stainless steel.Variation during microstructure and properties in joints obtained by different welding methods was studied.The results show that the effect of severe mechanical stirring and intense plastic deformation creat a fine recrystallized grain in the welding joint during FSW.As for TIG,the temperature of welding joint exceeds the melting point of welded material itself.The entire welding process belongs to the solidification of a small molten pool;and the microstructure of the joint takes on a typical casting structure.When the welding parameters were selected appropriately,the average ultimate tensile strength of FSW joints can reach 493 MPa,which is 83.6%of base metal;the average elongation is 52.1%of base metal.The average ultimate tensile strength of TIG joints is 475 MPa, which is 80.5%of base metal;the average elongation is 40.8%of base metal.The tensile test of FSW joints is superior to the TIG joints.The microhardness of FSW joint compared to base metal and TIG joint having a significant improvement,which arel95.5 HV,159.7 HV and 160.7 HV,respectively;grain refinement strengthening plays an important role in enhancing the microhardness.The electrochemical corrosion tests show that the joint of FSW 316L austenitic stainless steel has a good corrosion resistance.展开更多
基金financially supported by the Shanxi Provincial Key Programs for Science and Technology Development (No. 20100321084)Taiyuan Special Foundation for Excellent Talents (No. 20111075)
文摘The arc characteristics of submerged arc welding (SAW) with stainless steel wire were studied by using Analysator Hannover (AH). The tests were carded out under the same preset arc voltage combined with different welding currents. By comparing the probability density distribution (PDD) curves of arc voltage and welding current, the changes were analyzed, the metal transfer mode in SAW was deduced, and the characteristics of a stable arc were summarized. The analysis results show that, with an increase of welding parameters, the short-circuiting peak in the PDD curves of arc voltage decreases gradually until it disappears, and the dominant metal transfer mode changes from flux-wall guided transfer to projected transfer and then to streaming transfer. Moreover, when the PDD curves of arc voltage are both unimodal and generally symmetrical, the greater the peak probability and the smaller the peak span, the more stable the arc becomes.
基金the Thai Government scholarship given via Rajamangala University of Technology Krungthep (UTK), Bangkok, Thailand, for their financial support through this funded research project
文摘This present study applied gas tungsten arc welding in order to join AISI 304 and AISI 201 stainless steels.The objective was to find the optimum welding condition that gave a weld bead in accordance with DIN EN ISO 25817 quality level B, pitting corrosion potential of the weld metal of not less than that of the AISI304 base metal and a ratio of delta-ferrite in austenite matrix of the weld metal of not lower than 3%.Such a ratio is a criterion widely accepted to protect the weld metal from solidification cracking. At the welding current of 75 A and by using pure argon as a shielding gas 0 to 8 vol.% and applying a welding speed in the range of 2-3.5 mm·s^(-1) was found to give a complete weld bead with an increased depthper-width ratio(promote weldability). For welding speed in the range of 3 and 3.5 mm·s^(-1)(promote corrosion resistance). Increasing the welding speed in such a range decreased the amount of delta-ferrite in the austenite matrix, and increased the pitting corrosion potential of the weld metal to be 302 mV_(SCE).This value was still lower than the pitting corrosion potential of the AISI 304 base metal. Mixing nitrogen in argon shielding gas increased the nitrogen content in the weld. The optimum condition was found when using a welding speed of 3 mm· s^(-1) and mixing 1 vol.% of nitrogen in the argon shielding gas(promote weldability and corrosion resistance). Pitted areas after potentiodynamic test were observed in the austenite in which its Cr content was relatively low.
基金Project(50735006) supported by the National Natural Science Foundation of ChinaProject(2006BAF02A19) supported by the National Science and Technology Support Program of China
文摘A typical 321 stainless steel/aluminum composite coating (321/Al coating) was prepared by high velocity arc spraying technique (HVAS) with 321 stainless steel wire as the anode and aluminum wire as the cathode. The traditional 321 stainless steel coating was also prepared for comparison. Tribological properties of the coatings were evaluated with the ring-block wear tester under different conditions. The structure and worn surface of the coatings were analyzed by scanning electron microscopy(SEM), X-ray diffractometry(XRD) and energy dispersion spectroscopy(EDS). The results show that, except for aluminum phase addition in the 321/Al coating, no other phases are created compared with the 321 coating. However, due to the addition of aluminum, the 321/Al coating forms a type of "ductile/hard phases inter-deposited" structure and performs quite different tribological behavior. Under the dry sliding condition, the anti-wear property of 321/Al coating is about 42% lower than that of 321 coating. But under the oil lubricated conditions with or without 32 h oil-dipping pretreatment, the anti-wear property of 321/Al coating is about 9% and 5% higher than that of 321 coating, respectively. The anti-wear mechanism of the composite coating is mainly relevant to the decrease of oxide impurities and the strengthening action resulted from the "ductile/hard phases inter-deposited" coating structure.
文摘The present study is concerned with the effect of filler metals such as austenitic stainless steel, ferritic stainless steel and duplex stainless steel on tensile and impact properties of the ferritic stainless steel conforming to AISI 409M grade. Rolled plates of 4 mm thickness were used as the base material for preparing single pass butt welded joints. Tensile and impact properties, microhardness, microstructure and fracture surface morphology of the joints fabricated by austenitic stainless steel, ferritic stainless steel and duplex stainless steel filler metals were evaluated and the results were reported. From this investigation, it is found that the joints fabricated by duplex stainless steel filler metal showed higher tensile strength and hardness compared to the joints fabricated by austenitic and ferritic stainless steel filler metals. Joints fabricated by austenitic stainless steel filler metal exhibited higher ductility and impact toughness compared with the joints fabricated by ferritic stainless steel and duplex stainless steel filler metals.
文摘Double-sided arc welding with a single power source can effectively increase the weld penetration, diminish distortion, improve welding speed and save energy. Compared to conventional arc welding processes, double-sided arc welding can generate a penetrating electromaguetic field to help to form fine dendritic microstrueture in the weld due to the symmetry of heating. Type 1Cr1SNi9Ti aastenitic stainless steel was bead-on-plate welded with double-sided arc welding and conventional plasma arc welding processes, respectively, and microstructure in the weld, heat-affected zone and base metal were examined. After analyzing the black carbon-enriched band in the weld during plasma arc welding with electron probe microanalyzer ( EPMA ) and X-ray diffraction (XRD) technology, it was found that the black band was shaped from the aggregation of ferrite in the fasion boundary. Hardness measurement showed that this black band does not apparently affect the microhardncss distribution in the weld.
文摘AISI 304 stainless steel was ion implanted with Co, and the tribological property on the surface of the stainless steelwas investigated. The Co ion implantation was carried out using a metal vapor vacuum arc (Mevva) broad-beam ionsource with an extraction voltage of 40 kV, implantation doses of 3×10^(17)/cm^2 and 5×10^(17)/cm^2, and ion currentdensities of 13, 22 and 32μA/cm^2. The results showed that the near-surface hardness of Co-implanted stainless steelsample was increased by 50% or more, and it increased with increasing ion current density at first and then declined.The friction coefficient decreased from 0.74 to 0.20 after Co implantation. The wear rate after Co implantationreduced by 25% or more as compared to the unimplanted sample. The wear rate initially decreased with increasingion current density and then an increase was observed. Within the range of experimental parameters, there existsa critical ion current density for the Co-implanted stainless steel, at which the wear rate decreased with increasingretained dose, going through a minimum and then increased. The critical ion current density in this paper is about22μA/cm^2.
基金financially supported by the National Basic Research Program of China (973 Program) (no. 2012CB215500)the National Key Technology Research and Development Program of China (no. 2015BAG06B00)+1 种基金Major Program of the National Natural Science Foundation of China (no. 61433013)National Natural Science Foundation of China (no. 21206012)
文摘Arc ion plating (AIP) is applied to form Ti/(Ti,Cr)N/CrN multilayer coating on the surface of 316L stainless steel (SS316L) as bipolar plates for proton exchange membrane fuel cells (PEMFCs). The characterizations of the coating are analyzed by scanning electron microscopy (SEM) and X-ray diffraction (XRD). Interfacial contact resistance (ICR) between the coated sample and carbon paper is 4.9 m Omega cm(2) under 150 N/cm(2), which is much lower than that of the SS316L substrate. Potentiodynamic and potentiostatic tests are performed in the simulated PEMFC working conditions to investigate the corrosion behaviors of the coated sample. Superior anticorrosion performance is observed for the coated sample, whose corrosion current density is 0.12 mu A/cm(2). Surface morphology results after corrosion tests indicate that the substrate is well protected by the multilayer coating. Performances of the single cell with the multilayer coated SS316L bipolar plate are improved significantly compared with that of the cell with the uncoated SS316L bipolar plate, presenting a great potential for PEMFC application. (C) 2016 Science Press and Dalian Institute of Chemical Physics, Chinese Academy of Sciences. Published by Elsevier B.V. and Science Press. All rights reserved.
文摘The present work is aimed at studying the microstructure and pitting corrosion behaviour of shielded metal arc welded high nitrogen steel made of Cromang-N electrode. Basis for selecting this electrode is to increase the solubility of nitrogen in weld metal due to high chromium and manganese content. Microscopic studies were carried out using optical microscopy(OM) and field emission scanning electron microscopy(FESEM). Energy back scattered diffraction(EBSD) method was used to determine the phase analysis, grain size and orientation image mapping. Potentio-dynamic polarization testing was carried out to study the pitting corrosion resistance in aerated 3.5% NaCl environment using a GillAC electrochemical system. The investigation results showed that the selected Cr-Mn-N type electrode resulted in a maximum reduction in delta-ferrite and improvement in pitting corrosion resistance of the weld zone was attributed to the coarse austenite grains owing to the reduction in active sites of the austenite/delta ferrite interface and the decrease in galvanic interaction between austenite and delta-ferrite.
基金the National Natural Science Foundation of China(Grant No.51374111&51175185)Science and Technology Plan Project of Guangdong Province(Grant No.2015B050502005)for financial support
文摘To study the influence laws of welding parameters on weld porosity, underwater wet flux-cored arc welding ( FCAW) duplex stainless steel S32101 was carried out in a hyperbaric chamber, and the second-order multiple regression equation was established. The interactive effects of welding parameters on the porosity were analyzed by the three dimensional response surfaces and the contour plots. The results present that the interaction effect between water depth and voltage on the porosity is the most significant. Theoretically, a non-pores weld bead can be gained by reasonably matching these parameters with water depth less than 10 m. Always, the weld porosity reaches its peak value with a 7 mm/s welding speed.
文摘Pulsed current Micro Plasma Arc Welding is used to joint thin sheets of AISI 304L sheets, which are used in manufacturing of metallic bellows and diaphragms. In this article the effects of pulsing current parameters on weld pool geometry namely front width, back width, front height and back height of pulsed current micro plasma arc welded AISI 304L stainless steel sheets was analyzed. Four factors, five levels, central composite design was used to develop mathematical models, incorporating pulsed current parameters and weld pool geometry. The mathematical models have been developed by Response Surface Method. The adequacy of the models was checked by ANOVA technique. Variation of output responses with input process variables are discussed. By using the developed mathematical models, weld pool geometry parameters can be predicted.
文摘The 2205 duplex stainless + DH36 clad steel plate was welded by gas metal arc welding(GMAW), and the welding performance of the clad steel plate was investigated. The results show that the adaptability of the welding procedure for the base metal of carbon steel, the transition layer, and the cladding material is excellent. The test results indicate that the phase proportion and component dilution of the GMAW-welded joints of clad steel plate can be effectively controlled to yield joints with good mechanical properties and corrosion resistance.
基金the Department of Science and Technology (DST), Government of India for the financial support through Fast Track Scheme for Young Scientists R&D project (SR/FTP/ETA043/2009) to carry out this investigation
文摘An attempt is made to develop the tools that are capable enough to withstand the shear, impact and thermal forces that occur during friction stir welding of stainless steels. The atmospheric plasma spray and plasma transferred arc hardfacing processes are employed to deposit refractory ceramic based composite coatings on the Inconel 738 alloy. Five different combinations of self-fluxing alloy powder and 60% ceramic reinforcement particulate mixtures are used for coating. The best friction stir welding tool selected based on tool wear analysis is used to fabricate the austenitic stainless steel joints.
文摘The fatigue behaviors of 48MnV steel, both uncoated and coated with different thicknesses of 3Cr13 deposits using twin arc spraying, were investigated. The fatigue properties of the 48MnV steel, determined under axial loading conditions, can be substantially decreased by coating 3Cr13 films, deposited by twin arc spraying. And the fatigue behavior of the thinner coatings is better than that of the thicker ones, of which the fatigue limits decrease by 9%[CD*2]14%. The decrease in fatigue life attributes to the less mechanical properties of the coatings in comparison with those of the substrate, their relative bad bonding strength and trapped oxide or Al2O3 particles retain in the matrix after blasting responsible for the initiation of fatigue cracks.
文摘High nitrogen stainless steel(HNS) is a nickel free austenitic stainless steel that is used as a structural component in defence applications for manufacturing battle tanks as a replacement of the existing armour grade steel owing to its low cost, excellent mechanical properties and better corrosion resistance.Conventional fusion welding causes problems like nitrogen desorption, solidification cracking in weld zone, liquation cracking in heat affected zone, nitrogen induced porosity and poor mechanical properties.The above problems can be overcome by proper selection and procedure of joining process. In the present work, an attempt has been made to correlate the microstructural changes with mechanical properties of fusion and solid state welds of high nitrogen steel. Shielded metal arc welding(SMAW), gas tungsten arc welding(GTAW), electron beam welding(EBW) and friction stir welding(FSW) processes were used in the present work. Optical microscopy, scanning electron microscopy and electron backscatter diffraction were used to characterize microstructural changes. Hardness, tensile and bend tests were performed to evaluate the mechanical properties of welds. The results of the present investigation established that fully austenitic dendritic structure was found in welds of SMAW. Reverted austenite pools in the martensite matrix in weld zone and unmixed zones near the fusion boundary were observed in GTA welds. Discontinuous ferrite network in austenite matrix was observed in electron beam welds.Fine recrystallized austenite grain structure was observed in the nugget zone of friction stir welds.Improved mechanical properties are obtained in friction stir welds when compared to fusion welds. This is attributed to the refined microstructure consisting of equiaxed and homogenous austenite grains.
基金This work was supported by the Natural Science Foundation of Shanxi Province of China (2013021021-1), and the Graduate Innovation Project of Shanxi Province of China (20123031).
文摘The microstracture, mechanical and corrosion resistance properties of 445J2 ultra pure ferritic stainless steel thin plate joints conducted by the pulsed current gas tungsten arc welding (PCGTAW) were discussed in this paper. In order to avoid weld defects, the appropriate welding process was adjusted. The joints were subjected to optical microscopy, transverse static tensile, plastic deformation, intergranular corrosion and electrochemistry corrosion tests. The results indicated that the weld zone (WZ) is characterized with columnar grains and equiaxed grains and the heat-affected zone (HAZ) shows coarse ferrite grains due to the rapid solidification of thin plate welding. The PCGTAW joint exhibited acceptable mechanical properties and equivalent corrosion resistance properties as the base metal.
文摘The foaming slag practice can effectively solve the problems existing in EAF smelting of stainless steel, such as high electrical consumption ,high refractory consumption and long tap to tap time. In this paper, theoretical analyses were made on the technical difficulties and development feasibility of the technology. Slag foaming experiments were performed in a 10t EAF where crude stainless steel with a Cr content of 13% - 15% and a carbon content of 1.5% - 2.5% was smelted and special foaming pellets were added to release additional gas for better foaming. Good foaming slag was observed with the electric arc fully covered by the foam when the content of Cr2O3 is between 7% - 12%. The industrial scale experiments were performed in a 110 t EAF by the use of the same foaming pellets. Compared with the traditional operation, these experiments resulted in better foaming effects.
文摘2205 duplex stainless steels ( DSSs) are welded in gas tungsten arc welding (GTAW) with the addition of N2 to argon, and the desirable microstructure and properties of the joints are obtained by altering the nitrogen percentage in the shielding gas mixture. The mechanical properties of joints are tested with tensile and microhardness machine, and the joint micrustructure is analyzed with scanning electron microscope (SEM) and optical microscope ( OM ) , and detrimental phase precipitate is investigated with X-ray diffraction (XRD), respectively. Finally, the corrosion behaviour of joint is also evaluated. Results show that the favorable joint strength and corrosion resistance can be obtained with appropriate shielding gas mixture in GTA W. No detrimental phase precipitates in the weldment, and the joint tensile fracture obviously presents the characteristic of ductile fracture.
文摘This study reports a hybrid method which allows the formation of biocomposites on stainless steel implants. The main idea of the method is to create multilayer coatings consisting of titanium primer layer and a microarc calcium-phosphate coating. The titanium layer is deposited from plasma of continuous vacuum-arc discharge, and calcium-phosphate coating is formed by the microarc oxidation technique. The purpose of the hybrid method is to combine the properties of good strength stainless steel with high bioactivity of calcium-phosphate coating. This paper describes the chemical composition, morphology characteristics, adhesion and the ability of the formed biocomposites to stimulate the processes of osteoinduction. It is expedient to use such biocomposites for implants which carry heavy loads and are intended for long-term use, e.g. total knee endoprosthesis.
文摘FSW and TIG were conducted on 316L stainless steel.Variation during microstructure and properties in joints obtained by different welding methods was studied.The results show that the effect of severe mechanical stirring and intense plastic deformation creat a fine recrystallized grain in the welding joint during FSW.As for TIG,the temperature of welding joint exceeds the melting point of welded material itself.The entire welding process belongs to the solidification of a small molten pool;and the microstructure of the joint takes on a typical casting structure.When the welding parameters were selected appropriately,the average ultimate tensile strength of FSW joints can reach 493 MPa,which is 83.6%of base metal;the average elongation is 52.1%of base metal.The average ultimate tensile strength of TIG joints is 475 MPa, which is 80.5%of base metal;the average elongation is 40.8%of base metal.The tensile test of FSW joints is superior to the TIG joints.The microhardness of FSW joint compared to base metal and TIG joint having a significant improvement,which arel95.5 HV,159.7 HV and 160.7 HV,respectively;grain refinement strengthening plays an important role in enhancing the microhardness.The electrochemical corrosion tests show that the joint of FSW 316L austenitic stainless steel has a good corrosion resistance.