The wear resistances of austempered ductile iron （ADI） were improved through intxoduction of a new phase （carbide） into the ma- txix by addition of chromium. In the present investigation, low-caxbon-equivalent duc...The wear resistances of austempered ductile iron （ADI） were improved through intxoduction of a new phase （carbide） into the ma- txix by addition of chromium. In the present investigation, low-caxbon-equivalent ductile iron （LCEDI） （CE = 3.06%, and CE represents cax- bon-equivalent） with 2.42% chromium was selected. LCEDI was austeintized at two difl＇erent temperatures （900 and 975~C） a^ld soaked for 1 h and then quenched in a salt bath at 325~C for 0 to 10 h. Samples were analyzed using optical microscopy and X-ray diffraction. Wear tests were carded out on a pin-on-disk-type machine. The efl＇ect of austenization temperature on the wear resistance, impact strength, and the mi- crostructure was evaluated. A stxucture-property correlation based on the observations is established.展开更多
Measurements of dry sliding wear are presented for ductile irons with composition Fe-3.56C-2.67Si-0.25Mo-0.5Cu and Ni contents of 0.8 and 1.5 in wt.% with applied loads of 50, 100 and 150 N for austempering temperatur...Measurements of dry sliding wear are presented for ductile irons with composition Fe-3.56C-2.67Si-0.25Mo-0.5Cu and Ni contents of 0.8 and 1.5 in wt.% with applied loads of 50, 100 and 150 N for austempering temperatures of 270, 320, and 370 °C after austenitizing at 870 °C for 120 min. The mechanical property measurements show that the grades of the ASTM 897M: 1990 Standard can be satisfied for the selected austempering conditions. The results show that wear resistance is independent of austempering temperature with an applied load of 50 N, but there is a strong dependence at higher austempering temperatures with applied loads of 100 and 150 N. Observations indicate that wear is due to subsurface fatigue with cracks nucleated at deformed graphite nodules.展开更多
By continuous quenching process, the effect of austenitizing temperature and time on the structure and hardness of bainiteductile cast iron was studied. It was found that (l) low austenitizing temperature would result...By continuous quenching process, the effect of austenitizing temperature and time on the structure and hardness of bainiteductile cast iron was studied. It was found that (l) low austenitizing temperature would result in scrap ferrite existing in matrix, whichreduces the macro-hardness of bainite ductile cast iron; (2) high austenitizing temperature would make carbide decomposed, which alsoinduces the macro-hardness of bainite cast iron, and (3) austenitizing time has little effect on the structure of bainite ductile cast iron, butas it increases, the macro-hardness ofbainite ductile cast iron and micro-hardness of bainite increases. To the ductile cast iron, as a result,the suitable austenitizing temperature and time are recommended as 880 and 120 min respectively.展开更多
The effect of sub-zero cooling on microstructure and mechanical properties of a low alloyed austempered ductile iron has been investigated. Austempering of samples was performed at 325℃and 400℃after austenitizing at...The effect of sub-zero cooling on microstructure and mechanical properties of a low alloyed austempered ductile iron has been investigated. Austempering of samples was performed at 325℃and 400℃after austenitizing at 875℃and 950℃. The sub-zero treatments were carried out by cooling down the samples to -30℃, -70℃and -196℃. The changes in volume fraction of austenite and mechanical properties were determined after cooling to each temperature. The austenite volume fraction of samples which were austenitized at 875℃and austempered at 325℃remained unchanged, whilst it reduced in samples austenitized at 950℃and 875℃for austempering temperature of 400℃. In these specimens, some austenite transformed to martensite after subzero cooling. Mechanical property measurements showed a slight increase in strength and hardness and decrease in elongation and toughness due to this transformation behavior.展开更多
This study focused on the development of austempered ductile iron(ADI)with desirable combination of mechanical properties for crankshaft applications by the combined effect of vanadium(V)alloying and an optimized heat...This study focused on the development of austempered ductile iron(ADI)with desirable combination of mechanical properties for crankshaft applications by the combined effect of vanadium(V)alloying and an optimized heat treatment process.The produced unalloyed GGG60,0.15%V-alloyed GGG60(V-15),and 0.30%V-alloyed GGG60 samples were subjected to austenitizing at 900℃for 1 h and subsequent austempering processes at 250,300,and 350℃for 15,30,60,90,and 180 min.As a result of these austempering processes,different bainitic structures were obtained,which led to the formation of diverse combinations of mechanical properties.The mechanical properties of the austempered samples were tested comprehensively,and the results were correlated with their microstructures and the stability of the retained austenite phases.From the microstructural observations,the V-alloyed samples exhibited a finer microstructure and a more acicular ferrite phase than unalloyed samples.The V addition delayed the coarsening of the acicular ferrite structures and considerably contributed to the improvement of the mechanical properties of GGG60.Moreover,the X-ray diffraction results revealed that the retained austenite volume and the carbon enrichment of austenite phases in ADI samples were remarkably affected by the addition of vanadium.The increase in volume fraction of retained austenite and its carbon content provided favorable ductility and toughness to V-15,as confirmed by the elongation and impact test results.Consequently,the dual-phase ausferrite microstructure of V-15 that was austempered at 300℃for 60 min exhibited high strength with substantial ductility and toughness for crankshaft applications.展开更多
The equilibrium partition ratio, k, has been measured for Mn, Mo, Si, Ni and Cu in a ductile iron with composition(wt.%): 3.45 C, 0.25 Mn, 0.25 Mo, 2.45 Si, 0.5Ni and 0.5Cu with different nodule counts obtained from d...The equilibrium partition ratio, k, has been measured for Mn, Mo, Si, Ni and Cu in a ductile iron with composition(wt.%): 3.45 C, 0.25 Mn, 0.25 Mo, 2.45 Si, 0.5Ni and 0.5Cu with different nodule counts obtained from different section sizes of13, 25, 75 mm in the as cast, austenitized(at 870 °C for times 1, 4 and 6 hours) and austempered(at 375 °C for times 1 to 1,440 min) samples. Results show that Mn and Mo segregate positively at cell boundaries, but Si, Ni and Cu concentrate in an inverse manner in the vicinity ofgraphite nodules and there is a depletion ofthese elements at cell boundaries. Segregation curves for Ni and Cu are more smooth than for Si. Carbide formation has been observed at cell boundaries. Based on the results, the partition ratios for all elements decrease with increasing the nodule count. More carbide with coarser morphology has been observed in the microstructure with a lower nodule count. Austenitization for a longer time can decrease partition ratio, but cannot eliminate it entirely. Increasing the austenitization temperature has the same effect. Austenitizing parameters have no significant effect on carbides volume fraction. The kinetics ofaustempering is faster in higher nodule counts and subsequently better mechanical properties including higher ductility, strength and toughness have been observed for all austempering conditions studied.展开更多
In the present research, TTT curve of bainitic ductile iron under the condition of controlled cooling was generated. The cooling rate of grinding ball and its temperature distribution were also measured at the same ti...In the present research, TTT curve of bainitic ductile iron under the condition of controlled cooling was generated. The cooling rate of grinding ball and its temperature distribution were also measured at the same time. It can be concluded that the bainitic zone of TTT curve is separated from the pearlitic zone. As compared to the water-quenching condition, more even cooling rate and temperature distribution can be achieved in the controlled cooling process. The controlled cooling can keep away from pearlitic zone in the high temperature cooling stage and produce similar results to the process of traditional isothermal cooling with a low cooling rate in the low temperature cooling stage.展开更多
The effects of nickel （2.2 %） and molybdenum （0.6 % ） additions on the kinetics, microstrueture, and mechanical properties of ductile aluminum cast iron were studied under the as-cast and tempered conditions. Test...The effects of nickel （2.2 %） and molybdenum （0.6 % ） additions on the kinetics, microstrueture, and mechanical properties of ductile aluminum cast iron were studied under the as-cast and tempered conditions. Test bars machined from cast to size samples were used for mechanical and metallurgical studies. The results showed that adding nickel and molybdenum to the base iron produced an upper bainitic structure, resulting in an increase in strength and hardness. The same trend was shown when the test bars were tempered at 300 ℃in the range of 300 ℃ to 400 ℃. The elongation increased with increasing the temperature from 300 ℃ to 400 ℃. The carbon content of the retained austenite also increased with increasing the temperature. The results also showed that the kinetics, microstructure, and mechanical properties of this iron were similar to those of Ni-Mo alloyed silicon ductile iron.展开更多
文摘The wear resistances of austempered ductile iron （ADI） were improved through intxoduction of a new phase （carbide） into the ma- txix by addition of chromium. In the present investigation, low-caxbon-equivalent ductile iron （LCEDI） （CE = 3.06%, and CE represents cax- bon-equivalent） with 2.42% chromium was selected. LCEDI was austeintized at two difl＇erent temperatures （900 and 975~C） a^ld soaked for 1 h and then quenched in a salt bath at 325~C for 0 to 10 h. Samples were analyzed using optical microscopy and X-ray diffraction. Wear tests were carded out on a pin-on-disk-type machine. The efl＇ect of austenization temperature on the wear resistance, impact strength, and the mi- crostructure was evaluated. A stxucture-property correlation based on the observations is established.
基金the Sahand University of Technology for providing the research facilities and financial support
文摘Measurements of dry sliding wear are presented for ductile irons with composition Fe-3.56C-2.67Si-0.25Mo-0.5Cu and Ni contents of 0.8 and 1.5 in wt.% with applied loads of 50, 100 and 150 N for austempering temperatures of 270, 320, and 370 °C after austenitizing at 870 °C for 120 min. The mechanical property measurements show that the grades of the ASTM 897M: 1990 Standard can be satisfied for the selected austempering conditions. The results show that wear resistance is independent of austempering temperature with an applied load of 50 N, but there is a strong dependence at higher austempering temperatures with applied loads of 100 and 150 N. Observations indicate that wear is due to subsurface fatigue with cracks nucleated at deformed graphite nodules.
文摘By continuous quenching process, the effect of austenitizing temperature and time on the structure and hardness of bainiteductile cast iron was studied. It was found that (l) low austenitizing temperature would result in scrap ferrite existing in matrix, whichreduces the macro-hardness of bainite ductile cast iron; (2) high austenitizing temperature would make carbide decomposed, which alsoinduces the macro-hardness of bainite cast iron, and (3) austenitizing time has little effect on the structure of bainite ductile cast iron, butas it increases, the macro-hardness ofbainite ductile cast iron and micro-hardness of bainite increases. To the ductile cast iron, as a result,the suitable austenitizing temperature and time are recommended as 880 and 120 min respectively.
文摘The effect of sub-zero cooling on microstructure and mechanical properties of a low alloyed austempered ductile iron has been investigated. Austempering of samples was performed at 325℃and 400℃after austenitizing at 875℃and 950℃. The sub-zero treatments were carried out by cooling down the samples to -30℃, -70℃and -196℃. The changes in volume fraction of austenite and mechanical properties were determined after cooling to each temperature. The austenite volume fraction of samples which were austenitized at 875℃and austempered at 325℃remained unchanged, whilst it reduced in samples austenitized at 950℃and 875℃for austempering temperature of 400℃. In these specimens, some austenite transformed to martensite after subzero cooling. Mechanical property measurements showed a slight increase in strength and hardness and decrease in elongation and toughness due to this transformation behavior.
文摘This study focused on the development of austempered ductile iron(ADI)with desirable combination of mechanical properties for crankshaft applications by the combined effect of vanadium(V)alloying and an optimized heat treatment process.The produced unalloyed GGG60,0.15%V-alloyed GGG60(V-15),and 0.30%V-alloyed GGG60 samples were subjected to austenitizing at 900℃for 1 h and subsequent austempering processes at 250,300,and 350℃for 15,30,60,90,and 180 min.As a result of these austempering processes,different bainitic structures were obtained,which led to the formation of diverse combinations of mechanical properties.The mechanical properties of the austempered samples were tested comprehensively,and the results were correlated with their microstructures and the stability of the retained austenite phases.From the microstructural observations,the V-alloyed samples exhibited a finer microstructure and a more acicular ferrite phase than unalloyed samples.The V addition delayed the coarsening of the acicular ferrite structures and considerably contributed to the improvement of the mechanical properties of GGG60.Moreover,the X-ray diffraction results revealed that the retained austenite volume and the carbon enrichment of austenite phases in ADI samples were remarkably affected by the addition of vanadium.The increase in volume fraction of retained austenite and its carbon content provided favorable ductility and toughness to V-15,as confirmed by the elongation and impact test results.Consequently,the dual-phase ausferrite microstructure of V-15 that was austempered at 300℃for 60 min exhibited high strength with substantial ductility and toughness for crankshaft applications.
基金the Sahand University of Technology for providing the research facilities and financial support
文摘The equilibrium partition ratio, k, has been measured for Mn, Mo, Si, Ni and Cu in a ductile iron with composition(wt.%): 3.45 C, 0.25 Mn, 0.25 Mo, 2.45 Si, 0.5Ni and 0.5Cu with different nodule counts obtained from different section sizes of13, 25, 75 mm in the as cast, austenitized(at 870 °C for times 1, 4 and 6 hours) and austempered(at 375 °C for times 1 to 1,440 min) samples. Results show that Mn and Mo segregate positively at cell boundaries, but Si, Ni and Cu concentrate in an inverse manner in the vicinity ofgraphite nodules and there is a depletion ofthese elements at cell boundaries. Segregation curves for Ni and Cu are more smooth than for Si. Carbide formation has been observed at cell boundaries. Based on the results, the partition ratios for all elements decrease with increasing the nodule count. More carbide with coarser morphology has been observed in the microstructure with a lower nodule count. Austenitization for a longer time can decrease partition ratio, but cannot eliminate it entirely. Increasing the austenitization temperature has the same effect. Austenitizing parameters have no significant effect on carbides volume fraction. The kinetics ofaustempering is faster in higher nodule counts and subsequently better mechanical properties including higher ductility, strength and toughness have been observed for all austempering conditions studied.
文摘In the present research, TTT curve of bainitic ductile iron under the condition of controlled cooling was generated. The cooling rate of grinding ball and its temperature distribution were also measured at the same time. It can be concluded that the bainitic zone of TTT curve is separated from the pearlitic zone. As compared to the water-quenching condition, more even cooling rate and temperature distribution can be achieved in the controlled cooling process. The controlled cooling can keep away from pearlitic zone in the high temperature cooling stage and produce similar results to the process of traditional isothermal cooling with a low cooling rate in the low temperature cooling stage.
文摘The effects of nickel （2.2 %） and molybdenum （0.6 % ） additions on the kinetics, microstrueture, and mechanical properties of ductile aluminum cast iron were studied under the as-cast and tempered conditions. Test bars machined from cast to size samples were used for mechanical and metallurgical studies. The results showed that adding nickel and molybdenum to the base iron produced an upper bainitic structure, resulting in an increase in strength and hardness. The same trend was shown when the test bars were tempered at 300 ℃in the range of 300 ℃ to 400 ℃. The elongation increased with increasing the temperature from 300 ℃ to 400 ℃. The carbon content of the retained austenite also increased with increasing the temperature. The results also showed that the kinetics, microstructure, and mechanical properties of this iron were similar to those of Ni-Mo alloyed silicon ductile iron.
