A 3D temperature field reconstruction method using the colored background oriented schlieren(CBOS)method is proposed to address image blurring due to the different refractive index of the multi-wavelength light and si...A 3D temperature field reconstruction method using the colored background oriented schlieren(CBOS)method is proposed to address image blurring due to the different refractive index of the multi-wavelength light and significant errors produced when the traditional background oriented schlieren(BOS)method is applied to high-temperature gas.First,the traditional method is employed to reconstruct the non-uniform 3D temperature field.Second,the CBOS method is applied to correct the distortion.Then,by analyzing the correlation coefficient among different color points of the colored background pattern,the non-uniform temperature field is reconstructed much more accurately.Finally,the experimental results are verified by applying the Runge-Kutta ray-tracing method and the thermocouple contact measurement method.The maximum average temperature error of the CBOS-reconstructed temperature field is 12.92°C,compared with the thermocouples.Therefore,an accurate three-dimensional reconstruction of the temperature field can be achieved by the proposed method effectively.展开更多
For the measurement of X-ray energy spectrum with filter-fluorescer method,the high energy tail at the rearward of response function is the main source of background.There are,traditionally,two techniques for measurin...For the measurement of X-ray energy spectrum with filter-fluorescer method,the high energy tail at the rearward of response function is the main source of background.There are,traditionally,two techniques for measuring the background contributions:the same element Z for the fluorescer and filter,or the same element Z?1 for them.Using the formula of fluorescence intensity,and the elemental combinations of cobalt and iron,the backgrounds which the two techniques provide and the real one for measuring black-body radiation at equilibrium temperature of 7×106 K,were calculated.The results show that the Co-Co combination for the filter-fluorescer spectrometer can achieve better effect.A semi-quantitative analysis for the calculation results is discussed.展开更多
In the measurement of G with the angular acceleration method,the improved correlation method developed by Wu et al.（Wu W H,Tian Y,Luo J,Shao C G,Xu J H and Wang DH 2016 Rev.Sci.Instrum.87 094501） is used to accurate...In the measurement of G with the angular acceleration method,the improved correlation method developed by Wu et al.（Wu W H,Tian Y,Luo J,Shao C G,Xu J H and Wang DH 2016 Rev.Sci.Instrum.87 094501） is used to accurately estimate the amplitudes of the prominent harmonic components of the gravitational background signal with time-varying frequency.Except the quadratic slow drift,the angular frequency of the gravitational background signal also includes a cosine oscillation coming from the useful angular acceleration signal,which leads to a deviation from the estimated amplitude.We calculate the correction of the cosine oscillation to the amplitude estimation.The result shows that the corrections of the cosine oscillation to the amplitudes of the fundamental frequency and second harmonic components obtained by the improved correlation method are within respective errors.展开更多
A patented kinetic uricase method was evaluated for serum uric acid assay. Initial absorbance of the reaction mixture before uricase action (A0) was obtained by correcting the absorbance at 293 nm measured before the ...A patented kinetic uricase method was evaluated for serum uric acid assay. Initial absorbance of the reaction mixture before uricase action (A0) was obtained by correcting the absorbance at 293 nm measured before the addition of uricase solution, and background absorbance (Ab) was predicted by an integrated method. Uric acid concentration in reaction solution was calcu-lated from ?A, the difference between A0 and Ab, using the absorptivity preset for uric acid. This kinetic uricase method exhibited CV<4.3% and recovery of 100%. Lipids, bilirubin, hemoglobin, ascorbic acid, reduced glutathione and xanthine <0.32 mmol/L in serum had no significant effects. ?A linearly responded to 1.2 to 37.5 μmol/L uric acid in reaction solution containing 15 μl serum. The slope of linear response was consistent with the absorptivity preset for uric acid while the intercept was consistent with that for serum alone. Uric acid concentrations in clinic sera by different uricase methods positively correlated to each other. By Bland-Altman analysis, this kinetic uricase method accorded with that by quantifying the total change of UV absorbance on the completion of uricase reaction. These results demonstrated that this kinetic uricase method is reliable for serum uric acid assay with enhanced resistance to both xanthine and other common errors, wider range of linear response and much lower cost.展开更多
基金Supported by the National Natural Science Foundation of China(52005500)Foundation of Tianjin Educational Committee(2018KJ242)Basic Science-Research Funds of National University(3122019088)。
文摘A 3D temperature field reconstruction method using the colored background oriented schlieren(CBOS)method is proposed to address image blurring due to the different refractive index of the multi-wavelength light and significant errors produced when the traditional background oriented schlieren(BOS)method is applied to high-temperature gas.First,the traditional method is employed to reconstruct the non-uniform 3D temperature field.Second,the CBOS method is applied to correct the distortion.Then,by analyzing the correlation coefficient among different color points of the colored background pattern,the non-uniform temperature field is reconstructed much more accurately.Finally,the experimental results are verified by applying the Runge-Kutta ray-tracing method and the thermocouple contact measurement method.The maximum average temperature error of the CBOS-reconstructed temperature field is 12.92°C,compared with the thermocouples.Therefore,an accurate three-dimensional reconstruction of the temperature field can be achieved by the proposed method effectively.
文摘For the measurement of X-ray energy spectrum with filter-fluorescer method,the high energy tail at the rearward of response function is the main source of background.There are,traditionally,two techniques for measuring the background contributions:the same element Z for the fluorescer and filter,or the same element Z?1 for them.Using the formula of fluorescence intensity,and the elemental combinations of cobalt and iron,the backgrounds which the two techniques provide and the real one for measuring black-body radiation at equilibrium temperature of 7×106 K,were calculated.The results show that the Co-Co combination for the filter-fluorescer spectrometer can achieve better effect.A semi-quantitative analysis for the calculation results is discussed.
基金Project supported by the National Natural Science Foundation of China(Grant Nos.11575160,11175160,11275075,and 11511130011)
文摘In the measurement of G with the angular acceleration method,the improved correlation method developed by Wu et al.（Wu W H,Tian Y,Luo J,Shao C G,Xu J H and Wang DH 2016 Rev.Sci.Instrum.87 094501） is used to accurately estimate the amplitudes of the prominent harmonic components of the gravitational background signal with time-varying frequency.Except the quadratic slow drift,the angular frequency of the gravitational background signal also includes a cosine oscillation coming from the useful angular acceleration signal,which leads to a deviation from the estimated amplitude.We calculate the correction of the cosine oscillation to the amplitude estimation.The result shows that the corrections of the cosine oscillation to the amplitudes of the fundamental frequency and second harmonic components obtained by the improved correlation method are within respective errors.
基金Project (No. 30200266) supported by the National Natural Science Foundation of China
文摘A patented kinetic uricase method was evaluated for serum uric acid assay. Initial absorbance of the reaction mixture before uricase action (A0) was obtained by correcting the absorbance at 293 nm measured before the addition of uricase solution, and background absorbance (Ab) was predicted by an integrated method. Uric acid concentration in reaction solution was calcu-lated from ?A, the difference between A0 and Ab, using the absorptivity preset for uric acid. This kinetic uricase method exhibited CV<4.3% and recovery of 100%. Lipids, bilirubin, hemoglobin, ascorbic acid, reduced glutathione and xanthine <0.32 mmol/L in serum had no significant effects. ?A linearly responded to 1.2 to 37.5 μmol/L uric acid in reaction solution containing 15 μl serum. The slope of linear response was consistent with the absorptivity preset for uric acid while the intercept was consistent with that for serum alone. Uric acid concentrations in clinic sera by different uricase methods positively correlated to each other. By Bland-Altman analysis, this kinetic uricase method accorded with that by quantifying the total change of UV absorbance on the completion of uricase reaction. These results demonstrated that this kinetic uricase method is reliable for serum uric acid assay with enhanced resistance to both xanthine and other common errors, wider range of linear response and much lower cost.
