A new approach for fabricating B4C/Cu graded composite by rapid self-resistance sintering under ultra-high pressure was presented, by which a near dense B4C/Cu graded composite with a compositional spectrum of 0-100% ...A new approach for fabricating B4C/Cu graded composite by rapid self-resistance sintering under ultra-high pressure was presented, by which a near dense B4C/Cu graded composite with a compositional spectrum of 0-100% was successfully fabricated. Plasma relevant performances of sintered B4C/Cu composite were preliminarily characterized, it is found that its chemical sputtering yield is 70% lower than that of SMF800 nuclear graphite under 2.7keV D+ irradiation, and almost no damages after 66 shots of in situ plasma discharge in HL-1 Tokamak facility, which indicates B4C/Cu plasma facing component has a good physical and chemical sputtering resistance performance compared with nuclear graphite.展开更多
Background:The simplest and most convenient food technology is the using of dry composite mixtures.They have a lot of advantages.Dry composite mixtures,which would completely be the basis for the production of persona...Background:The simplest and most convenient food technology is the using of dry composite mixtures.They have a lot of advantages.Dry composite mixtures,which would completely be the basis for the production of personalized food concentrates,are not represented.The development of such dry composite mixtures is actual and of scientific and practical interest.The purpose of this research is the selection and justification of local import-substituting raw materials components for dry composite mixtures used as the basis for the production of food concentrates.As the objects of research,the raw materials components of the starch,fruit and vegetable,industry were selected.The work uses currently accepted standard research methods for organoleptic and physic-chemical parameters of raw materials components.The research was carried out within of the project“Theoretical Substantiation of Production Technology and the Development of Import-Substituting Food Products of Functional Purpose Based on Dry Composite Mixtures”,funded by the Belarusian Republican Foundation for Basic Research.Based on the researches,it was found out that in the composition of dry composite mixtures for the production of food concentrates it is expedient to use the following raw materials:potato starch,extruded corn starch,dried carrots,dried beets,dried topinambur and dried apples in chopped form.展开更多
Due to the fact that the existing web service description methods cannot address the issue of service reuse of various levels of granularity, the concept of service component is introduced, which packages together web...Due to the fact that the existing web service description methods cannot address the issue of service reuse of various levels of granularity, the concept of service component is introduced, which packages together web services and choreography, and their operations and properties are presented in a consistent and uniform manner. Service components are published externally as normal web services and can thus be employed by webbased applications. In order to improve reusability and testability of service components, the concept of composition pattern is also proposed, which presents the relationships among service components. The relationships and relationship compositions have a rigorous semantic, so that composite components can be validated at the configuration stage. The composition patterns support to integrate service components of various levels of granularity. Experience indicates that the application assembly can effectively be conducted by understanding, selecting, and reusing components easily.展开更多
To determine the chemical composition of Galla chinensisextract (GCE) by several analysis techniques and to compare the efficacy of GCE and its main component(s) in inhibition of enamel demineralization, for the d...To determine the chemical composition of Galla chinensisextract (GCE) by several analysis techniques and to compare the efficacy of GCE and its main component(s) in inhibition of enamel demineralization, for the development of future anticaries agents, main organic composition of GCE was qualitatively determined by liquid chromatography-time of flight-mass spectrometry (LC-TOF-MS) and quantified by high-performance liquid chromatography-diode array detector (HPLC-DAD). Inorganic ions were tested by inductively coupled plasma-atomic emission spectroscopy and F was especially measured by ion chromatography. Then, bovine enamel blocks were randomly divided into four treatment groups and were subjected to a pH-cycling regime for 12 times. Each cycle included 5-min applications with one of four treatments: 4g.L-1 GCE solution, 4g.L-1 gallic acid (GA) solution, I g.L-1 NaF solution (positive control), deionized water (DDW, negative control), and then 60-min application in pH 5.0 acidic buffer and 5-min application in neutral buffer. Acidic buffers were retained for calcium analysis. The main organic composition of GCE were GA and its isomer, and, to a lesser extent, small molecule gallotannins. The content of GA in GCE was 71.3%±0.2% (w/w). Inorganic ions were present in various amounts, of which Ca was (136±2.82) μg.g-1, and Zn was (6.8±0.1) μg.g-1. No F was detected in GCE. in pH cycling, GA showed an effect similar to GCE in inhibiting enamel demineralization (P〉0.05). GA was found to be the main effective, demineralization inhibiting component of GCE and could be a promising agent for the development of anticaries agents.展开更多
After describing the characteristics of programming paradigm, this paper introduces the approach of code component composition reuse in detail, proposes and discusses viewpoint that code component composition reuse is...After describing the characteristics of programming paradigm, this paper introduces the approach of code component composition reuse in detail, proposes and discusses viewpoint that code component composition reuse is a kind of new programming paradigm. This paper also specifies the characteristics of this new programming paradigm in detail, and points out some issues that must be resolved for using this new programming paradigm.展开更多
Natural wax gelators have different compositions of compounds(hydrocarbons,wax esters,free fatty alcohols,and free fatty acids),which results in oleogels with varying properties.To maintain a consistent composition,th...Natural wax gelators have different compositions of compounds(hydrocarbons,wax esters,free fatty alcohols,and free fatty acids),which results in oleogels with varying properties.To maintain a consistent composition,the individual components can be added to the original wax gelator.The content of hydrocarbons and wax esters greatly affects the structuring process of liquid edible oils with waxes.The aim of this study was to evaluate the possibility of modifying the properties of beeswax as a gelling agent by adding hydrocarbons or monoesters to obtain oleogels with specific properties.Various tests were conducted to assess the changes in the oleogel properties,such as color,microstructure,oil-binding capacity,thermal and textural properties.The research results have shown that the addition of the studied fractions has led to a significant change in all properties of oleogels.The initial size of oleogel crystals(7.29±1.80μm)changed after adding fractions,varying from 5.28μm to 12.58μm with hydrocarbons and from 9.95μm to 30.41μm with wax esters.The addition of 30%–50% hydrocarbons decreased the ability of the oleogels to bind oil and made them less firm compared to samples with 10%-20% hydrocarbons.Adding 10%-20% monoesters increased the firmness of the oleogels,but this indicator decreased when their content was increased to 50%.The obtained data indicate that hydrocarbons and wax esters can be used for targeted correction of the gelling properties of beeswax.展开更多
A system of finished Componeer composite veneers is a unique and having no analogy in the world elaboration of the Swisscompany Coltene/Whaledent, an outcome of almost halfa century experience of the company working i...A system of finished Componeer composite veneers is a unique and having no analogy in the world elaboration of the Swisscompany Coltene/Whaledent, an outcome of almost halfa century experience of the company working in a field of composite materials.It combines the best features of direct and indirect restoration methods. The system is fulfilled of nanocomposite Synergy D6 that hashigh mechanical strength, convenience for workable consistency, color stability and a system of halftone shades, which facilitates colormatching. All this allows achieving excellent aesthetic results in minimal time. Application of an original standard scale givespossibility effectively assess optical properties of dental hard tissues and develop an implementation strategy of restoration before workstarted. Formation of Componeer form, polymerization and polishing at factory allow a practitioner fully utilize effect of"fluorescence" inherent to the material. All this allows us to position the Componeer system as a serious alternative to non-directmethods of restoration with the possibility of both high aesthetic and cosmetic reconstruction reliability.展开更多
Inductively coupled plasma optical emission spectrometric approach(1CP-OES) is used to determine the potassium content as principal component in pyrotechnic compositions used for fireworks and firecrackers. Element ...Inductively coupled plasma optical emission spectrometric approach(1CP-OES) is used to determine the potassium content as principal component in pyrotechnic compositions used for fireworks and firecrackers. Element of potassium is conunonly found in potassium nitrate and potassium perchlorate in pyrotechnic compositions in fireworks and firecrackers. Statistical analysis shows that potassium nitrate content in pyrotechnics is between 10% to 60% and the potassium perchlorate content is between 20% to 70%,which counted in the content of potassium element is between 4% to 23%. Concept of this method: considering the weight of the sample is 400rag,constant volume is 1L and the concentration of potassium is between 10 mg/L to 90 mg/L in sample solution, the determination scope of the method for the potassium content would be between 1% to 23%.Further experiments proved that the fitting correlation coefficient of potassium calibration curve is 0.9997 or higher, recovery is 89.15%-100.23%.The allowable differential value is 0.4% between two single tests under repeatable conditions. This method can completely satisfy the requirements of the fireworks and firecrackers industry with high accuracy and good precision.展开更多
Inductively coupled plasma optical emission spectrometric approach(ICP-OES)is used to determine the magnesium and aluminum content as principal components in pyrotechnic compositions used for fireworks and firecrack...Inductively coupled plasma optical emission spectrometric approach(ICP-OES)is used to determine the magnesium and aluminum content as principal components in pyrotechnic compositions used for fireworks and firecrackers. Elements of magnesium and aluminum are commonly found in aluminum powder or magnesium-aluminum alloy powder in pyrotechnic compositions in fireworks and firecrackers. Statistical analysis shows that the magnesium content in pyrotechnics is between 8% to 30% and the aluminum content is between 8% to 35%(roughly).Concept of this method: suppose the weight of the sample is 400rag,constant volume is IL and the concentlation of magnesium and aluminum is between 12mg/L to 160mg/L in sample solution, the determination scope of the method for magnesium and aluminum content would be between 3% to 40%.Further experiments proved that the fitting correlation coefficient of the magnesium calibration curve is 0.9999 or higher, recovery is 101.01% -101.96%.The fitting correlation coefficient of the aluminum calibration curve is 0.9999 or higher, recovery is 99.36%-103.07%. The allowable differential value is 0.4% between two single tests under repeatable conditions. This method can completely satisfy the requirements of the fireworks and firecrackers industry with high accuracy and good precision.展开更多
The sensitivity of aerosol radiative properties (i.e., scattering coefficient, extinction coefficient, single scatter albedo, and asymmetry factor) and radiation transmission to aerosol composition, size distributions...The sensitivity of aerosol radiative properties (i.e., scattering coefficient, extinction coefficient, single scatter albedo, and asymmetry factor) and radiation transmission to aerosol composition, size distributions, and relative humidity (RH) is examined in this paper. Mie calculations and radiation calculations using a tropospheric visible radiation model are performed. The aerosol systems considered include inorganic and organic ions (e.g., Cl-, Br-, , , Na+, , K+, Ca2+, Mg2+, HCOO-, CH3COO-, CH3CH2COO-, CH3COCOO-, OOCCOO2-, MSA1-), and (2) water-insoluble inorganic and organic compounds e.g., (black carbon, n-alkanes, SiO2, Al2O3, Fe2O3 and other organic compounds). The partial molar refraction method and the volume-average method are used to calculate the real and imaginary parts of refractive index of real aerosols, respectively. The sensitivity simulations show that extinction coefficient increases by 70% when RH varies from 0 to 80%. Both extinction coefficient and asymmetry factor increase by ~48% when real part varies from 1.40 to 1.65. Scattering coefficient and single scattering albedo decrease by 18% and 24%, respectively, when the imaginary part varies from –0.005 to –0.1. Scattering and extinction coefficients increase by factors of 118 and 123, respectively, when the geometric mean radius varies from 0.05 to 0.3 ?m. Scattering and extinction coefficients and asymmetry factor increase by factors of 389, 334, and 5.4, respectively, when geometric standard deviation varies from 1.2 to 3.0. The sensitivity simulations using a tropospheric visible radiation model show that the radiation transmission is very sensitive to the change in geometric mean radius and standard deviation;other factors are insignificant.展开更多
An engine rubber mounting is one of the important parts of a vehicle. It is a function to isolate or absorb and to reduce vibration to the vehicle body thus to the passenger itself. Due to the engine compartments envi...An engine rubber mounting is one of the important parts of a vehicle. It is a function to isolate or absorb and to reduce vibration to the vehicle body thus to the passenger itself. Due to the engine compartments environment such as heat and massive vibration due to road conditions, the engine rubber mountings lifespan has been reduced. Thus several studies have been conducted to upgrade the material lifespan to make it more reliable and better engine mounting components. This paper presents the conceptual design of kenaf fiber polymer as automotive engine rubber mounting composites using the integration of Theory of Inventive Problem Solving(TRIZ). In this early stage, the solution is generated using 40 inventive principles and TRIZ contradiction method. The solution parameter for the specific design character is the selected using the morphological chart to develop a systematic conceptual design for the component. Four(4) innovative design concepts were produced and Analytic Network Process(ANP)methods were utilized to perform the multi-criteria decision-making process of selecting the best concept design for the polymer composite engine rubber mounting component.展开更多
An automatic brush-plating system was developed for component remanufacturing. With this system, Ni/nano-alumina composite coatings from an electrolyte containing 20g/L nano-alumina particles were prepared. Microstr...An automatic brush-plating system was developed for component remanufacturing. With this system, Ni/nano-alumina composite coatings from an electrolyte containing 20g/L nano-alumina particles were prepared. Microstructure, surface morphology, microhardness and wear resistance of automatically plated coatings and manually plated coatings were investigated comparatively. The results show that the automatically plated coatings are relatively dense and uniform and have lower friction coefficient of 0.089 under lubricant condition, when compared with manually plated coatings with friction coefficient of 0.14.展开更多
IntelligentPad approach provides a standard for dynamically linkable components. Based on the standard, this paper introduces an approach of developing dynamically linkable components by using object oriented techniques.
Hydrogen absorption composite powder of Mg incorporated with Ni and CrCl3 (88∶10∶2 in mass ratio) was prepared by reactive milling in hydrogen atmosphere. Hydriding/dehydriding performances were measured by self-m...Hydrogen absorption composite powder of Mg incorporated with Ni and CrCl3 (88∶10∶2 in mass ratio) was prepared by reactive milling in hydrogen atmosphere. Hydriding/dehydriding performances were measured by self-made apparatus. The results show that reactive milling and multi-component addition of Ni and CrCl3 reduce the stability of hydride and improve the sorption performance of Mg-based materials. With powder milled for 60h, hydriding basically completes within 300s (250℃, 2.0MPa) and phase transformation fraction reaches 0.78. The phase transformation rate of hydriding/dehydriding progress increases significantly with the reduced particles size of powder while good kinetics of dehydriding at a relatively low temperature is gained with small grain size of hydride. Rapid temperature variations in a short span of time resulted from remarkable calorific effects of rapid phase transformation are detected in hydriding/dehydriding progress. The results of thermogravimetric and differential scanning calorimetric(TG/DSC) indicate that the onset temperature of desorption of composite milled for 100h is 272℃.展开更多
A novel La-Co-O-C (LC-C) composites were prepared via a facile co-hydrothermal route with oxides and glycerol and further optimized for methane catalytic activity and thermal stability via component regulation.It was ...A novel La-Co-O-C (LC-C) composites were prepared via a facile co-hydrothermal route with oxides and glycerol and further optimized for methane catalytic activity and thermal stability via component regulation.It was demonstrated that Co3O_(4)phase was the main component in regulation.The combined results of X-ray photoelectron spectroscopy (XPS),temperature-programmed desorption of oxygen (O_(2)-TPD),temperature-programmed reduction of hydrogen (H_(2)-TPR),temperature-programmed desorption of ammonia/carbon dioxide (NH_(3)/CO_(2)-TPD) revealed that component regulation led to more oxygen vacancies and exposure of surface Co_(2)+,lower surface basicity and optimized acidity,which were beneficial for adsorption of active oxygen species and activation of methane molecules,resulting in the excellent catalytic oxidation performance.Especially,the (3.5)LC-C (3.5 is Co-to-La molar ratio) showed the optimum activity and the T50and T90(the temperature at which the CH_(4)conversion rate was 50%and 90%,respectively) were 318 and 367℃,respectively.Using theoretical calculations and in situ diffuse reflection infrared Fourier transform spectroscopy characterization,it was also found that the catalytic mechanism changes from the “Rideal-Eley” mechanism to the “Two-term” mechanism depending on the temperature windows in which the reaction takes place.Besides,the use of the “Flynn-Wall-Ozawa” model in thermoanalytical kinetics revealed that component regulation simultaneously optimized the decomposition activation energy,further expanding the application scope of carboncontaining composites.展开更多
SUMMARY In many statistical applications,composite variables are constructed to reduce the number of variables and improve the performances of statistical analyses of these variables,especially when some of the variab...SUMMARY In many statistical applications,composite variables are constructed to reduce the number of variables and improve the performances of statistical analyses of these variables,especially when some of the variables are highly correlated.Principal component analysis(PCA)and factor analysis(FA)are generally used for such purposes.If the variables are used as explanatory or independent variables in linear regression analysis,partial least squares(PLS)regression is a better alternative.Unlike PCA and FA,PLS creates composite variables by also taking into account the response,or dependent variable,so that they have higher correlations with the response than composites from their PCA and FA counterparts.In this report,we provide an introduction to this useful approach and illustrate it with data from a real study.展开更多
One important application of independent component analysis (ICA) is in image processing. A two dimensional (2-D) composite ICA algorithm framework for 2-D image independent component analysis (2-D ICA) is propo...One important application of independent component analysis (ICA) is in image processing. A two dimensional (2-D) composite ICA algorithm framework for 2-D image independent component analysis (2-D ICA) is proposed. The 2-D nature of the algorithm provides it an advantage of circumventing the roundabout transforming procedures between two dimensional (2-D) image deta and one-dimensional (l-D) signal. Moreover the combination of the Newton (fixed-point algorithm) and natural gradient algorithms in this composite algorithm increases its efficiency and robustness. The convincing results of a successful example in functional magnetic resonance imaging (fMRI) show the potential application of composite 2-D ICA in the brain activity detection.展开更多
基金This work was financially supported by "863 " key foundation of China (No. 715-011-0230).
文摘A new approach for fabricating B4C/Cu graded composite by rapid self-resistance sintering under ultra-high pressure was presented, by which a near dense B4C/Cu graded composite with a compositional spectrum of 0-100% was successfully fabricated. Plasma relevant performances of sintered B4C/Cu composite were preliminarily characterized, it is found that its chemical sputtering yield is 70% lower than that of SMF800 nuclear graphite under 2.7keV D+ irradiation, and almost no damages after 66 shots of in situ plasma discharge in HL-1 Tokamak facility, which indicates B4C/Cu plasma facing component has a good physical and chemical sputtering resistance performance compared with nuclear graphite.
文摘Background:The simplest and most convenient food technology is the using of dry composite mixtures.They have a lot of advantages.Dry composite mixtures,which would completely be the basis for the production of personalized food concentrates,are not represented.The development of such dry composite mixtures is actual and of scientific and practical interest.The purpose of this research is the selection and justification of local import-substituting raw materials components for dry composite mixtures used as the basis for the production of food concentrates.As the objects of research,the raw materials components of the starch,fruit and vegetable,industry were selected.The work uses currently accepted standard research methods for organoleptic and physic-chemical parameters of raw materials components.The research was carried out within of the project“Theoretical Substantiation of Production Technology and the Development of Import-Substituting Food Products of Functional Purpose Based on Dry Composite Mixtures”,funded by the Belarusian Republican Foundation for Basic Research.Based on the researches,it was found out that in the composition of dry composite mixtures for the production of food concentrates it is expedient to use the following raw materials:potato starch,extruded corn starch,dried carrots,dried beets,dried topinambur and dried apples in chopped form.
基金The National Basic Research Program of China (973Program) (No.1999032710).
文摘Due to the fact that the existing web service description methods cannot address the issue of service reuse of various levels of granularity, the concept of service component is introduced, which packages together web services and choreography, and their operations and properties are presented in a consistent and uniform manner. Service components are published externally as normal web services and can thus be employed by webbased applications. In order to improve reusability and testability of service components, the concept of composition pattern is also proposed, which presents the relationships among service components. The relationships and relationship compositions have a rigorous semantic, so that composite components can be validated at the configuration stage. The composition patterns support to integrate service components of various levels of granularity. Experience indicates that the application assembly can effectively be conducted by understanding, selecting, and reusing components easily.
基金supported by the National Natural Science Foundation of China (grant nos. 30572409 and 30430800)Youth Foundation of Sichuan Province in China (grant no. 07ZQ026-020)
文摘To determine the chemical composition of Galla chinensisextract (GCE) by several analysis techniques and to compare the efficacy of GCE and its main component(s) in inhibition of enamel demineralization, for the development of future anticaries agents, main organic composition of GCE was qualitatively determined by liquid chromatography-time of flight-mass spectrometry (LC-TOF-MS) and quantified by high-performance liquid chromatography-diode array detector (HPLC-DAD). Inorganic ions were tested by inductively coupled plasma-atomic emission spectroscopy and F was especially measured by ion chromatography. Then, bovine enamel blocks were randomly divided into four treatment groups and were subjected to a pH-cycling regime for 12 times. Each cycle included 5-min applications with one of four treatments: 4g.L-1 GCE solution, 4g.L-1 gallic acid (GA) solution, I g.L-1 NaF solution (positive control), deionized water (DDW, negative control), and then 60-min application in pH 5.0 acidic buffer and 5-min application in neutral buffer. Acidic buffers were retained for calcium analysis. The main organic composition of GCE were GA and its isomer, and, to a lesser extent, small molecule gallotannins. The content of GA in GCE was 71.3%±0.2% (w/w). Inorganic ions were present in various amounts, of which Ca was (136±2.82) μg.g-1, and Zn was (6.8±0.1) μg.g-1. No F was detected in GCE. in pH cycling, GA showed an effect similar to GCE in inhibiting enamel demineralization (P〉0.05). GA was found to be the main effective, demineralization inhibiting component of GCE and could be a promising agent for the development of anticaries agents.
文摘After describing the characteristics of programming paradigm, this paper introduces the approach of code component composition reuse in detail, proposes and discusses viewpoint that code component composition reuse is a kind of new programming paradigm. This paper also specifies the characteristics of this new programming paradigm in detail, and points out some issues that must be resolved for using this new programming paradigm.
基金supported by the Russian Science Foundation under grant(Project No.19-16-00113).
文摘Natural wax gelators have different compositions of compounds(hydrocarbons,wax esters,free fatty alcohols,and free fatty acids),which results in oleogels with varying properties.To maintain a consistent composition,the individual components can be added to the original wax gelator.The content of hydrocarbons and wax esters greatly affects the structuring process of liquid edible oils with waxes.The aim of this study was to evaluate the possibility of modifying the properties of beeswax as a gelling agent by adding hydrocarbons or monoesters to obtain oleogels with specific properties.Various tests were conducted to assess the changes in the oleogel properties,such as color,microstructure,oil-binding capacity,thermal and textural properties.The research results have shown that the addition of the studied fractions has led to a significant change in all properties of oleogels.The initial size of oleogel crystals(7.29±1.80μm)changed after adding fractions,varying from 5.28μm to 12.58μm with hydrocarbons and from 9.95μm to 30.41μm with wax esters.The addition of 30%–50% hydrocarbons decreased the ability of the oleogels to bind oil and made them less firm compared to samples with 10%-20% hydrocarbons.Adding 10%-20% monoesters increased the firmness of the oleogels,but this indicator decreased when their content was increased to 50%.The obtained data indicate that hydrocarbons and wax esters can be used for targeted correction of the gelling properties of beeswax.
文摘A system of finished Componeer composite veneers is a unique and having no analogy in the world elaboration of the Swisscompany Coltene/Whaledent, an outcome of almost halfa century experience of the company working in a field of composite materials.It combines the best features of direct and indirect restoration methods. The system is fulfilled of nanocomposite Synergy D6 that hashigh mechanical strength, convenience for workable consistency, color stability and a system of halftone shades, which facilitates colormatching. All this allows achieving excellent aesthetic results in minimal time. Application of an original standard scale givespossibility effectively assess optical properties of dental hard tissues and develop an implementation strategy of restoration before workstarted. Formation of Componeer form, polymerization and polishing at factory allow a practitioner fully utilize effect of"fluorescence" inherent to the material. All this allows us to position the Componeer system as a serious alternative to non-directmethods of restoration with the possibility of both high aesthetic and cosmetic reconstruction reliability.
文摘Inductively coupled plasma optical emission spectrometric approach(1CP-OES) is used to determine the potassium content as principal component in pyrotechnic compositions used for fireworks and firecrackers. Element of potassium is conunonly found in potassium nitrate and potassium perchlorate in pyrotechnic compositions in fireworks and firecrackers. Statistical analysis shows that potassium nitrate content in pyrotechnics is between 10% to 60% and the potassium perchlorate content is between 20% to 70%,which counted in the content of potassium element is between 4% to 23%. Concept of this method: considering the weight of the sample is 400rag,constant volume is 1L and the concentration of potassium is between 10 mg/L to 90 mg/L in sample solution, the determination scope of the method for the potassium content would be between 1% to 23%.Further experiments proved that the fitting correlation coefficient of potassium calibration curve is 0.9997 or higher, recovery is 89.15%-100.23%.The allowable differential value is 0.4% between two single tests under repeatable conditions. This method can completely satisfy the requirements of the fireworks and firecrackers industry with high accuracy and good precision.
文摘Inductively coupled plasma optical emission spectrometric approach(ICP-OES)is used to determine the magnesium and aluminum content as principal components in pyrotechnic compositions used for fireworks and firecrackers. Elements of magnesium and aluminum are commonly found in aluminum powder or magnesium-aluminum alloy powder in pyrotechnic compositions in fireworks and firecrackers. Statistical analysis shows that the magnesium content in pyrotechnics is between 8% to 30% and the aluminum content is between 8% to 35%(roughly).Concept of this method: suppose the weight of the sample is 400rag,constant volume is IL and the concentlation of magnesium and aluminum is between 12mg/L to 160mg/L in sample solution, the determination scope of the method for magnesium and aluminum content would be between 3% to 40%.Further experiments proved that the fitting correlation coefficient of the magnesium calibration curve is 0.9999 or higher, recovery is 101.01% -101.96%.The fitting correlation coefficient of the aluminum calibration curve is 0.9999 or higher, recovery is 99.36%-103.07%. The allowable differential value is 0.4% between two single tests under repeatable conditions. This method can completely satisfy the requirements of the fireworks and firecrackers industry with high accuracy and good precision.
文摘The sensitivity of aerosol radiative properties (i.e., scattering coefficient, extinction coefficient, single scatter albedo, and asymmetry factor) and radiation transmission to aerosol composition, size distributions, and relative humidity (RH) is examined in this paper. Mie calculations and radiation calculations using a tropospheric visible radiation model are performed. The aerosol systems considered include inorganic and organic ions (e.g., Cl-, Br-, , , Na+, , K+, Ca2+, Mg2+, HCOO-, CH3COO-, CH3CH2COO-, CH3COCOO-, OOCCOO2-, MSA1-), and (2) water-insoluble inorganic and organic compounds e.g., (black carbon, n-alkanes, SiO2, Al2O3, Fe2O3 and other organic compounds). The partial molar refraction method and the volume-average method are used to calculate the real and imaginary parts of refractive index of real aerosols, respectively. The sensitivity simulations show that extinction coefficient increases by 70% when RH varies from 0 to 80%. Both extinction coefficient and asymmetry factor increase by ~48% when real part varies from 1.40 to 1.65. Scattering coefficient and single scattering albedo decrease by 18% and 24%, respectively, when the imaginary part varies from –0.005 to –0.1. Scattering and extinction coefficients increase by factors of 118 and 123, respectively, when the geometric mean radius varies from 0.05 to 0.3 ?m. Scattering and extinction coefficients and asymmetry factor increase by factors of 389, 334, and 5.4, respectively, when geometric standard deviation varies from 1.2 to 3.0. The sensitivity simulations using a tropospheric visible radiation model show that the radiation transmission is very sensitive to the change in geometric mean radius and standard deviation;other factors are insignificant.
基金Universiti Kuala Lumpurthe Ministry of Higher Education,Malaysia for providing the scholarship award and financially support through UniKL Grant Scheme(STRG 15144)to the principal author in this projectHiCOE grant(6369107)from Ministry of Higher Education,Malaysia
文摘An engine rubber mounting is one of the important parts of a vehicle. It is a function to isolate or absorb and to reduce vibration to the vehicle body thus to the passenger itself. Due to the engine compartments environment such as heat and massive vibration due to road conditions, the engine rubber mountings lifespan has been reduced. Thus several studies have been conducted to upgrade the material lifespan to make it more reliable and better engine mounting components. This paper presents the conceptual design of kenaf fiber polymer as automotive engine rubber mounting composites using the integration of Theory of Inventive Problem Solving(TRIZ). In this early stage, the solution is generated using 40 inventive principles and TRIZ contradiction method. The solution parameter for the specific design character is the selected using the morphological chart to develop a systematic conceptual design for the component. Four(4) innovative design concepts were produced and Analytic Network Process(ANP)methods were utilized to perform the multi-criteria decision-making process of selecting the best concept design for the polymer composite engine rubber mounting component.
文摘An automatic brush-plating system was developed for component remanufacturing. With this system, Ni/nano-alumina composite coatings from an electrolyte containing 20g/L nano-alumina particles were prepared. Microstructure, surface morphology, microhardness and wear resistance of automatically plated coatings and manually plated coatings were investigated comparatively. The results show that the automatically plated coatings are relatively dense and uniform and have lower friction coefficient of 0.089 under lubricant condition, when compared with manually plated coatings with friction coefficient of 0.14.
文摘IntelligentPad approach provides a standard for dynamically linkable components. Based on the standard, this paper introduces an approach of developing dynamically linkable components by using object oriented techniques.
文摘Hydrogen absorption composite powder of Mg incorporated with Ni and CrCl3 (88∶10∶2 in mass ratio) was prepared by reactive milling in hydrogen atmosphere. Hydriding/dehydriding performances were measured by self-made apparatus. The results show that reactive milling and multi-component addition of Ni and CrCl3 reduce the stability of hydride and improve the sorption performance of Mg-based materials. With powder milled for 60h, hydriding basically completes within 300s (250℃, 2.0MPa) and phase transformation fraction reaches 0.78. The phase transformation rate of hydriding/dehydriding progress increases significantly with the reduced particles size of powder while good kinetics of dehydriding at a relatively low temperature is gained with small grain size of hydride. Rapid temperature variations in a short span of time resulted from remarkable calorific effects of rapid phase transformation are detected in hydriding/dehydriding progress. The results of thermogravimetric and differential scanning calorimetric(TG/DSC) indicate that the onset temperature of desorption of composite milled for 100h is 272℃.
基金supported by the National Natural Science Foundation of China (No.U20A201714)Hebei Education Department (No.QN2021059)Natural Science Foundation of Hebei Province (Nos.B2021208033 and B2021208040)。
文摘A novel La-Co-O-C (LC-C) composites were prepared via a facile co-hydrothermal route with oxides and glycerol and further optimized for methane catalytic activity and thermal stability via component regulation.It was demonstrated that Co3O_(4)phase was the main component in regulation.The combined results of X-ray photoelectron spectroscopy (XPS),temperature-programmed desorption of oxygen (O_(2)-TPD),temperature-programmed reduction of hydrogen (H_(2)-TPR),temperature-programmed desorption of ammonia/carbon dioxide (NH_(3)/CO_(2)-TPD) revealed that component regulation led to more oxygen vacancies and exposure of surface Co_(2)+,lower surface basicity and optimized acidity,which were beneficial for adsorption of active oxygen species and activation of methane molecules,resulting in the excellent catalytic oxidation performance.Especially,the (3.5)LC-C (3.5 is Co-to-La molar ratio) showed the optimum activity and the T50and T90(the temperature at which the CH_(4)conversion rate was 50%and 90%,respectively) were 318 and 367℃,respectively.Using theoretical calculations and in situ diffuse reflection infrared Fourier transform spectroscopy characterization,it was also found that the catalytic mechanism changes from the “Rideal-Eley” mechanism to the “Two-term” mechanism depending on the temperature windows in which the reaction takes place.Besides,the use of the “Flynn-Wall-Ozawa” model in thermoanalytical kinetics revealed that component regulation simultaneously optimized the decomposition activation energy,further expanding the application scope of carboncontaining composites.
基金This study was funded by National Institutes of Health(UL1TR001442).
文摘SUMMARY In many statistical applications,composite variables are constructed to reduce the number of variables and improve the performances of statistical analyses of these variables,especially when some of the variables are highly correlated.Principal component analysis(PCA)and factor analysis(FA)are generally used for such purposes.If the variables are used as explanatory or independent variables in linear regression analysis,partial least squares(PLS)regression is a better alternative.Unlike PCA and FA,PLS creates composite variables by also taking into account the response,or dependent variable,so that they have higher correlations with the response than composites from their PCA and FA counterparts.In this report,we provide an introduction to this useful approach and illustrate it with data from a real study.
基金Supported by the 973 Project (No.2003CB716106), NSFC (No.90208003, 30200059), TRAPOYT, Doctor Training Fund of MOE, PRC, Key Research Project of Science and Technology of MOE, Fok Ying Tong Education Foundation (No.91041)
文摘One important application of independent component analysis (ICA) is in image processing. A two dimensional (2-D) composite ICA algorithm framework for 2-D image independent component analysis (2-D ICA) is proposed. The 2-D nature of the algorithm provides it an advantage of circumventing the roundabout transforming procedures between two dimensional (2-D) image deta and one-dimensional (l-D) signal. Moreover the combination of the Newton (fixed-point algorithm) and natural gradient algorithms in this composite algorithm increases its efficiency and robustness. The convincing results of a successful example in functional magnetic resonance imaging (fMRI) show the potential application of composite 2-D ICA in the brain activity detection.