A reliable and sensitive method is developed for the detection of common diuretics in human urine. diuretics along with probenecid are methylated and subjected to GC-MS analysis.Both chromatographic and mass spectrom...A reliable and sensitive method is developed for the detection of common diuretics in human urine. diuretics along with probenecid are methylated and subjected to GC-MS analysis.Both chromatographic and mass spectrometric data are obtained in selected ion monitoring and full scanning modes.The average detection limit is 0.1-1.0 ag/mi urine.This method is suitable to large-scale and routine screening or confirmation of diuretics in doping control.展开更多
The overburden failure causes the changes of the constant electric field, and the resistivity is the main parameter in these changes. The experimental simulation about tbe response relation between the overburden fail...The overburden failure causes the changes of the constant electric field, and the resistivity is the main parameter in these changes. The experimental simulation about tbe response relation between the overburden failure and its electrical parameter changes is made by building the similar material physics model of mining. The experiment results are used to analyze and test the in-situ detection. The research indicates that the resistivity changes with the electric characteristic of the rock in cracked zone and caving zone caused by overburden failure, the response characteristics of resistivity vary with the failure degrees at different overburden failure zone and that they are corresponding. The resistivity method used in monitoring the overburden failure can determine the height and the affecting scopes of the cracked zone and caving zone. This can provide reliable techaological guarantee for mining design and safe production.展开更多
文摘A reliable and sensitive method is developed for the detection of common diuretics in human urine. diuretics along with probenecid are methylated and subjected to GC-MS analysis.Both chromatographic and mass spectrometric data are obtained in selected ion monitoring and full scanning modes.The average detection limit is 0.1-1.0 ag/mi urine.This method is suitable to large-scale and routine screening or confirmation of diuretics in doping control.
文摘The overburden failure causes the changes of the constant electric field, and the resistivity is the main parameter in these changes. The experimental simulation about tbe response relation between the overburden failure and its electrical parameter changes is made by building the similar material physics model of mining. The experiment results are used to analyze and test the in-situ detection. The research indicates that the resistivity changes with the electric characteristic of the rock in cracked zone and caving zone caused by overburden failure, the response characteristics of resistivity vary with the failure degrees at different overburden failure zone and that they are corresponding. The resistivity method used in monitoring the overburden failure can determine the height and the affecting scopes of the cracked zone and caving zone. This can provide reliable techaological guarantee for mining design and safe production.
