Bulk YBa2Cu3O7 samples were prepared by PMP method. Through adjusting ingredients and preparation procedures, a pellet with 3. 5 cm in diameter and 0. 9 cm in thickness was synthesized. A mass of 1. 3 kg on a magnet c...Bulk YBa2Cu3O7 samples were prepared by PMP method. Through adjusting ingredients and preparation procedures, a pellet with 3. 5 cm in diameter and 0. 9 cm in thickness was synthesized. A mass of 1. 3 kg on a magnet can be levitated at about 1 mm height at 77 K. The XRD and SEM indicated that magnetic lifting property can be enhanced by addition of Ag2O and Y2BaCuO5.展开更多
Rotary swaging processing on commercial as-cast pure Mg has been carried out. Bulk texture variation with the processing passes was investigated using large gauge volume by neutron diffraction, of which results showed...Rotary swaging processing on commercial as-cast pure Mg has been carried out. Bulk texture variation with the processing passes was investigated using large gauge volume by neutron diffraction, of which results showed a combination of different components such as {00.2} basal fibre and two weak {10.0} and {11.0} fibres. Asymmetric distribution of the basal fibre around swaging direction was observed and being related to the processing parameters. Texture gradient analysis by synchrotron radiation demonstrates a non-uniform deformation of the RS processed pure Mg from surface to the centre.展开更多
The paper presents fabrication and characterization of spark plasma sintered textured(001) MgB_(2)with a record degree of orientation of about 40% and 16% by high-energy ultra-sonication and slip casting in high magne...The paper presents fabrication and characterization of spark plasma sintered textured(001) MgB_(2)with a record degree of orientation of about 40% and 16% by high-energy ultra-sonication and slip casting in high magnetic field(12 T) and 0 T magnetic field, respectively.Structural characterization was performed by X-ray diffraction, and electron microscopy. The analysis revealed unexpected preferred orientation also in the MgO secondary phase due to the epitaxial growth of(111) MgO on(001) MgB_(2). The influence of oriented microstructure on the superconducting characteristics expressed by critical current density(J_(c)), irreversibility field(H_(irr)), and on the pinning properties were assessed. High anisotropy versus sample orientation in applied magnetic field, H, was observed for J_(c), Hirr, pinning activation energy(U^(*))extracted from relaxation measurements. The zero-field critical current, J_(c0)and F_(p),maxare weakly or not dependent on the direction of H,while the other indicated parameters are significantly influenced. Results enable control of superconducting parameters by further optimization of microstructure through MgB_(2) texturing as a novel and viable strategy for development of bulk MgB2with enhanced properties when taking advantage of its anisotropy.展开更多
The first neutron texture diffractometer in China has been built at the China Advanced Research Reactor,due to strong demand for texture measurement with neutrons from the domestic user community. This neutron texture...The first neutron texture diffractometer in China has been built at the China Advanced Research Reactor,due to strong demand for texture measurement with neutrons from the domestic user community. This neutron texture diffractometer has high neutron intensity, moderate resolution and is mainly applied to study texture in commonly used industrial materials and engineering components. In this paper, the design and characteristics of this instrument are described. The results for calibration with neutrons and quantitative texture analysis of zirconium alloy plate are presented. The comparison of texture measurements with the results obtained in HIPPO at LANSCE and Kowari at ANSTO illustrates the reliability of the texture diffractometer.展开更多
文摘Bulk YBa2Cu3O7 samples were prepared by PMP method. Through adjusting ingredients and preparation procedures, a pellet with 3. 5 cm in diameter and 0. 9 cm in thickness was synthesized. A mass of 1. 3 kg on a magnet can be levitated at about 1 mm height at 77 K. The XRD and SEM indicated that magnetic lifting property can be enhanced by addition of Ag2O and Y2BaCuO5.
文摘Rotary swaging processing on commercial as-cast pure Mg has been carried out. Bulk texture variation with the processing passes was investigated using large gauge volume by neutron diffraction, of which results showed a combination of different components such as {00.2} basal fibre and two weak {10.0} and {11.0} fibres. Asymmetric distribution of the basal fibre around swaging direction was observed and being related to the processing parameters. Texture gradient analysis by synchrotron radiation demonstrates a non-uniform deformation of the RS processed pure Mg from surface to the centre.
基金financial support from MCI-UEFISCDI Romania, the projects PN030101 (21 N/2019), 5PTE/2020 – BIOTEHKER, and POC 37_697 no. 28/01.09.2016 REBMAT。
文摘The paper presents fabrication and characterization of spark plasma sintered textured(001) MgB_(2)with a record degree of orientation of about 40% and 16% by high-energy ultra-sonication and slip casting in high magnetic field(12 T) and 0 T magnetic field, respectively.Structural characterization was performed by X-ray diffraction, and electron microscopy. The analysis revealed unexpected preferred orientation also in the MgO secondary phase due to the epitaxial growth of(111) MgO on(001) MgB_(2). The influence of oriented microstructure on the superconducting characteristics expressed by critical current density(J_(c)), irreversibility field(H_(irr)), and on the pinning properties were assessed. High anisotropy versus sample orientation in applied magnetic field, H, was observed for J_(c), Hirr, pinning activation energy(U^(*))extracted from relaxation measurements. The zero-field critical current, J_(c0)and F_(p),maxare weakly or not dependent on the direction of H,while the other indicated parameters are significantly influenced. Results enable control of superconducting parameters by further optimization of microstructure through MgB_(2) texturing as a novel and viable strategy for development of bulk MgB2with enhanced properties when taking advantage of its anisotropy.
基金Supported by National Nature Science Foundation of China(11105231,11205248,51327902)International Atomic Energy Agency-TC program(CPR0012)
文摘The first neutron texture diffractometer in China has been built at the China Advanced Research Reactor,due to strong demand for texture measurement with neutrons from the domestic user community. This neutron texture diffractometer has high neutron intensity, moderate resolution and is mainly applied to study texture in commonly used industrial materials and engineering components. In this paper, the design and characteristics of this instrument are described. The results for calibration with neutrons and quantitative texture analysis of zirconium alloy plate are presented. The comparison of texture measurements with the results obtained in HIPPO at LANSCE and Kowari at ANSTO illustrates the reliability of the texture diffractometer.
