Despite the CaCO<sub>3</sub> estimation using titration method was not reliable, but up to the present time, some soil laboratories in Sudan still used this method. The objective of this study was to compa...Despite the CaCO<sub>3</sub> estimation using titration method was not reliable, but up to the present time, some soil laboratories in Sudan still used this method. The objective of this study was to compare and assess the results of calcimetric and titrimetric methods of quantitative estimation for soil calcium carbonate of different soils in Sudan. 26 soil samples from five soil profiles were collected from different climatological and ecological regions in central Sudan. CaCO<sub>3</sub> equivalent was estimated using calcimeter and titration methods in order to find accurate, rapid and suitable method for soils of Sudan. The results revealed that there are no significant differences between calcimeter and titration methods for calcium carbonate estimation in all studied samples except in samples from Gedaref area. We concluded that when the Calcimeter method used for CaCO<sub>3</sub> estimation, the differences between one person and another in detecting titration end point would be avoided, rapid and accurate results would be obtained compared to titration method. Additionally, time would be saved;fewer amounts of chemicals would be used. From this study, we highly recommend using calcimeter method for CaCO<sub>3</sub> estimation for soils of Sudan.展开更多
This study was conducted during 2008-2009 ,which included calcium carbonate determination from 84 locations (40 soil samples from Erbil, 24 samples from Sulaimani and Kirkuk in addition to 20 samples from Duhok) using...This study was conducted during 2008-2009 ,which included calcium carbonate determination from 84 locations (40 soil samples from Erbil, 24 samples from Sulaimani and Kirkuk in addition to 20 samples from Duhok) using calimetric and titration method. The results indicated to significance correlation coefficient between the studied methods or it means that the results of both methods are similar.展开更多
There is a need for determinations of soil organic carbon (SOC) and inorganic carbon (SIC) due to increasing interest in soil carbon sequestration. Two sets of soil samples were collected separately from the Yanqi Bas...There is a need for determinations of soil organic carbon (SOC) and inorganic carbon (SIC) due to increasing interest in soil carbon sequestration. Two sets of soil samples were collected separately from the Yanqi Basin of northwest China to evaluate loss-on-ignition (LOI) method for estimating SOC and SIC in arid soils through determining SOC using an element analyzer, a modified Walkley-Black method and a LOI method with combustion at 375℃ for 17 h and determining SIC using a pressure calcimeter method and a LOI procedure estimated by a weight loss between 375 to 800℃. Our results indicated that the Walkley-Black method provided 99%recovery of SOC for the arid soils tested. There were strong linear relationships(r > 0.93, P < 0.001) for both SOC and SIC between the traditional method and the LOI technique. One set of soil samples was used to develop relationships between LOI and SOC(by the Walkley-Black method), and between LOI and SIC(by the pressure calcimeter method), and the other set of soil samples was used to evaluate the derived equations by comparing predicted SOC and SIC with measured values. The mean absolute errors were small for both SOC (1.7 g C kg-1) and SIC(1.22 g C kg-1), demonstrating that the LOI method was reliable and could provide accurate estimates of SOC and SIC for arid soils.展开更多
文摘Despite the CaCO<sub>3</sub> estimation using titration method was not reliable, but up to the present time, some soil laboratories in Sudan still used this method. The objective of this study was to compare and assess the results of calcimetric and titrimetric methods of quantitative estimation for soil calcium carbonate of different soils in Sudan. 26 soil samples from five soil profiles were collected from different climatological and ecological regions in central Sudan. CaCO<sub>3</sub> equivalent was estimated using calcimeter and titration methods in order to find accurate, rapid and suitable method for soils of Sudan. The results revealed that there are no significant differences between calcimeter and titration methods for calcium carbonate estimation in all studied samples except in samples from Gedaref area. We concluded that when the Calcimeter method used for CaCO<sub>3</sub> estimation, the differences between one person and another in detecting titration end point would be avoided, rapid and accurate results would be obtained compared to titration method. Additionally, time would be saved;fewer amounts of chemicals would be used. From this study, we highly recommend using calcimeter method for CaCO<sub>3</sub> estimation for soils of Sudan.
文摘This study was conducted during 2008-2009 ,which included calcium carbonate determination from 84 locations (40 soil samples from Erbil, 24 samples from Sulaimani and Kirkuk in addition to 20 samples from Duhok) using calimetric and titration method. The results indicated to significance correlation coefficient between the studied methods or it means that the results of both methods are similar.
基金Supported by the "Hundred Talents Program" of the Chinese Academy of Sciences
文摘There is a need for determinations of soil organic carbon (SOC) and inorganic carbon (SIC) due to increasing interest in soil carbon sequestration. Two sets of soil samples were collected separately from the Yanqi Basin of northwest China to evaluate loss-on-ignition (LOI) method for estimating SOC and SIC in arid soils through determining SOC using an element analyzer, a modified Walkley-Black method and a LOI method with combustion at 375℃ for 17 h and determining SIC using a pressure calcimeter method and a LOI procedure estimated by a weight loss between 375 to 800℃. Our results indicated that the Walkley-Black method provided 99%recovery of SOC for the arid soils tested. There were strong linear relationships(r > 0.93, P < 0.001) for both SOC and SIC between the traditional method and the LOI technique. One set of soil samples was used to develop relationships between LOI and SOC(by the Walkley-Black method), and between LOI and SIC(by the pressure calcimeter method), and the other set of soil samples was used to evaluate the derived equations by comparing predicted SOC and SIC with measured values. The mean absolute errors were small for both SOC (1.7 g C kg-1) and SIC(1.22 g C kg-1), demonstrating that the LOI method was reliable and could provide accurate estimates of SOC and SIC for arid soils.
