The tensile-shear interactive damage(TSID)model is a novel and powerful constitutive model for rock-like materials.This study proposes a methodology to calibrate the TSID model parameters to simulate sandstone.The bas...The tensile-shear interactive damage(TSID)model is a novel and powerful constitutive model for rock-like materials.This study proposes a methodology to calibrate the TSID model parameters to simulate sandstone.The basic parameters of sandstone are determined through a series of static and dynamic tests,including uniaxial compression,Brazilian disc,triaxial compression under varying confining pressures,hydrostatic compression,and dynamic compression and tensile tests with a split Hopkinson pressure bar.Based on the sandstone test results from this study and previous research,a step-by-step procedure for parameter calibration is outlined,which accounts for the categories of the strength surface,equation of state(EOS),strain rate effect,and damage.The calibrated parameters are verified through numerical tests that correspond to the experimental loading conditions.Consistency between numerical results and experimental data indicates the precision and reliability of the calibrated parameters.The methodology presented in this study is scientifically sound,straightforward,and essential for improving the TSID model.Furthermore,it has the potential to contribute to other rock constitutive models,particularly new user-defined models.展开更多
An HPLC-DAD method combined with second-order calibration based on the alternating trilinear decomposition(ATLD)algorithm with the aid of region selection was developed to simultaneously and quantitatively characteriz...An HPLC-DAD method combined with second-order calibration based on the alternating trilinear decomposition(ATLD)algorithm with the aid of region selection was developed to simultaneously and quantitatively characterize the synergistic relationships and cumulative excretion of the four bioactive ingredients of Radix Gentianae Macrophyllae in vivo.Although the analytes spectra substantially overlapped with that of the biological matrix,the overlapping profiles between analytes and co-eluting interferences can be successfully separated and accurately quantified by the ATLD method on the basis of the strength of region selection.The proposed approach not only determined the content change but also revealed the synergistic relationships and the cumulative excretion in vivo of the four ingredients in urine and feces samples collected at different excretion time intervals.In addition,several statistical parameters were employed to evaluate the accuracy and precision of the method.Quantitative results were confirmed by HPLC-mass spectrometry.Satisfactory results indicated that the proposed approach can be utilized to investigate the pharmacokinetics of Radix Gentianae Macrophyllae excretion in vivo.展开更多
A new calibration method of L-band radar accuracy using a rotary-wing drone equipped with"GPS"satellite positioning system was proposed.The L-band radar calibration system scheme based on this method was des...A new calibration method of L-band radar accuracy using a rotary-wing drone equipped with"GPS"satellite positioning system was proposed.The L-band radar calibration system scheme based on this method was designed.The theoretical basis required for system realization was studied,and the system calibration method was given.The calibration results referred to the domestic new generation weather radar antenna beam pointing calibration technical indicator(≤0.3°),and its accuracy met relevant business requirement.It show that this method can easily and quickly complete the radar system calibration.Compared with the traditional radar calibration method,it is more convenient,less affected by surrounding environment,and has low requirements on the weather.展开更多
The six-component force/torque sensor has become one kind of the most important sensors with the ability of measuring all the external forces and torques. A novel hyperstatic six-component force/torque sensor based on...The six-component force/torque sensor has become one kind of the most important sensors with the ability of measuring all the external forces and torques. A novel hyperstatic six-component force/torque sensor based on the Stewart platform structure, which can be used for the force measurement of the robot wrist, is proposed, and its structural optimal design, finite element analysis and calibration experimentation is presented. The characteristic of the sensor structure is analyzed in comparison with the traditional Stewart platform-based sensor. The mathematical expression of the sensor's force mapping matrix is introduced. The condition number and generalized amplifying coefficient defined by singular values of force Jacobian matrix are used to evaluate the performances of isotropy and sensitivity of the sensor respectively. The optimal design of the sensor structure is performed with the objective of achieving high measurement sensitivity and good isotropy. The sensor prototype is fabricated, and the static and dynamic characteristics of the sensor are analyzed with finite element analysis software package ANSYS. The calibration device is manufactured, and the data acquisition and processing system is developed. The theoretical and experimental study of the static calibration of the sensor prototype is carried out. The results of simulation analysis and calibration experimentation prove the feasibility of the hyperstatic sensor structure, and the contents of this paper possess theoretical significance and engineering value for the further research and practical application of the six-component force sensor.展开更多
We use the High-energy Electron Experiments(HEP)instrument onboard Arase(ERG)to conduct an energy-dependent cross-satellite calibration of electron fluxes measured by the High Energy Particle Detector(HEPD)onboard Fen...We use the High-energy Electron Experiments(HEP)instrument onboard Arase(ERG)to conduct an energy-dependent cross-satellite calibration of electron fluxes measured by the High Energy Particle Detector(HEPD)onboard FengYun-4A(FY-4A)spanning from April 1,2017,to September 30,2019.By tracing the two-dimensional magnetic positions(L,magnetic local time[MLT])of FY-4A at each time,we compare the datasets of the conjugate electron fluxes over the range of 245–894 keV in 6 energy channels for the satellite pair within different sets of L×MLT.The variations in the electron fluxes observed by FY-4A generally agree with the Arase measurements,and the percentages of the ratios of electron flux conjunctions within a factor of 2 are larger than 50%.Compared with Arase,FY-4A systematically overestimates electron fluxes at all 6 energy channels,with the corresponding calibration factors ranging from 0.67 to 0.81.After the cross-satellite calibration,the electron flux conjunctions between FY-4A and Arase show better agreement,with much smaller normalized root mean square errors.Our results provide a valuable reference for the application of FY-4A high-energy electron datasets to in-depth investigations of the Earth’s radiation belt electron dynamics.展开更多
Due to the low spatial resolution of sea surface temperature(T_S)retrieval by real aperture microwave radiometers,in this study,an iterative retrieval method that minimizes the differences between brightness temperatu...Due to the low spatial resolution of sea surface temperature(T_S)retrieval by real aperture microwave radiometers,in this study,an iterative retrieval method that minimizes the differences between brightness temperature(T_B)measured and modeled was used to retrieve sea surface temperature with a one-dimensional synthetic aperture microwave radiometer,temporarily named 1 D-SAMR.Regarding the configuration of the radiometer,an angular resolution of 0.43°was reached by theoretical calculation.Experiments on sea surface temperature retrieval were carried out with ideal parameters;the results show that the main factors affecting the retrieval accuracy of sea surface temperature are the accuracy of radiometer calibration and the precision of auxiliary geophysical parameters.In the case of no auxiliary parameter errors,the greatest error in retrieved sea surface temperature is obtained at low T_S scene(i.e.,0.7106 K for the incidence angle of 35°under the radiometer calibration accuracy of0.5 K).While errors on auxiliary parameters are assumed to follow a Gaussian distribution,the greatest error on retrieved sea surface temperature was 1.3305 K at an incidence angle of 65°in poorly known sea surface wind speed(W)(the error on W of 1.0 m/s)over high W scene,for the radiometer calibration accuracy of 0.5 K.展开更多
The objective of this paper is to develop a methodology for calibration of a discrete element grain-based model(GBM)to replicate the hydro-mechanical properties of a brittle rock measured in the laboratory,and to appl...The objective of this paper is to develop a methodology for calibration of a discrete element grain-based model(GBM)to replicate the hydro-mechanical properties of a brittle rock measured in the laboratory,and to apply the calibrated model to simulating the formation of excavation damage zone(EDZ)around underground excavations.Firstly,a new cohesive crack model is implemented into the universal distinct element code(UDEC)to control the fracturing behaviour of materials under various loading modes.Next,a methodology for calibration of the components of the UDEC-Voronoi model is discussed.The role of connectivity of induced microcracks on increasing the permeability of laboratory-scale samples is investigated.The calibrated samples are used to investigate the influence of pore fluid pressure on weakening the drained strength of the laboratory-scale rock.The validity of the Terzaghi’s effective stress law for the drained peak strength of low-porosity rock is tested by performing a series of biaxial compression test simulations.Finally,the evolution of damage and pore pressure around two unsupported circular tunnels in crystalline granitic rock is studied.展开更多
The effectiveness of traditional Chinese medicine (TCM) against various diseases urges more low cost, speed and sensitive analytical methods for investigating the phamacology of TCM and providing a theoretical basis f...The effectiveness of traditional Chinese medicine (TCM) against various diseases urges more low cost, speed and sensitive analytical methods for investigating the phamacology of TCM and providing a theoretical basis for clinical use. The potential of second-order calibration method was validated for the quantification of two effective ingredients of Schisandra chinensis in human plasma using spectrofluorimetry. The results obtained in the present study demonstrate the advantages of this strategy for multi-target determination in complex matrices. Although the spectra of the analytes are similar and a large number of interferences also exist, second-order calibration method could predict the accurate concentrations together with reasonable resolution of spectral profiles for analytes of interest owing to its ‘second-order advantage’. Moreover, the method presented in this work allows one to simply experimental procedure as well as reduces the use of harmful chemical solvents.展开更多
In a crowd density estimation dataset,the annotation of crowd locations is an extremely laborious task,and they are not taken into the evaluation metrics.In this paper,we aim to reduce the annotation cost of crowd dat...In a crowd density estimation dataset,the annotation of crowd locations is an extremely laborious task,and they are not taken into the evaluation metrics.In this paper,we aim to reduce the annotation cost of crowd datasets,and propose a crowd density estimation method based on weakly-supervised learning,in the absence of crowd position supervision information,which directly reduces the number of crowds by using the number of pedestrians in the image as the supervised information.For this purpose,we design a new training method,which exploits the correlation between global and local image features by incremental learning to train the network.Specifically,we design a parent-child network(PC-Net)focusing on the global and local image respectively,and propose a linear feature calibration structure to train the PC-Net simultaneously,and the child network learns feature transfer factors and feature bias weights,and uses the transfer factors and bias weights to linearly feature calibrate the features extracted from the Parent network,to improve the convergence of the network by using local features hidden in the crowd images.In addition,we use the pyramid vision transformer as the backbone of the PC-Net to extract crowd features at different levels,and design a global-local feature loss function(L2).We combine it with a crowd counting loss(LC)to enhance the sensitivity of the network to crowd features during the training process,which effectively improves the accuracy of crowd density estimation.The experimental results show that the PC-Net significantly reduces the gap between fullysupervised and weakly-supervised crowd density estimation,and outperforms the comparison methods on five datasets of Shanghai Tech Part A,ShanghaiTech Part B,UCF_CC_50,UCF_QNRF and JHU-CROWD++.展开更多
Cone penetration testing (CPT) is an extensively utilized and cost effective tool for geotechnical site characterization. CPT consists of pushing at a constant rate an electronic cone into penetrable soils and recordi...Cone penetration testing (CPT) is an extensively utilized and cost effective tool for geotechnical site characterization. CPT consists of pushing at a constant rate an electronic cone into penetrable soils and recording the resistance to the cone tip (q<sub>c</sub> value). The measured q<sub>c</sub> values (after correction for the pore water pressure) are utilized to estimate soil type and associated soil properties based predominantly on empirical correlations. The most common cone tips have associated areas of 10 cm<sup>2</sup> and 15 cm<sup>2</sup>. Investigators also utilized significantly larger cone tips (33 cm<sup>2</sup> and 40 cm<sup>2</sup>) so that gravelly soils can be penetrated. Small cone tips (2 cm<sup>2</sup> and 5 cm<sup>2</sup>) are utilized for shallow soil investigations. The cone tip resistance measured at a particular depth is affected by the values above and below the depth of interest which results in a smoothing or blurring of the true bearing values. Extensive work has been carried out in mathematically modelling the smoothing function which results in the blurred cone bearing measurements. This paper outlines a technique which facilitates estimating the dominant parameters of the cone smoothing function from processing real cone bearing data sets. This cone calibration technique is referred to as the so-called CPSPE algorithm. The mathematical details of the CPSPE algorithm are outlined in this paper along with the results from a challenging test bed simulation.展开更多
Microphone array can be used in sound source localization and separation. But gain, phase, and position errors can seriously influence the performance of localization algorithms such as multiple signal classification ...Microphone array can be used in sound source localization and separation. But gain, phase, and position errors can seriously influence the performance of localization algorithms such as multiple signal classification (MUSIC) algorithm. In this paper, a new calibration method for microphone array with gain, phase, and position errors is proposed. Unlike traditional calibration methods for antenna array, the proposed method can be used in the broadband and near-field signal model such as microphone array with arbitrary sensor geometries in one plane. Computer simulations are presented and simulation results show the new method having good performance.展开更多
Global efforts for environmental cleanliness through the control of gaseous emissions from vehicles are gaining momentum and attracting increasing attention. Calibration plays a crucial role in these efforts by ensuri...Global efforts for environmental cleanliness through the control of gaseous emissions from vehicles are gaining momentum and attracting increasing attention. Calibration plays a crucial role in these efforts by ensuring the quantitative assessment of emissions for informed decisions on environmental treatments. This paper describes a method for the calibration of CO/CO<sub>2</sub> monitors used for periodic inspections of vehicles in cites. The calibration was performed in the selected ranges: 900 - 12,000 µmol/mol for CO and 2000 - 20,000 µmol/mol for CO<sub>2</sub>. The traceability of the measurement results to the SI units was ensured by using certified reference materials from CO/N<sub>2</sub> and CO<sub>2</sub>/N<sub>2</sub> primary gas mixtures. The method performance was evaluated by assessing its linearity, accuracy, precision, bias, and uncertainty of the calibration results. The calibration data exhibited a strong linear trend with R² values close to 1, indicating an excellent fit between the measured values and the calibration lines. Precision, expressed as relative standard deviation (%RSD), ranged from 0.48 to 4.56% for CO and from 0.97 to 3.53% for CO<sub>2</sub>, staying well below the 5% threshold for reporting results at a 95% confidence level. Accuracy measured as percent recovery, was consistently high (≥ 99.1%) for CO and ranged from 84.90% to 101.54% across the calibration range for CO<sub>2</sub>. In addition, the method exhibited minimal bias for both CO and CO<sub>2</sub> calibrations and thus provided a reliable and accurate approach for calibrating CO/CO<sub>2</sub> monitors used in vehicle inspections. Thus, it ensures the effectiveness of exhaust emission control for better environment.展开更多
To make the problems of existing high requirements of calibration tools, complex global calibration process addressed for monocular multi-view visual measurement system during measurement, in the paper, a global calib...To make the problems of existing high requirements of calibration tools, complex global calibration process addressed for monocular multi-view visual measurement system during measurement, in the paper, a global calibration method is proposed for the geometric properties of rotational correlation motion and the absolute orientation of the field of view without over lap. Firstly, a dual-camera system is constructed for photographing and collecting the rotating image sequence of two flat targets rigidly connected by a long rod at different positions, and based on the known parameters, such as, target feature image, world coordinates, camera internal parameters and so on, then the global PnP optimization method is used to solve the rotation axis and the reference point at different positions;Then, the absolute orientation matrix is constructed based on the parameters of rotation axis, reference point and connecting rod length obtained by this method. In the end, the singular value decomposition method is used to find the optimal rotation matrix, and then get the translation matrix. It’s shown based on simulation and actual tests that in comparison with the existing methods, the maximum attitude and pose errors is 0.0083˚ and 0.3657 mm, respectively, which improves the accuracy by 27.8% and 24.4%, respectively. The calibration device in this paper is simple, and there are no parallel, vertical and coplanar requirements between multiple rotating positions. At the same time, in view of the calibration accuracy, the accuracy requirements of most application scenarios can be met.展开更多
The instability of a pit mine slope diagnostic caused by the slipping of a localized deep shear zone is described. The slope was designed on ultra basic, serpentine and metabasite rock formations with an angle varying...The instability of a pit mine slope diagnostic caused by the slipping of a localized deep shear zone is described. The slope was designed on ultra basic, serpentine and metabasite rock formations with an angle varying from 40 to 45 de- grees. The perturbed slope zone was classified as RMR 12 and the non-perturbed zone as RMR 75. The boundary of these zones is defined as the shear zone. The pit slope was field mapped in detail and the mechanical properties of the rock were obtained through a laboratory test. The lab data were further processed using the RMR mechanical classifi- cation system. The Distinct Elements Code numerical modeling and simulation software was used to design the pit slope. The model was calibrated through topographic mapping of the points on the ground. The task of calibrating a numerical model is far from simple. Exhaustive attempts to find points of reference are required. The mechanical be- havior in function of the time factor is a problem that has yet to be solved. The instant deformation generated in the numerical model generated functions that can be compared with the deformations of quick shifts acquired in the topog- raphic monitoring. SMR is indeed more often recommended for Pit Slopes, though the fact that we have used RMR does not invalidate the classification for the modeling effect. The main parameters such as spacing, filling, diving direc- tion and continuity allow for compartmentalization of the modeled area. The objective of the modeling was not to pro- ject slopes because this massif was undergoing a progressive slow rupture. The objective of the modeling was to study the movement of the mass of rock and its progressive rupture caused by a shear zone.展开更多
Soft sensor is an efficacious solution to predict the hard-to-measure target variable by using the process variables.In practical application scenarios, however, the feedback cycle of target variable is usually larger...Soft sensor is an efficacious solution to predict the hard-to-measure target variable by using the process variables.In practical application scenarios, however, the feedback cycle of target variable is usually larger than that of the process variables, which causes the deficiency of prediction errors. Consequently soft sensor cannot be calibrated timely and deteriorates. We proposed a soft sensor calibration method by using Just-in-time modeling and Ada Boost learning method. A moving window consisting of a primary part and a secondary part is constructed.The primary part is made of history data from certain number of constant feedback cycles of target variable and the secondary part includes some coarse target values estimated initially by Just-in-time modeling during the latest feedback cycle of target variable. The data set of the whole moving window is processed by Ada Boost learning method to build an auxiliary estimation model and then target variable values of the latest corresponding feedback cycle are reestimated. Finally the soft sensor model is calibrated by using the reestimated target variable values when the target feedback is unavailable; otherwise using the feedback value. The feasibility and effectiveness of the proposed calibration method is tested and verified through a series of comparative experiments on a pH neutralization facility in our laboratory.展开更多
A method using HPLC-DAD coupled with second-order calibration was developed to simultaneously determine metronidazole and tinidazole in plasma samples in this paper. The second-order calibration method based on APTLD ...A method using HPLC-DAD coupled with second-order calibration was developed to simultaneously determine metronidazole and tinidazole in plasma samples in this paper. The second-order calibration method based on APTLD (alternating penalty trilinear decomposition) algorithm was proposed to analyze the three-way HPLC-DAD data from both standard and prediction samples, which makes it possible that calibration can be performed even in the presence of unknown interferences with a simple and green chromatographic condition and short analysis time. The results showed that good recoveries were obtained although the chromatographic and spectral profiles of the analytes of interest as well as background were partially overlapped with each other in plasma samples.展开更多
In order to solve the problems of the fine division of sedimentary sequence cycles and their change in two-dimensional space as well as lateral extension contrast, we developed a method of wavelet depth-frequency anal...In order to solve the problems of the fine division of sedimentary sequence cycles and their change in two-dimensional space as well as lateral extension contrast, we developed a method of wavelet depth-frequency analysis. The single signal and composite signal of different Milankovitch cycles are obtained by numerical simulation. The simulated composite signal can be separated into single signals of a single frequency cycle. We also develop a well-seismic calibration insertion technology which helps to realize the calibration from the spectrum characteristics of a single well to the seismic profile. And then we determine the change and distribution characteristics of spectrum cycles in the two-dimensional space. It points out the direction in determining the variations of the regional sedimentary sequence cycles, underground strata structure and the contact relationship.展开更多
Design and simulation results of a novel multifunctional electronic calibration kit based on microelectromechanical system(MEMS)single-pole double-throw(SPDT)switches are presented in this paper.The short-open-load-th...Design and simulation results of a novel multifunctional electronic calibration kit based on microelectromechanical system(MEMS)single-pole double-throw(SPDT)switches are presented in this paper.The short-open-load-through(SOLT)calibration states can be completed simultaneously by using the MEMS electronic calibration,and the electronic calibrator can be reused 10^(6) times.The simulation results show that this novel electronic calibration can be used in a frequency range of 0.1 GHz–20 GHz,the return loss is less than 0.18 dB and 0.035 dB in short-circuit and open-circuit states,respectively,and the insertion loss in through(thru)state is less than 0.27 dB.On the other hand,the size of this novel calibration kit is only 6 mm×2.8 mm×0.8 mm.Our results demonstrate that the calibrator with integrated radiofrequency microelectromechanical system(RF MEMS)switches can not only provide reduced size,loss,and calibration cost compared with traditional calibration kit but also improves the calibration accuracy and efficiency.It has great potential applications in millimeter-wave measurement and testing technologies,such as device testing,vector network analyzers,and RF probe stations.展开更多
Charged particle diagnosis is an important aspect of laser–plasma experiments conducted at super-intense laser facilities. In recent years, Columbia Resin #39 (CR- 39) detectors have been widely employed for detectin...Charged particle diagnosis is an important aspect of laser–plasma experiments conducted at super-intense laser facilities. In recent years, Columbia Resin #39 (CR- 39) detectors have been widely employed for detecting charged particles in laser–plasma experiments. This is because the CR-39 polymer does not respond to electromagnetic pulses or X-rays. This study presents a method for calibrating the relationship between particle energy and track diameter in a CR-39 detector (TasTrak■) using 3-8 MeV protons, 6-30 MeV carbon ions, and 1–5 MeV alpha particles. The particle tracks were compared under the manufacturer’s recommended etching conditions of 6.25 mol/l NaOH at 98℃ and under the widely adopted experimental conditions of 6.25 mol/l NaOH at 70℃. The results show that if the NaOH solution concentration is 6.25 mol/l, then the temperature of 70℃is more suitable for etching proton tracks than 98℃ and employing a temperature of 98 ℃ to etch alpha-particle and carbon-ion tracks can significantly reduce the etching time. Moreover, this result implies that C3+ ion or alpha-particle tracks can be distinguished from proton tracks with energy above 3 MeV by controlling the etching time. This calibration method for the CR-39 detector can be applied to the diagnosis of reaction products in laser–plasma experiments.展开更多
Some approaches to measure parallel 6-degree of freedom platform's posturestatically and to calibrate the platform's actual structural parameters by measuring a series of theplatform's varying postures are...Some approaches to measure parallel 6-degree of freedom platform's posturestatically and to calibrate the platform's actual structural parameters by measuring a series of theplatform's varying postures are studied. In the case where high posture accuracy is requiredrelatively, to obtain the platform's actual structural parameters is very important. Threedimensions measurement with 2 theodolites are used to obtain the platform's postures statically andNewton iterative method is adopted to calibrate structural parameters. Some measures taken in themeasurement and the calibration are discussed in detail. And the experiment results of theplatform's posture control before and after the calibration are given. The results show that theplatform's posture control accuracy after the calibration is improved notably.展开更多
基金funded by the National Natural Science Foundation of China(Grant No.12272247)National Key Project(Grant No.GJXM92579)Major Research and Development Project of Metallurgical Corporation of China Ltd.in the Non-Steel Field(Grant No.2021-5).
文摘The tensile-shear interactive damage(TSID)model is a novel and powerful constitutive model for rock-like materials.This study proposes a methodology to calibrate the TSID model parameters to simulate sandstone.The basic parameters of sandstone are determined through a series of static and dynamic tests,including uniaxial compression,Brazilian disc,triaxial compression under varying confining pressures,hydrostatic compression,and dynamic compression and tensile tests with a split Hopkinson pressure bar.Based on the sandstone test results from this study and previous research,a step-by-step procedure for parameter calibration is outlined,which accounts for the categories of the strength surface,equation of state(EOS),strain rate effect,and damage.The calibrated parameters are verified through numerical tests that correspond to the experimental loading conditions.Consistency between numerical results and experimental data indicates the precision and reliability of the calibrated parameters.The methodology presented in this study is scientifically sound,straightforward,and essential for improving the TSID model.Furthermore,it has the potential to contribute to other rock constitutive models,particularly new user-defined models.
基金support from the National Natural Science Foundation of China(Grants Nos.21776321,21576297,21205145,21575039)Key Projects of Technological Innovation of Hubei Province(2016ACA138)The Open Research Program(Grant Nos.2015ZD001,2015ZD002 and 2015ZY006)。
文摘An HPLC-DAD method combined with second-order calibration based on the alternating trilinear decomposition(ATLD)algorithm with the aid of region selection was developed to simultaneously and quantitatively characterize the synergistic relationships and cumulative excretion of the four bioactive ingredients of Radix Gentianae Macrophyllae in vivo.Although the analytes spectra substantially overlapped with that of the biological matrix,the overlapping profiles between analytes and co-eluting interferences can be successfully separated and accurately quantified by the ATLD method on the basis of the strength of region selection.The proposed approach not only determined the content change but also revealed the synergistic relationships and the cumulative excretion in vivo of the four ingredients in urine and feces samples collected at different excretion time intervals.In addition,several statistical parameters were employed to evaluate the accuracy and precision of the method.Quantitative results were confirmed by HPLC-mass spectrometry.Satisfactory results indicated that the proposed approach can be utilized to investigate the pharmacokinetics of Radix Gentianae Macrophyllae excretion in vivo.
文摘A new calibration method of L-band radar accuracy using a rotary-wing drone equipped with"GPS"satellite positioning system was proposed.The L-band radar calibration system scheme based on this method was designed.The theoretical basis required for system realization was studied,and the system calibration method was given.The calibration results referred to the domestic new generation weather radar antenna beam pointing calibration technical indicator(≤0.3°),and its accuracy met relevant business requirement.It show that this method can easily and quickly complete the radar system calibration.Compared with the traditional radar calibration method,it is more convenient,less affected by surrounding environment,and has low requirements on the weather.
基金supported by National Natural Science Foundation of China (Grant No. 50575192)Hebei Provincial Natural Science Foundation of China (Grant No. E2007000349)
文摘The six-component force/torque sensor has become one kind of the most important sensors with the ability of measuring all the external forces and torques. A novel hyperstatic six-component force/torque sensor based on the Stewart platform structure, which can be used for the force measurement of the robot wrist, is proposed, and its structural optimal design, finite element analysis and calibration experimentation is presented. The characteristic of the sensor structure is analyzed in comparison with the traditional Stewart platform-based sensor. The mathematical expression of the sensor's force mapping matrix is introduced. The condition number and generalized amplifying coefficient defined by singular values of force Jacobian matrix are used to evaluate the performances of isotropy and sensitivity of the sensor respectively. The optimal design of the sensor structure is performed with the objective of achieving high measurement sensitivity and good isotropy. The sensor prototype is fabricated, and the static and dynamic characteristics of the sensor are analyzed with finite element analysis software package ANSYS. The calibration device is manufactured, and the data acquisition and processing system is developed. The theoretical and experimental study of the static calibration of the sensor prototype is carried out. The results of simulation analysis and calibration experimentation prove the feasibility of the hyperstatic sensor structure, and the contents of this paper possess theoretical significance and engineering value for the further research and practical application of the six-component force sensor.
基金supported by the National Natural Science Foundation of China(Grant Nos.42025404,42188101,42241143,41931073,and 42204160)the National Key R&D Program of China(Grant Nos.2022YFF0503700,2022YFF0503900,and 2021YFA0718600)+1 种基金the B-type Strategic Priority Program of the Chinese Academy of Sciences(Grant No.XDB41000000)the Fundamental Research Funds for the Central Universities(Grant Nos.2042022kf1012 and 2042022kf1016).
文摘We use the High-energy Electron Experiments(HEP)instrument onboard Arase(ERG)to conduct an energy-dependent cross-satellite calibration of electron fluxes measured by the High Energy Particle Detector(HEPD)onboard FengYun-4A(FY-4A)spanning from April 1,2017,to September 30,2019.By tracing the two-dimensional magnetic positions(L,magnetic local time[MLT])of FY-4A at each time,we compare the datasets of the conjugate electron fluxes over the range of 245–894 keV in 6 energy channels for the satellite pair within different sets of L×MLT.The variations in the electron fluxes observed by FY-4A generally agree with the Arase measurements,and the percentages of the ratios of electron flux conjunctions within a factor of 2 are larger than 50%.Compared with Arase,FY-4A systematically overestimates electron fluxes at all 6 energy channels,with the corresponding calibration factors ranging from 0.67 to 0.81.After the cross-satellite calibration,the electron flux conjunctions between FY-4A and Arase show better agreement,with much smaller normalized root mean square errors.Our results provide a valuable reference for the application of FY-4A high-energy electron datasets to in-depth investigations of the Earth’s radiation belt electron dynamics.
基金The National Natural Science Foundation of China under contract Nos 41475019,41575028,41705007,41605016,and 41505016。
文摘Due to the low spatial resolution of sea surface temperature(T_S)retrieval by real aperture microwave radiometers,in this study,an iterative retrieval method that minimizes the differences between brightness temperature(T_B)measured and modeled was used to retrieve sea surface temperature with a one-dimensional synthetic aperture microwave radiometer,temporarily named 1 D-SAMR.Regarding the configuration of the radiometer,an angular resolution of 0.43°was reached by theoretical calculation.Experiments on sea surface temperature retrieval were carried out with ideal parameters;the results show that the main factors affecting the retrieval accuracy of sea surface temperature are the accuracy of radiometer calibration and the precision of auxiliary geophysical parameters.In the case of no auxiliary parameter errors,the greatest error in retrieved sea surface temperature is obtained at low T_S scene(i.e.,0.7106 K for the incidence angle of 35°under the radiometer calibration accuracy of0.5 K).While errors on auxiliary parameters are assumed to follow a Gaussian distribution,the greatest error on retrieved sea surface temperature was 1.3305 K at an incidence angle of 65°in poorly known sea surface wind speed(W)(the error on W of 1.0 m/s)over high W scene,for the radiometer calibration accuracy of 0.5 K.
文摘The objective of this paper is to develop a methodology for calibration of a discrete element grain-based model(GBM)to replicate the hydro-mechanical properties of a brittle rock measured in the laboratory,and to apply the calibrated model to simulating the formation of excavation damage zone(EDZ)around underground excavations.Firstly,a new cohesive crack model is implemented into the universal distinct element code(UDEC)to control the fracturing behaviour of materials under various loading modes.Next,a methodology for calibration of the components of the UDEC-Voronoi model is discussed.The role of connectivity of induced microcracks on increasing the permeability of laboratory-scale samples is investigated.The calibrated samples are used to investigate the influence of pore fluid pressure on weakening the drained strength of the laboratory-scale rock.The validity of the Terzaghi’s effective stress law for the drained peak strength of low-porosity rock is tested by performing a series of biaxial compression test simulations.Finally,the evolution of damage and pore pressure around two unsupported circular tunnels in crystalline granitic rock is studied.
基金the National Natural Science Foundation of China (Grant No. 21175041)the National Basic Research Program (Grant No. 2012CB910602)Program for Changjiang Scholars and Innovative Research Team in University (PCSIRT) for financial supports
文摘The effectiveness of traditional Chinese medicine (TCM) against various diseases urges more low cost, speed and sensitive analytical methods for investigating the phamacology of TCM and providing a theoretical basis for clinical use. The potential of second-order calibration method was validated for the quantification of two effective ingredients of Schisandra chinensis in human plasma using spectrofluorimetry. The results obtained in the present study demonstrate the advantages of this strategy for multi-target determination in complex matrices. Although the spectra of the analytes are similar and a large number of interferences also exist, second-order calibration method could predict the accurate concentrations together with reasonable resolution of spectral profiles for analytes of interest owing to its ‘second-order advantage’. Moreover, the method presented in this work allows one to simply experimental procedure as well as reduces the use of harmful chemical solvents.
基金the Humanities and Social Science Fund of the Ministry of Education of China(21YJAZH077)。
文摘In a crowd density estimation dataset,the annotation of crowd locations is an extremely laborious task,and they are not taken into the evaluation metrics.In this paper,we aim to reduce the annotation cost of crowd datasets,and propose a crowd density estimation method based on weakly-supervised learning,in the absence of crowd position supervision information,which directly reduces the number of crowds by using the number of pedestrians in the image as the supervised information.For this purpose,we design a new training method,which exploits the correlation between global and local image features by incremental learning to train the network.Specifically,we design a parent-child network(PC-Net)focusing on the global and local image respectively,and propose a linear feature calibration structure to train the PC-Net simultaneously,and the child network learns feature transfer factors and feature bias weights,and uses the transfer factors and bias weights to linearly feature calibrate the features extracted from the Parent network,to improve the convergence of the network by using local features hidden in the crowd images.In addition,we use the pyramid vision transformer as the backbone of the PC-Net to extract crowd features at different levels,and design a global-local feature loss function(L2).We combine it with a crowd counting loss(LC)to enhance the sensitivity of the network to crowd features during the training process,which effectively improves the accuracy of crowd density estimation.The experimental results show that the PC-Net significantly reduces the gap between fullysupervised and weakly-supervised crowd density estimation,and outperforms the comparison methods on five datasets of Shanghai Tech Part A,ShanghaiTech Part B,UCF_CC_50,UCF_QNRF and JHU-CROWD++.
文摘Cone penetration testing (CPT) is an extensively utilized and cost effective tool for geotechnical site characterization. CPT consists of pushing at a constant rate an electronic cone into penetrable soils and recording the resistance to the cone tip (q<sub>c</sub> value). The measured q<sub>c</sub> values (after correction for the pore water pressure) are utilized to estimate soil type and associated soil properties based predominantly on empirical correlations. The most common cone tips have associated areas of 10 cm<sup>2</sup> and 15 cm<sup>2</sup>. Investigators also utilized significantly larger cone tips (33 cm<sup>2</sup> and 40 cm<sup>2</sup>) so that gravelly soils can be penetrated. Small cone tips (2 cm<sup>2</sup> and 5 cm<sup>2</sup>) are utilized for shallow soil investigations. The cone tip resistance measured at a particular depth is affected by the values above and below the depth of interest which results in a smoothing or blurring of the true bearing values. Extensive work has been carried out in mathematically modelling the smoothing function which results in the blurred cone bearing measurements. This paper outlines a technique which facilitates estimating the dominant parameters of the cone smoothing function from processing real cone bearing data sets. This cone calibration technique is referred to as the so-called CPSPE algorithm. The mathematical details of the CPSPE algorithm are outlined in this paper along with the results from a challenging test bed simulation.
基金This work was supported by the Key Project of Science and Technology of Sichuan Province under Grant No. 04GG21-02-20.
文摘Microphone array can be used in sound source localization and separation. But gain, phase, and position errors can seriously influence the performance of localization algorithms such as multiple signal classification (MUSIC) algorithm. In this paper, a new calibration method for microphone array with gain, phase, and position errors is proposed. Unlike traditional calibration methods for antenna array, the proposed method can be used in the broadband and near-field signal model such as microphone array with arbitrary sensor geometries in one plane. Computer simulations are presented and simulation results show the new method having good performance.
文摘Global efforts for environmental cleanliness through the control of gaseous emissions from vehicles are gaining momentum and attracting increasing attention. Calibration plays a crucial role in these efforts by ensuring the quantitative assessment of emissions for informed decisions on environmental treatments. This paper describes a method for the calibration of CO/CO<sub>2</sub> monitors used for periodic inspections of vehicles in cites. The calibration was performed in the selected ranges: 900 - 12,000 µmol/mol for CO and 2000 - 20,000 µmol/mol for CO<sub>2</sub>. The traceability of the measurement results to the SI units was ensured by using certified reference materials from CO/N<sub>2</sub> and CO<sub>2</sub>/N<sub>2</sub> primary gas mixtures. The method performance was evaluated by assessing its linearity, accuracy, precision, bias, and uncertainty of the calibration results. The calibration data exhibited a strong linear trend with R² values close to 1, indicating an excellent fit between the measured values and the calibration lines. Precision, expressed as relative standard deviation (%RSD), ranged from 0.48 to 4.56% for CO and from 0.97 to 3.53% for CO<sub>2</sub>, staying well below the 5% threshold for reporting results at a 95% confidence level. Accuracy measured as percent recovery, was consistently high (≥ 99.1%) for CO and ranged from 84.90% to 101.54% across the calibration range for CO<sub>2</sub>. In addition, the method exhibited minimal bias for both CO and CO<sub>2</sub> calibrations and thus provided a reliable and accurate approach for calibrating CO/CO<sub>2</sub> monitors used in vehicle inspections. Thus, it ensures the effectiveness of exhaust emission control for better environment.
文摘To make the problems of existing high requirements of calibration tools, complex global calibration process addressed for monocular multi-view visual measurement system during measurement, in the paper, a global calibration method is proposed for the geometric properties of rotational correlation motion and the absolute orientation of the field of view without over lap. Firstly, a dual-camera system is constructed for photographing and collecting the rotating image sequence of two flat targets rigidly connected by a long rod at different positions, and based on the known parameters, such as, target feature image, world coordinates, camera internal parameters and so on, then the global PnP optimization method is used to solve the rotation axis and the reference point at different positions;Then, the absolute orientation matrix is constructed based on the parameters of rotation axis, reference point and connecting rod length obtained by this method. In the end, the singular value decomposition method is used to find the optimal rotation matrix, and then get the translation matrix. It’s shown based on simulation and actual tests that in comparison with the existing methods, the maximum attitude and pose errors is 0.0083˚ and 0.3657 mm, respectively, which improves the accuracy by 27.8% and 24.4%, respectively. The calibration device in this paper is simple, and there are no parallel, vertical and coplanar requirements between multiple rotating positions. At the same time, in view of the calibration accuracy, the accuracy requirements of most application scenarios can be met.
文摘The instability of a pit mine slope diagnostic caused by the slipping of a localized deep shear zone is described. The slope was designed on ultra basic, serpentine and metabasite rock formations with an angle varying from 40 to 45 de- grees. The perturbed slope zone was classified as RMR 12 and the non-perturbed zone as RMR 75. The boundary of these zones is defined as the shear zone. The pit slope was field mapped in detail and the mechanical properties of the rock were obtained through a laboratory test. The lab data were further processed using the RMR mechanical classifi- cation system. The Distinct Elements Code numerical modeling and simulation software was used to design the pit slope. The model was calibrated through topographic mapping of the points on the ground. The task of calibrating a numerical model is far from simple. Exhaustive attempts to find points of reference are required. The mechanical be- havior in function of the time factor is a problem that has yet to be solved. The instant deformation generated in the numerical model generated functions that can be compared with the deformations of quick shifts acquired in the topog- raphic monitoring. SMR is indeed more often recommended for Pit Slopes, though the fact that we have used RMR does not invalidate the classification for the modeling effect. The main parameters such as spacing, filling, diving direc- tion and continuity allow for compartmentalization of the modeled area. The objective of the modeling was not to pro- ject slopes because this massif was undergoing a progressive slow rupture. The objective of the modeling was to study the movement of the mass of rock and its progressive rupture caused by a shear zone.
基金Supported by the National Basic Research Program of China(2012CB720500)
文摘Soft sensor is an efficacious solution to predict the hard-to-measure target variable by using the process variables.In practical application scenarios, however, the feedback cycle of target variable is usually larger than that of the process variables, which causes the deficiency of prediction errors. Consequently soft sensor cannot be calibrated timely and deteriorates. We proposed a soft sensor calibration method by using Just-in-time modeling and Ada Boost learning method. A moving window consisting of a primary part and a secondary part is constructed.The primary part is made of history data from certain number of constant feedback cycles of target variable and the secondary part includes some coarse target values estimated initially by Just-in-time modeling during the latest feedback cycle of target variable. The data set of the whole moving window is processed by Ada Boost learning method to build an auxiliary estimation model and then target variable values of the latest corresponding feedback cycle are reestimated. Finally the soft sensor model is calibrated by using the reestimated target variable values when the target feedback is unavailable; otherwise using the feedback value. The feasibility and effectiveness of the proposed calibration method is tested and verified through a series of comparative experiments on a pH neutralization facility in our laboratory.
基金financially supported by The National Natural Science Foundation of China(No.20775025)The National Basic Research Program(No.2007CB216404) as well as PCSIRT
文摘A method using HPLC-DAD coupled with second-order calibration was developed to simultaneously determine metronidazole and tinidazole in plasma samples in this paper. The second-order calibration method based on APTLD (alternating penalty trilinear decomposition) algorithm was proposed to analyze the three-way HPLC-DAD data from both standard and prediction samples, which makes it possible that calibration can be performed even in the presence of unknown interferences with a simple and green chromatographic condition and short analysis time. The results showed that good recoveries were obtained although the chromatographic and spectral profiles of the analytes of interest as well as background were partially overlapped with each other in plasma samples.
基金supported by the Fundamental Research Funds for the Central Universities(Grant No.2011YYL128)the CNPC Innovation Foundation(GrantNo.2012D-5006-0103)the Ministry of Land and Resources special funds for scientific research on public cause(Grant No.201311107)
文摘In order to solve the problems of the fine division of sedimentary sequence cycles and their change in two-dimensional space as well as lateral extension contrast, we developed a method of wavelet depth-frequency analysis. The single signal and composite signal of different Milankovitch cycles are obtained by numerical simulation. The simulated composite signal can be separated into single signals of a single frequency cycle. We also develop a well-seismic calibration insertion technology which helps to realize the calibration from the spectrum characteristics of a single well to the seismic profile. And then we determine the change and distribution characteristics of spectrum cycles in the two-dimensional space. It points out the direction in determining the variations of the regional sedimentary sequence cycles, underground strata structure and the contact relationship.
基金Project supported by the National Defense Technology Industry Strong,China (Grant No. JCKY2018408B006)the Information System New Items Project,China (Grant Nos. 2018XW0026 and 2019XW0010)the Information System Pre-research Project,China (Grant No. 31513060101)
文摘Design and simulation results of a novel multifunctional electronic calibration kit based on microelectromechanical system(MEMS)single-pole double-throw(SPDT)switches are presented in this paper.The short-open-load-through(SOLT)calibration states can be completed simultaneously by using the MEMS electronic calibration,and the electronic calibrator can be reused 10^(6) times.The simulation results show that this novel electronic calibration can be used in a frequency range of 0.1 GHz–20 GHz,the return loss is less than 0.18 dB and 0.035 dB in short-circuit and open-circuit states,respectively,and the insertion loss in through(thru)state is less than 0.27 dB.On the other hand,the size of this novel calibration kit is only 6 mm×2.8 mm×0.8 mm.Our results demonstrate that the calibrator with integrated radiofrequency microelectromechanical system(RF MEMS)switches can not only provide reduced size,loss,and calibration cost compared with traditional calibration kit but also improves the calibration accuracy and efficiency.It has great potential applications in millimeter-wave measurement and testing technologies,such as device testing,vector network analyzers,and RF probe stations.
基金supported in part by the Strategic Priority Research Program of the Chinese Academy of Sciences(No.XDB160203)the National Natural Science Foundation of China(Nos.11875311,11421505,and 11475245)
文摘Charged particle diagnosis is an important aspect of laser–plasma experiments conducted at super-intense laser facilities. In recent years, Columbia Resin #39 (CR- 39) detectors have been widely employed for detecting charged particles in laser–plasma experiments. This is because the CR-39 polymer does not respond to electromagnetic pulses or X-rays. This study presents a method for calibrating the relationship between particle energy and track diameter in a CR-39 detector (TasTrak■) using 3-8 MeV protons, 6-30 MeV carbon ions, and 1–5 MeV alpha particles. The particle tracks were compared under the manufacturer’s recommended etching conditions of 6.25 mol/l NaOH at 98℃ and under the widely adopted experimental conditions of 6.25 mol/l NaOH at 70℃. The results show that if the NaOH solution concentration is 6.25 mol/l, then the temperature of 70℃is more suitable for etching proton tracks than 98℃ and employing a temperature of 98 ℃ to etch alpha-particle and carbon-ion tracks can significantly reduce the etching time. Moreover, this result implies that C3+ ion or alpha-particle tracks can be distinguished from proton tracks with energy above 3 MeV by controlling the etching time. This calibration method for the CR-39 detector can be applied to the diagnosis of reaction products in laser–plasma experiments.
基金This project is supported by National Defense Science and Technology Multi-vocation Foundation in Advance Research of China(No. 97J465JW0408).
文摘Some approaches to measure parallel 6-degree of freedom platform's posturestatically and to calibrate the platform's actual structural parameters by measuring a series of theplatform's varying postures are studied. In the case where high posture accuracy is requiredrelatively, to obtain the platform's actual structural parameters is very important. Threedimensions measurement with 2 theodolites are used to obtain the platform's postures statically andNewton iterative method is adopted to calibrate structural parameters. Some measures taken in themeasurement and the calibration are discussed in detail. And the experiment results of theplatform's posture control before and after the calibration are given. The results show that theplatform's posture control accuracy after the calibration is improved notably.