Effect of Low-Temperature Thermal Oxidation on the Capillary Performance of Sintered Copper Powder Wicks

In this study,a composite powder capillary wick is prepared,manufactured by sintering copper powder and surface treated by low-temperature thermal oxidation.It is used to improve the performance of the capillary wick.The forced flow method and infrared imaging method are used to test the permeability and capillary performance of the samples.The effects of different oxidation temperatures on the performance of capillary wick are investigated.The experimental results show that the wetting performance of the oxidized samples is significantly enhanced.With the increase of oxidation temperature,the permeability decreases.The capillary height and velocity of the thermally oxidized samples are significantly higher than those of the untreated capillary wick.However,the oxidation temperature needs to be adjusted to obtain the best capillary performance.The highest capillary performance is found at oxidation temperature of 300℃,with an increase of 46% compared to the untreated ones.Comparisons with other composite wicks show that the sample with an oxidation temperature of 300℃ has competitive capillary performance,making it a favorable alternative to two-phase heat transfer device.This study shows that combining low-temperature thermal oxidation technology with powder sintering is a convenient and effective method to improve the capillary performance of powder wicks.

Effect of stagger angle on capillary performance of microgroove structures with reentrant cavities

Aluminum-based microgroove surfaces with reentrant cavities (MSRCs) were fabricated by two staggered ploughing/extrusion processes to meet the requirements of lightweight phase change heat transfer devices.Five MSRCs with different stagger angles between cavities and microgrooves (MGs) were fabricated to study the effect of stagger angle on capillary performance.Capillary rise and permeability tests were performed on all MSRCs and the results were compared with MGs having the same processing parameters.It was found that MSRCs with smaller stagger angles have higher capillary height,and the maximum enhancement maintained by MSRC45 was about 54.84%.However,MSRCs with larger stagger angles were found to have higher permeability.Therefore,the capillary parameter K·ΔP_(cap)was used as a comprehensive index to evaluate these wicks.MSRC90 and MSRC75 obtained the largest K·ΔP_(cap)values without and with the effect of gravity considered,respectively.Although all MSRCs had a higher capillary rise height than MGs,smaller stagger angles (≤60°) seriously reduced the permeability of MSRCs and even resulted in smaller K·ΔP_(cap)value than that of MGs when calculated considering the effect of gravity.Therefore,MSRCs with larger stagger angles (≥75°) may be the optimum wicks due to the good balance between capillary pressure and permeability.

Capillary Performance of Nanoporous Aluminum Braided Wicks Prepared by Anodic Oxidation

With the rapid development of two-phase heat exchangers,the further improvement of the capillary performance of their internal wick faces a great challenge.As an important technology in the surface treatment of aluminum alloys,anodic oxidation has been widely used to develop various functional nanostructures.In this study,nanopores with diameters of 30–40 nm were fabricated on the surface of aluminum fibers through anodic oxidation under an oxalic acid system.Results showed that anodizing increased the specific surface area of the aluminum braid by 163 times,and changed its surface wettability from hydrophobic to superhydrophilic.A significant reduction in the effective capillary radius can substantially increase the capillary force of aluminum braids on the basis of capillary theory.Therefore,the nanoporous aluminum braids can be used as a novel wick in the vapor chamber to improve its capillary performance.Capillary rate-of-rise tests with ethanol and acetone were performed to characterize the capillary of this novel wick structure.Infrared thermal imaging was utilized to monitor the capillary rise of aluminum braided wicks.The capillary force of the anodized wicks was greater than that of a normal wick,and the maximum capillary rise height was 81 mm.The nanoporous aluminum braided wicks prepared by anodizing could be applied in heat transfer.

Determination of Chromate Ion in Water Using High Performance Capillary Electrophoresis

A new rapid method for the analysis of chromate ion in water by using high performance capillary electrophoresis is described. The detection limit is 1.0 mu g/ml by using 100 m mol/l Tris-HCl buffer containing 2 m mol/l 1,6-hexanediamine which was used as an electroosmosis modifier to improve the separation and detection sensitivity.

Com parison of Amino Acids in Root Exudates of Flue-cured Tobacco Varieties with Different Resistances against Black Shank

In order to explore the differences of amino acids in root exudates and plant tissues, we selected four flue-cured tobacco varieties [ Yunyan 87 （ Ⅰ）, K326 （Ⅱ）, NC102（Ⅲ）, Hongda （Ⅳ）] as the test materials and studied the components and mass fractions of amino acids in rhizosphere soil, non rhizosphere soil, roots and leaves via high performance capillary zone electrophoresis. Ten amino acids were detected out from four varieties, including histidine, lysine, tryptophan, phenylalanine, valine, threonine, proline, serine, alanine and glycine. The mass fractions of amino acids in leaves and roots were higher than those in rhizosphere soil and non rhizosphere soil. In rhizosphere soil and non-rhizosphere soil, the mass fractions of lysine, phenylalanine, threonine, proline and glycine in susceptible varieties （ Ⅲ, Ⅳ） were higher than those in resistant varieties （ Ⅰ, Ⅱ）. In rhizosphere soil, the total amino acids successively were Ⅳ 〉 Ⅲ 〉 Ⅰ 〉 Ⅱ, and in non rhi- zosphere soil were Ⅲ 〉 Ⅳ 〉 Ⅰ 〉 Ⅱ. The total amino acids in roots of variety Ⅳ was the highest, up to 6 359. 195 μg/g. In leaves, the total amino acids in varieties I and If were higher than those in varieties IfI and IV. The results indicated that amino acids could secrete to rhizosphere via root secretion, and the compositions and mass fractions of amino acids varied with flue-cured tobacco varieties, thus the secretion amount of susceptible varieties was higher than that of resistant varieties.

Migration equation of solute in high performance capillary zone electrophoresis

In order to reveal the relationship between migration time and solute structure aswell as electrophoretic operation conditions in high performance capillary zoneelectrophoresis (HPCZE), researchers have presented many empirical and semi-empiricalmodels. These models have two main dissatisfactory points. Firstly, a constant is im-

Experimental Investigation on the Vapor Chambers with Sintered Copper Powder Wick

High power electronics units generate high-density heat flux,which poses a significant threat to the reliability of these devices.The vapor chamber(VC)has a very high heat transfer rate and has a wide range of applications in the heat dissipation of electronic products.VCs with sintered copper powder wicks sized as irregular shape copper powder 50μm(I-50μm),I-75μm,I-110μm,I-150μm were studied in this paper.The effect of liquid filling ratio was discussed.The results indicated that the thermal resistance of all VCs decreased with the increase of heating power.The capillary performance of wick was the dominant factor for the heat transfer performance of VCs with different kinds of wick.A capillary performance factor was proposed to evaluate the capillary performance of VCs.The capillary performance factor of VC with the wick of I-75μm was much higher than that of the other types of VC in this study.The heat source surface temperature of VCs could be affected by filling ratio and wick structure.But,it should be insensitive to the filling ratio when a better capillary performance factor was obtained.With the same heating area and similar structure,the maximum heat flux density of the VC would decrease as the height of vapor cavity decreased.