An experimental system of AC arc discharge in water was designed with pole-pole electrodes and a peak voltage of 1500 V and a test circuit was set up using virtual instrument technology. The mechanism of an AC plasma ...An experimental system of AC arc discharge in water was designed with pole-pole electrodes and a peak voltage of 1500 V and a test circuit was set up using virtual instrument technology. The mechanism of an AC plasma arc generated in water was analyzed. The voltage- current characteristic of the AC plasma are was obtained from the waveform. The temperature characteristic was tested with a spectrum diagnosis system, and the effect of different electrode materials on the striking voltage and peak current was analyzed. The results show that when a power supply of 6 kW is applied on electrodes with a gap of 2 mm in water, the striking voltage is from 900 V to 1300 V, the arc voltage is from 40 V to 100 V, the arc current is from 2 A to 7 A, and the zero rest period is from 1 ms to 2 ms. In addition, the arc voltage and current are different for electrodes in aluminum, copper and stainless steel. The arc voltage is lower and the current is higher for an aluminum electrode than those for copper and stainless steel ones. The highest temperature of the arc is 7643 K.展开更多
Generation characteristics of vacuum discharge plasma are very important for the applied research of metal plasma. The vacuum discharge electrode configuration and the cathode material affect the generation characteri...Generation characteristics of vacuum discharge plasma are very important for the applied research of metal plasma. The vacuum discharge electrode configuration and the cathode material affect the generation characteristics of the metal plasma which consists of metal ions coming from cathode and generated by vacuum discharge. In this research, the generation characteristics of the metal plasma generated by vacuum discharge are discussed for four patterns of electrode configurations, i.e. cone-mesh electrode setup, cone-cross line electrode setup, cone-line electrode setup and cone-ring electrode setup. Characteristics of the metal plasma, such as elec- tron density, electron temperature, space potential, ion energy, are measured by the probe method for discussing the impacts of different electrode configurations on the density of generated metal plasma. Moreover, the diffusion velocities of the metal plasma are measured for cathode materials of Pb, Al, and Cu, respectively. The experimental results indicate that the plasma generated by the discharge of cone-ring electrode configuration possesses the maximum density and the metal plasma generated by the Al cathode possesses the fastest diffusion velocity and the highest kinetic energy.展开更多
he present paper covers tlie preparation and isolation of a series of monosub-stituted molybdophosphates Na_5 [PZ(H_2O)Mo_11 O_39]· 5H_2O (Z=Mn ̄2+, Co ̄2+,Ni ̄2+, Cu ̄2+, Zn ̄2+)by an improved method. These comp...he present paper covers tlie preparation and isolation of a series of monosub-stituted molybdophosphates Na_5 [PZ(H_2O)Mo_11 O_39]· 5H_2O (Z=Mn ̄2+, Co ̄2+,Ni ̄2+, Cu ̄2+, Zn ̄2+)by an improved method. These complexes were characterized byfull elemental analysis, IR spectra and UV-Vis. The studies show that the pre-pared products still keep Keggin structure and the substituting metal would belooated in coordination site. Based on this, their some pysico-cliemical propertiesrelated with their catalytic beliaviour,such as thermal stability and acidity proper-ty, were studied.展开更多
Reduction of error due to the influence of temperature on the quartz flexible accelerometer without any heating device is a difficult task, and is also a tendency for research and application. In this paper, static an...Reduction of error due to the influence of temperature on the quartz flexible accelerometer without any heating device is a difficult task, and is also a tendency for research and application. In this paper, static and dynamic temperature compensation models are established in order to reduce the temperature influence on accelerometer measurement accuracy. Combined with the experiment data, the relationship between the accelerometer output accuracy, temperature and the magnitude of acceleration is analyzed. The data collected from the temperature experiment show that output value of the accelerometer varies with temperature. The method of uniaxial quadrature experiment is adopted and the accelerometer output value is gauged at temperature ranging from-20℃ to 50℃. Having used the static and the dynamic temperature compensation models, the accelerometer temperature error compensation experiment is conducted and the compensated errors by the two models are analyzed. The result shows that the compensated value meets the technical requirements. Two technical indicators, the zero bias K0 and the scaling factor K1, which are used to measure the degree of accelerometers, are both improved and their fluctuation ranges are reduced.展开更多
基金supported by National Natural Science Foundation of China (No. 50777014)
文摘An experimental system of AC arc discharge in water was designed with pole-pole electrodes and a peak voltage of 1500 V and a test circuit was set up using virtual instrument technology. The mechanism of an AC plasma arc generated in water was analyzed. The voltage- current characteristic of the AC plasma are was obtained from the waveform. The temperature characteristic was tested with a spectrum diagnosis system, and the effect of different electrode materials on the striking voltage and peak current was analyzed. The results show that when a power supply of 6 kW is applied on electrodes with a gap of 2 mm in water, the striking voltage is from 900 V to 1300 V, the arc voltage is from 40 V to 100 V, the arc current is from 2 A to 7 A, and the zero rest period is from 1 ms to 2 ms. In addition, the arc voltage and current are different for electrodes in aluminum, copper and stainless steel. The arc voltage is lower and the current is higher for an aluminum electrode than those for copper and stainless steel ones. The highest temperature of the arc is 7643 K.
文摘Generation characteristics of vacuum discharge plasma are very important for the applied research of metal plasma. The vacuum discharge electrode configuration and the cathode material affect the generation characteristics of the metal plasma which consists of metal ions coming from cathode and generated by vacuum discharge. In this research, the generation characteristics of the metal plasma generated by vacuum discharge are discussed for four patterns of electrode configurations, i.e. cone-mesh electrode setup, cone-cross line electrode setup, cone-line electrode setup and cone-ring electrode setup. Characteristics of the metal plasma, such as elec- tron density, electron temperature, space potential, ion energy, are measured by the probe method for discussing the impacts of different electrode configurations on the density of generated metal plasma. Moreover, the diffusion velocities of the metal plasma are measured for cathode materials of Pb, Al, and Cu, respectively. The experimental results indicate that the plasma generated by the discharge of cone-ring electrode configuration possesses the maximum density and the metal plasma generated by the Al cathode possesses the fastest diffusion velocity and the highest kinetic energy.
文摘he present paper covers tlie preparation and isolation of a series of monosub-stituted molybdophosphates Na_5 [PZ(H_2O)Mo_11 O_39]· 5H_2O (Z=Mn ̄2+, Co ̄2+,Ni ̄2+, Cu ̄2+, Zn ̄2+)by an improved method. These complexes were characterized byfull elemental analysis, IR spectra and UV-Vis. The studies show that the pre-pared products still keep Keggin structure and the substituting metal would belooated in coordination site. Based on this, their some pysico-cliemical propertiesrelated with their catalytic beliaviour,such as thermal stability and acidity proper-ty, were studied.
基金supported by the Importation and Development of High-caliber Talents Project of Beijing Municipal Institutions(No.IT&TCD201304115)
文摘Reduction of error due to the influence of temperature on the quartz flexible accelerometer without any heating device is a difficult task, and is also a tendency for research and application. In this paper, static and dynamic temperature compensation models are established in order to reduce the temperature influence on accelerometer measurement accuracy. Combined with the experiment data, the relationship between the accelerometer output accuracy, temperature and the magnitude of acceleration is analyzed. The data collected from the temperature experiment show that output value of the accelerometer varies with temperature. The method of uniaxial quadrature experiment is adopted and the accelerometer output value is gauged at temperature ranging from-20℃ to 50℃. Having used the static and the dynamic temperature compensation models, the accelerometer temperature error compensation experiment is conducted and the compensated errors by the two models are analyzed. The result shows that the compensated value meets the technical requirements. Two technical indicators, the zero bias K0 and the scaling factor K1, which are used to measure the degree of accelerometers, are both improved and their fluctuation ranges are reduced.