The effects of nutrients on the fluorescence characteristics and biochemical composition of marine diatom Thalassiosira pseudonana 3H in light and dark cycles were investigated with continuous culture. The results sho...The effects of nutrients on the fluorescence characteristics and biochemical composition of marine diatom Thalassiosira pseudonana 3H in light and dark cycles were investigated with continuous culture. The results show that with the increase of nutrient deficiency, the ratio of enhanced fluorescence to fluorescence (Fd/F), cellular chloropyll-a and protein content of the algae decline, but the fluorescence yield (F/Chl) , DCMU enhanced fluorescence yield (Fd/Chl) , cellular carbohydrate content, carbohydrate/Chl, protein/Chl, carbohydrate/protein increase. The changing amplitude of each parameter is different at different nutrition status, sampling time and different light intensity.展开更多
To understand the effects of leaf physiological and morphological characteristics on δ13C of alpine trees, we examined leaf δ13C value, LA, SD, LNC, LPC, LKC, Chla+b, LDMC, LMA and Narea in one-year-old needles of P...To understand the effects of leaf physiological and morphological characteristics on δ13C of alpine trees, we examined leaf δ13C value, LA, SD, LNC, LPC, LKC, Chla+b, LDMC, LMA and Narea in one-year-old needles of Picea schrenkiana var. tianschanica at ten points along an altitudinal gradient from 1420 m to 2300 m a.s.l. on the northern slopes of the Tianshan Mountains in northwest China. Our results indicated that all the leaf traits differed significantly among sampling sites along the altitudinal gradient(P<0.001). LA, SD, LPC, LKC increased linearly with increasing elevation, whereas leaf δ13C, LNC, Chla+b, LDMC, LMA and Narea varied non-linearly with changes in altitude. Stepwise multiple regression analyses showed that four controlled physiological and morphological characteristics influenced the variation of δ13C. Among these four controlled factors, LKC was the most profound physiological factor that affected δ13C values, LA was the secondary morphological factor, SD was the third morphological factor, LNC was the last physiological factor. This suggested that leaf δ13C was directly controlled by physiological and morphological adjustments with changing environmental conditions due to the elevation.展开更多
Fine particulate matter(PM_(2.5))and ozone(O_(3))double high pollution(DHP)events have occurred frequently over China in recent years,but their causes are not completely clear.In this study,the spatiotemporal distribu...Fine particulate matter(PM_(2.5))and ozone(O_(3))double high pollution(DHP)events have occurred frequently over China in recent years,but their causes are not completely clear.In this study,the spatiotemporal distribution of DHP events in China during 2013–20 is analyzed.The synoptic types affecting DHP events are identified with the Lamb–Jenkinson circulation classification method.The meteorological and chemical causes of DHP events controlled by the main synoptic types are further investigated.Results show that DHP events(1655 in total for China during 2013–20)mainly occur over the North China Plain,Yangtze River Delta,Pearl River Delta,Sichuan Basin,and Central China.The occurrence frequency increases by 5.1%during 2013–15,and then decreases by 56.1%during 2015–20.The main circulation types of DHP events are“cyclone”and“anticyclone”,accounting for over 40%of all DHP events over five main polluted regions in China,followed by southerly or easterly flat airflow types,like“southeast”,“southwest”,and“east”.Compared with non-DHP events,DHP events are characterized by static or weak wind,high temperature(20.9℃ versus 23.1℃)and low humidity(70.0%versus 64.9%).The diurnal cycles of meteorological conditions cause PM_(2.5)(0300–1200 LST,Local Standard Time=UTC+8 hours)and O_(3)(1500–2100 LST)to exceed the national standards at different periods of the DHP day.Three pollutant conversion indices further indicate the rapid secondary conversions during DHP events,and thus the concentrations of NO_(2),SO_(2) and volatile organic compounds decrease by 13.1%,4.7%and 4.4%,respectively.The results of this study can be informative for future decisions on the management of DHP events.展开更多
Spinel exsolution is widespread in titanomagnetite from the Fe-Ti oxide gabbro of the Panzhihua intrusion, Emeishan Large Igneous Province, SW China. However, little research has been conducted into the implications o...Spinel exsolution is widespread in titanomagnetite from the Fe-Ti oxide gabbro of the Panzhihua intrusion, Emeishan Large Igneous Province, SW China. However, little research has been conducted into the implications of patterns in the mineralogical characteristics of the spinel for spatial variation in the controls on the exsolution mechanism and, hence, the formation process of the ore deposit. This study selected the Lanjiahuoshan Ore Block in the Panzhihua V-Ti magnetite deposit to explore this issue, systematically studying exsolution textures in the titanomagnetite through petrographic observation and the integrated use of in-situ microanalysis. The results show that the exsolved spinel gradually becomes finer-grained and less abundant from the center to edge and the bottom to top of the ore bodies. Compositionally, there is an inverse correlation between the size of exsolved spinel grains and their Mg# value. In addition, there is compositional zonation in the spinel interiors, with a gradual increase in the Mg content and decrease in Fe content from the core to the rim. The analysis suggests that fractional crystallization of ferrotitanium magma with a high oxygen fugacity in a shallow magma chamber caused compositional differences in the primary magnetite solid solution in different parts of the Panzhihua intrusion. Additionally, the thermal evolution of the magnetite solid solution differed in different parts of orebody, bringing about variations in spinel development. Together, these effects resulted in spatial variation in the abundance, grain size, and morphology of spinel in different parts of the orebody and intrusion that follows an identifiable distribution law. Furthermore, the compositional zonation of exsolved spinels reflects the rapid growth of exsolution features in a high-temperature environment. Thus, the size, morphology, abundance, and composition of spinel exsolution features in titanomagnetite provide a valuable petrogenetic tool for estimating the maturity and formational environment of the deposit.展开更多
A multilayer tungsten carbide particle(WCp)-reinforced Ni-based alloy coating was fabricated on a steel substrate using vacuum cladding technology.The morphology,microstructure,and formation mechanism of the coating...A multilayer tungsten carbide particle(WCp)-reinforced Ni-based alloy coating was fabricated on a steel substrate using vacuum cladding technology.The morphology,microstructure,and formation mechanism of the coating were studied and discussed in different zones.The microstructure morphology and phase composition were investigated by scanning electron microscopy,optical microscopy,X-ray diffraction,and energy-dispersive X-ray spectroscopy.In the results,the coating presents a dense and homogeneous microstructure with few pores and is free from cracks.The whole coating shows a multilayer structure,including composite,transition,fusion,and diffusion-affected layers.Metallurgical bonding was achieved between the coating and substrate because of the formation of the fusion and diffusion-affected layers.The Ni-based alloy is mainly composed of y-Ni solid solution with finely dispersed Cr7C3/Cr(23)C6,CrB,and Ni+Ni3Si.WC particles in the composite layer distribute evenly in areas among initial Ni-based alloying particles,forming a special three-dimensional reticular microstructure.The macrohardness of the coating is HRC 55,which is remarkably improved compared to that of the substrate.The microhardness increases gradually from the substrate to the composite zone,whereas the microhardness remains almost unchanged in the transition and composite zones.展开更多
The analysis of cutting regularity is provided through using and comparing two typical cooling liquids. It is proved that cutting regularity is greatly affected by cooling liquid's washing ability. Discharge characte...The analysis of cutting regularity is provided through using and comparing two typical cooling liquids. It is proved that cutting regularity is greatly affected by cooling liquid's washing ability. Discharge characteristics and theoretic analysis between two electrodes are also discussed based on discharge waveform. By using composite cooling liquid which has strong washing ability, the efficiency in the first stable cutting phase has reached more than 200 mm^2/min, and the roughness of the surface has reached Ra〈0.8 μm after the fourth cutting with more than 50 mm^2/min average cutting efficiency. It is pointed out that cutting situation of the wire cut electrical discharge machine with high wire traveling speed (HSWEDM) is better than the wire cut electrical discharge machine with low wire traveling speed (LSWEDM) in the condition of improving the cooling liquid washing ability. The machining indices of HSWEDM will be increased remarkably by using the composite cooling liquid.展开更多
TiC reinforced titanium composites has been produced with different Al content and C content by XDTM. The results have shown that TiC particles are of two different morphologies f coarse dendritical primary TiC and sh...TiC reinforced titanium composites has been produced with different Al content and C content by XDTM. The results have shown that TiC particles are of two different morphologies f coarse dendritical primary TiC and short bar-shape eutectic TiC. Al content has great effects on the morphology of TiC. With the increasing of Al content, the morphology of primary TiC changes from coarse developed dendrite into short bar-shape or plate--shape TiC with 35%Al. Meanwhile, the structure of the matrix changes from single Ti to Ti and Ti3Al, and to Ti3Al and TiAl. However, the C content has no influence on the microstructure of matrix. When the C content is less than 1.2%, the dendrite TiC disappears and only short bar-shape or plate-shape TiC exists in the composites. In addition, the effect of he3t treatment on the morphology of TiC has also Studied.展开更多
Ni-W-P composite coatings reinforced by Ce O2 and Si O2 nano-particles on the surface of common carbon steels, were prepared by double pulse electrodeposition. The crystallization course was characterized by phase str...Ni-W-P composite coatings reinforced by Ce O2 and Si O2 nano-particles on the surface of common carbon steels, were prepared by double pulse electrodeposition. The crystallization course was characterized by phase structures, crystallinity, grain sizes and microstructures. The results indicate that as-deposited composite coating is amorphous. Whereas it turns into the crystalline structure with 98.25% crystallinity, and Ni3 P, Ni2 P and Ni5P2 alloy phases precipitate from structures at 400 °C. Thereafter, Ni2 P and Ni5P2 metastable alloy phases turn into Ni3 P stable alloy phase at 500 °C. The crystallization course of the composite coating has finished when being heat-treated at 700 °C. The average sizes of Ni grains increase with the rise of heat treatment temperature from400 °C to 700 °C. Ce O2 and Si O2 nano-particles deposited into Ni-W-P alloys can delay the crystallization course and habit the growth of alloy phases.展开更多
To investigate the ballistic performance and damage characteristics of quasi threedimensional(3D) needle-punched Cf/SiC composites prepared by chemical vapor infiltration(CVI),penetration experiments were conducte...To investigate the ballistic performance and damage characteristics of quasi threedimensional(3D) needle-punched Cf/SiC composites prepared by chemical vapor infiltration(CVI),penetration experiments were conducted by using 7.62 mm armor piercing incendiary(API).Macro and micro fracture morphologies were then observed on recycled targets.The results show that the protection coefficient of 3D Cf/SiC composites is 2.54.High porosity and many micro thermal stress cracks may directly lead to the lower ballistic performance.Flat fracture morphology was observed on the crater surface.The low dynamic fracture strength along layer direction may be attributed to the voids and microcracks caused by residual thermal stress.The damage characteristics of Cf/Si C composites include matrix cracking,fiber bundle cracking,interfacial debonding,fiber fracture,and fiber bundle pull-out.And interfacial debonding and fiber fracture may play major roles in energy absorption.展开更多
The flotation results of a phosphate ore are improved by replacing the conventional collectors of fatty acids with composite collectors. The synergistic effect on the froth characteristics in systems using composite c...The flotation results of a phosphate ore are improved by replacing the conventional collectors of fatty acids with composite collectors. The synergistic effect on the froth characteristics in systems using composite collectors has then been studied, and the concept of 'mixed hemimicellae' has been proposed in the adsorption of composite collectors at the air/solution interfaces.展开更多
In order to investigate the damage characteristic of ceramic-metal interpenetrating phase composite(IPC) under dynamic loading, uniaxial dynamic compression was performed to characterize the failure of SiC/Al compos...In order to investigate the damage characteristic of ceramic-metal interpenetrating phase composite(IPC) under dynamic loading, uniaxial dynamic compression was performed to characterize the failure of SiC/Al composite with 15% porosity using a modifi ed Split Hopkinson Pressure Bar(SHPB). High speed photography was used to capture the failure procedure and set up the relationship between deformation and real stress. The deformation control technology was used to obtain collected samples in different deformations under dynamic loading. Micro CT technology was utilized to acquire real damage distribution of these specimens. Moreover, SEM was employed in comparing the damage characteristics in IPC. A summary of the available experimental results showed that IPC without lateral confi nement formed double cones. The different features compared with ceramic materials without restraint was shown to be the result of the lateral restraint effect provided by metal phase to ceramics skeleton.展开更多
Concentrations of sixteen rare earth elements(REEs) in PM2.5 and potential-source samples, collected in Nanchang city in mid-September 2013, were determined by inductively coupled plasma mass spectrometry(ICP-MS)....Concentrations of sixteen rare earth elements(REEs) in PM2.5 and potential-source samples, collected in Nanchang city in mid-September 2013, were determined by inductively coupled plasma mass spectrometry(ICP-MS). The results showed that the concentrations of total REEs(ΣREE) ranged from 78.76 to 1351 ng/mg. The order of REEs in PM2.5 samples showed the anthropogenic effects, Ce and Eu were affected more than the other REEs according to the enrichment factors. The results of chondrite-normalized REEs patterns and characteristic parameters showed evident light REEs fractionation, and positive anomalies of Ce and Eu in PM2.5. The other non-local pollution sources affected the PM2.5 samples, according to the triangular diagram of La, Ce and Sm compositions and plot of ΣREE vs δEu. Moreover, plot of(La/Sm)N vs(Gd/Yb)N revealed the effects of local sources. In conclusion, the REEs in potential-source samples were close to the background of local soil, while the REEs in PM2.5 samples in Nanchang city were jointly affected by the investigated local sources and other non-local sources.展开更多
By using a ray method, a physical model that the backscattering of a tube is simplilied into reflection of a plane wave on layered media is suggested and reconstruction formulas of the parameters of a metallic tube co...By using a ray method, a physical model that the backscattering of a tube is simplilied into reflection of a plane wave on layered media is suggested and reconstruction formulas of the parameters of a metallic tube covered with sound-absorbing materials under the conditions of high frequency, fard field and thin tube are given. The internal and external radii of an aluminium tube filled by water or air and thickness of the covered material are reconstructed by using computer simulation and experimellts. The theoretical tesults obtained by this method are supported by experiments.展开更多
Using the new theoretical method managed by theory concerned with recurrent state and transient state obtains complete composite and switching characteristics of various kinds of sampling schemes, especially ISO 2859.
In this paper,we establish the model of a finite,irreducible non-periodic and ergodic Markov chain for the sampling scheme without discotinuing state,then calculate and analyse the composite characteristics of a three...In this paper,we establish the model of a finite,irreducible non-periodic and ergodic Markov chain for the sampling scheme without discotinuing state,then calculate and analyse the composite characteristics of a three-level skip-lot sampling scheme.展开更多
A study on ultrahigh strength steel plate subjected to novel thermo-mechanical control process was presented. The mechanical properties examination showed that the investigated steel exhibited excellent combination of...A study on ultrahigh strength steel plate subjected to novel thermo-mechanical control process was presented. The mechanical properties examination showed that the investigated steel exhibited excellent combination of ultra-high strength( 2 200 MPa) and toughness( 26 J). The microstructure of the experimental steel was observed by scanning electron microscope and transmission electron microscope. Desired martensitic lath with width of about 180- 250 nm was obtained. Nanostructured carbide precipitates with sizes of 20-50 nm,which contained Nb,Ti and Mo,were observed in the lath martensitic microstructure,and confirmed to be MC-type carbides with B1 structure by means of selected area electron diffraction.The compositional characteristics revealed by energy dispersive X-ray spectrometer mapping implied that the carbide forming elements Nb,Ti and Mo distributed in the precipitates evenly. Three-dimensional atom probe tomography reconstruction further indicated that Mo incorporated into the precipitates without enrichment in the carbide-matrix interface and probably substituted for Nb and Ti to form the( Nb,Ti,Mo) C carbides.展开更多
文摘The effects of nutrients on the fluorescence characteristics and biochemical composition of marine diatom Thalassiosira pseudonana 3H in light and dark cycles were investigated with continuous culture. The results show that with the increase of nutrient deficiency, the ratio of enhanced fluorescence to fluorescence (Fd/F), cellular chloropyll-a and protein content of the algae decline, but the fluorescence yield (F/Chl) , DCMU enhanced fluorescence yield (Fd/Chl) , cellular carbohydrate content, carbohydrate/Chl, protein/Chl, carbohydrate/protein increase. The changing amplitude of each parameter is different at different nutrition status, sampling time and different light intensity.
基金supported by the Major Research Plan of the National Natural Science Foundation of China (Grant No. Y411381001)the National Natural Science Foundation of China (Grant No. 91125025)the Postdoctoral Science Foundation of China (Grant No. 2013M532096)
文摘To understand the effects of leaf physiological and morphological characteristics on δ13C of alpine trees, we examined leaf δ13C value, LA, SD, LNC, LPC, LKC, Chla+b, LDMC, LMA and Narea in one-year-old needles of Picea schrenkiana var. tianschanica at ten points along an altitudinal gradient from 1420 m to 2300 m a.s.l. on the northern slopes of the Tianshan Mountains in northwest China. Our results indicated that all the leaf traits differed significantly among sampling sites along the altitudinal gradient(P<0.001). LA, SD, LPC, LKC increased linearly with increasing elevation, whereas leaf δ13C, LNC, Chla+b, LDMC, LMA and Narea varied non-linearly with changes in altitude. Stepwise multiple regression analyses showed that four controlled physiological and morphological characteristics influenced the variation of δ13C. Among these four controlled factors, LKC was the most profound physiological factor that affected δ13C values, LA was the secondary morphological factor, SD was the third morphological factor, LNC was the last physiological factor. This suggested that leaf δ13C was directly controlled by physiological and morphological adjustments with changing environmental conditions due to the elevation.
基金supported by the National Natural Science Foundation of China(Grant Nos.41830965 and 41905112)the Key Program of the Ministry of Science and Technology of the People’s Republic of China(Grant No.2019YFC0214703)+2 种基金the Hubei Natural Science Foundation(Grant No.2022CFB027)supported by the State Key Laboratory of Atmospheric Boundary Layer Physics and Atmospheric Chemistry(Grant No.LAPC-KF-2023-07)the Key Laboratory of Atmospheric Chemistry,China Meteorological Administration(Grant No.2023B08).
文摘Fine particulate matter(PM_(2.5))and ozone(O_(3))double high pollution(DHP)events have occurred frequently over China in recent years,but their causes are not completely clear.In this study,the spatiotemporal distribution of DHP events in China during 2013–20 is analyzed.The synoptic types affecting DHP events are identified with the Lamb–Jenkinson circulation classification method.The meteorological and chemical causes of DHP events controlled by the main synoptic types are further investigated.Results show that DHP events(1655 in total for China during 2013–20)mainly occur over the North China Plain,Yangtze River Delta,Pearl River Delta,Sichuan Basin,and Central China.The occurrence frequency increases by 5.1%during 2013–15,and then decreases by 56.1%during 2015–20.The main circulation types of DHP events are“cyclone”and“anticyclone”,accounting for over 40%of all DHP events over five main polluted regions in China,followed by southerly or easterly flat airflow types,like“southeast”,“southwest”,and“east”.Compared with non-DHP events,DHP events are characterized by static or weak wind,high temperature(20.9℃ versus 23.1℃)and low humidity(70.0%versus 64.9%).The diurnal cycles of meteorological conditions cause PM_(2.5)(0300–1200 LST,Local Standard Time=UTC+8 hours)and O_(3)(1500–2100 LST)to exceed the national standards at different periods of the DHP day.Three pollutant conversion indices further indicate the rapid secondary conversions during DHP events,and thus the concentrations of NO_(2),SO_(2) and volatile organic compounds decrease by 13.1%,4.7%and 4.4%,respectively.The results of this study can be informative for future decisions on the management of DHP events.
基金funded by the National Natural Science Foundation of China(Grant No.41172047)the Open Fund of the Key Laboratory of Ore Deposit Geochemistry(Institute of Geochemistry,Chinese Academy of Sciences,Guiyang),(Grant No.201308)the Open Fund of the Key Laboratory Metallogeny and Mineral Resource Assessment,Ministry of Land and Resources(Institute of Mineral Resources,Chinese Academy of Geological Sciences,Beijing)(Grant No.ZS1407)
文摘Spinel exsolution is widespread in titanomagnetite from the Fe-Ti oxide gabbro of the Panzhihua intrusion, Emeishan Large Igneous Province, SW China. However, little research has been conducted into the implications of patterns in the mineralogical characteristics of the spinel for spatial variation in the controls on the exsolution mechanism and, hence, the formation process of the ore deposit. This study selected the Lanjiahuoshan Ore Block in the Panzhihua V-Ti magnetite deposit to explore this issue, systematically studying exsolution textures in the titanomagnetite through petrographic observation and the integrated use of in-situ microanalysis. The results show that the exsolved spinel gradually becomes finer-grained and less abundant from the center to edge and the bottom to top of the ore bodies. Compositionally, there is an inverse correlation between the size of exsolved spinel grains and their Mg# value. In addition, there is compositional zonation in the spinel interiors, with a gradual increase in the Mg content and decrease in Fe content from the core to the rim. The analysis suggests that fractional crystallization of ferrotitanium magma with a high oxygen fugacity in a shallow magma chamber caused compositional differences in the primary magnetite solid solution in different parts of the Panzhihua intrusion. Additionally, the thermal evolution of the magnetite solid solution differed in different parts of orebody, bringing about variations in spinel development. Together, these effects resulted in spatial variation in the abundance, grain size, and morphology of spinel in different parts of the orebody and intrusion that follows an identifiable distribution law. Furthermore, the compositional zonation of exsolved spinels reflects the rapid growth of exsolution features in a high-temperature environment. Thus, the size, morphology, abundance, and composition of spinel exsolution features in titanomagnetite provide a valuable petrogenetic tool for estimating the maturity and formational environment of the deposit.
基金supported by the National Natural Science Foundation of China(No.51205178)the Natural Science Foundation of Gansu Province,China(No.1208RJZA189)the Doctor Fund Project of Lanzhou University of Technology
文摘A multilayer tungsten carbide particle(WCp)-reinforced Ni-based alloy coating was fabricated on a steel substrate using vacuum cladding technology.The morphology,microstructure,and formation mechanism of the coating were studied and discussed in different zones.The microstructure morphology and phase composition were investigated by scanning electron microscopy,optical microscopy,X-ray diffraction,and energy-dispersive X-ray spectroscopy.In the results,the coating presents a dense and homogeneous microstructure with few pores and is free from cracks.The whole coating shows a multilayer structure,including composite,transition,fusion,and diffusion-affected layers.Metallurgical bonding was achieved between the coating and substrate because of the formation of the fusion and diffusion-affected layers.The Ni-based alloy is mainly composed of y-Ni solid solution with finely dispersed Cr7C3/Cr(23)C6,CrB,and Ni+Ni3Si.WC particles in the composite layer distribute evenly in areas among initial Ni-based alloying particles,forming a special three-dimensional reticular microstructure.The macrohardness of the coating is HRC 55,which is remarkably improved compared to that of the substrate.The microhardness increases gradually from the substrate to the composite zone,whereas the microhardness remains almost unchanged in the transition and composite zones.
基金Provincial Key Laboratory of Precision and Micro-Manufacturing Technology of Jiangsu,China(No.Z0601-052-02).
文摘The analysis of cutting regularity is provided through using and comparing two typical cooling liquids. It is proved that cutting regularity is greatly affected by cooling liquid's washing ability. Discharge characteristics and theoretic analysis between two electrodes are also discussed based on discharge waveform. By using composite cooling liquid which has strong washing ability, the efficiency in the first stable cutting phase has reached more than 200 mm^2/min, and the roughness of the surface has reached Ra〈0.8 μm after the fourth cutting with more than 50 mm^2/min average cutting efficiency. It is pointed out that cutting situation of the wire cut electrical discharge machine with high wire traveling speed (HSWEDM) is better than the wire cut electrical discharge machine with low wire traveling speed (LSWEDM) in the condition of improving the cooling liquid washing ability. The machining indices of HSWEDM will be increased remarkably by using the composite cooling liquid.
文摘TiC reinforced titanium composites has been produced with different Al content and C content by XDTM. The results have shown that TiC particles are of two different morphologies f coarse dendritical primary TiC and short bar-shape eutectic TiC. Al content has great effects on the morphology of TiC. With the increasing of Al content, the morphology of primary TiC changes from coarse developed dendrite into short bar-shape or plate--shape TiC with 35%Al. Meanwhile, the structure of the matrix changes from single Ti to Ti and Ti3Al, and to Ti3Al and TiAl. However, the C content has no influence on the microstructure of matrix. When the C content is less than 1.2%, the dendrite TiC disappears and only short bar-shape or plate-shape TiC exists in the composites. In addition, the effect of he3t treatment on the morphology of TiC has also Studied.
基金Project(20806035)supported by the National Natural Science Foundation of ChinaProject(2009CI026)supported by the Back-up Personnel Foundation of Academic and Technology Leaders of Yunnan Province,ChinaProject(KKZ6200927001)supported by the Opening Fund of Key Laboratory of Inorganic Coating Materials,Chinese Academy of Sciences
文摘Ni-W-P composite coatings reinforced by Ce O2 and Si O2 nano-particles on the surface of common carbon steels, were prepared by double pulse electrodeposition. The crystallization course was characterized by phase structures, crystallinity, grain sizes and microstructures. The results indicate that as-deposited composite coating is amorphous. Whereas it turns into the crystalline structure with 98.25% crystallinity, and Ni3 P, Ni2 P and Ni5P2 alloy phases precipitate from structures at 400 °C. Thereafter, Ni2 P and Ni5P2 metastable alloy phases turn into Ni3 P stable alloy phase at 500 °C. The crystallization course of the composite coating has finished when being heat-treated at 700 °C. The average sizes of Ni grains increase with the rise of heat treatment temperature from400 °C to 700 °C. Ce O2 and Si O2 nano-particles deposited into Ni-W-P alloys can delay the crystallization course and habit the growth of alloy phases.
基金Funded by the National Natural Science Foundation of China(No.51271036)
文摘To investigate the ballistic performance and damage characteristics of quasi threedimensional(3D) needle-punched Cf/SiC composites prepared by chemical vapor infiltration(CVI),penetration experiments were conducted by using 7.62 mm armor piercing incendiary(API).Macro and micro fracture morphologies were then observed on recycled targets.The results show that the protection coefficient of 3D Cf/SiC composites is 2.54.High porosity and many micro thermal stress cracks may directly lead to the lower ballistic performance.Flat fracture morphology was observed on the crater surface.The low dynamic fracture strength along layer direction may be attributed to the voids and microcracks caused by residual thermal stress.The damage characteristics of Cf/Si C composites include matrix cracking,fiber bundle cracking,interfacial debonding,fiber fracture,and fiber bundle pull-out.And interfacial debonding and fiber fracture may play major roles in energy absorption.
文摘The flotation results of a phosphate ore are improved by replacing the conventional collectors of fatty acids with composite collectors. The synergistic effect on the froth characteristics in systems using composite collectors has then been studied, and the concept of 'mixed hemimicellae' has been proposed in the adsorption of composite collectors at the air/solution interfaces.
文摘In order to investigate the damage characteristic of ceramic-metal interpenetrating phase composite(IPC) under dynamic loading, uniaxial dynamic compression was performed to characterize the failure of SiC/Al composite with 15% porosity using a modifi ed Split Hopkinson Pressure Bar(SHPB). High speed photography was used to capture the failure procedure and set up the relationship between deformation and real stress. The deformation control technology was used to obtain collected samples in different deformations under dynamic loading. Micro CT technology was utilized to acquire real damage distribution of these specimens. Moreover, SEM was employed in comparing the damage characteristics in IPC. A summary of the available experimental results showed that IPC without lateral confi nement formed double cones. The different features compared with ceramic materials without restraint was shown to be the result of the lateral restraint effect provided by metal phase to ceramics skeleton.
基金Project supported by the National Natural Science Foundation of China(21477042,21377042)the Natural Science Foundation of Fujian Province(2016J01065)
文摘Concentrations of sixteen rare earth elements(REEs) in PM2.5 and potential-source samples, collected in Nanchang city in mid-September 2013, were determined by inductively coupled plasma mass spectrometry(ICP-MS). The results showed that the concentrations of total REEs(ΣREE) ranged from 78.76 to 1351 ng/mg. The order of REEs in PM2.5 samples showed the anthropogenic effects, Ce and Eu were affected more than the other REEs according to the enrichment factors. The results of chondrite-normalized REEs patterns and characteristic parameters showed evident light REEs fractionation, and positive anomalies of Ce and Eu in PM2.5. The other non-local pollution sources affected the PM2.5 samples, according to the triangular diagram of La, Ce and Sm compositions and plot of ΣREE vs δEu. Moreover, plot of(La/Sm)N vs(Gd/Yb)N revealed the effects of local sources. In conclusion, the REEs in potential-source samples were close to the background of local soil, while the REEs in PM2.5 samples in Nanchang city were jointly affected by the investigated local sources and other non-local sources.
文摘By using a ray method, a physical model that the backscattering of a tube is simplilied into reflection of a plane wave on layered media is suggested and reconstruction formulas of the parameters of a metallic tube covered with sound-absorbing materials under the conditions of high frequency, fard field and thin tube are given. The internal and external radii of an aluminium tube filled by water or air and thickness of the covered material are reconstructed by using computer simulation and experimellts. The theoretical tesults obtained by this method are supported by experiments.
文摘Using the new theoretical method managed by theory concerned with recurrent state and transient state obtains complete composite and switching characteristics of various kinds of sampling schemes, especially ISO 2859.
文摘In this paper,we establish the model of a finite,irreducible non-periodic and ergodic Markov chain for the sampling scheme without discotinuing state,then calculate and analyse the composite characteristics of a three-level skip-lot sampling scheme.
基金Item Sponsored by High Technology Research and Development Program of China(2012AA03A508)
文摘A study on ultrahigh strength steel plate subjected to novel thermo-mechanical control process was presented. The mechanical properties examination showed that the investigated steel exhibited excellent combination of ultra-high strength( 2 200 MPa) and toughness( 26 J). The microstructure of the experimental steel was observed by scanning electron microscope and transmission electron microscope. Desired martensitic lath with width of about 180- 250 nm was obtained. Nanostructured carbide precipitates with sizes of 20-50 nm,which contained Nb,Ti and Mo,were observed in the lath martensitic microstructure,and confirmed to be MC-type carbides with B1 structure by means of selected area electron diffraction.The compositional characteristics revealed by energy dispersive X-ray spectrometer mapping implied that the carbide forming elements Nb,Ti and Mo distributed in the precipitates evenly. Three-dimensional atom probe tomography reconstruction further indicated that Mo incorporated into the precipitates without enrichment in the carbide-matrix interface and probably substituted for Nb and Ti to form the( Nb,Ti,Mo) C carbides.