Aluminum killed cold rolled steel used for automobiles was welded in this paper by using CO 2 laser with wavelength 10.6μm.The experiment shows that high quality of welding can be realized at welding speed of 4 500m...Aluminum killed cold rolled steel used for automobiles was welded in this paper by using CO 2 laser with wavelength 10.6μm.The experiment shows that high quality of welding can be realized at welding speed of 4 500mm/min by optimizing the parameters.The strength and hardness of laser welded joints for aluminum killed cold rolled steel increased compared to those of the base metal while the formability decreased.Forming limit diagram of joint material indicated that the laser weld seam should avoid the maximum deformation area of automobile parts during the designing period for the position of weld seam.展开更多
A cold rolled dual phase (DP) steel with the C-Si-Mn alloy system was trial-produced in the laboratory, utilizing a Gleeble-3800 thermal simulator. The effects of continuous annealing parameters on the mechanical pr...A cold rolled dual phase (DP) steel with the C-Si-Mn alloy system was trial-produced in the laboratory, utilizing a Gleeble-3800 thermal simulator. The effects of continuous annealing parameters on the mechanical properties and microstructures of the DP steel were investigated by mechanical testing and microstructure observation. The results show that soaking between 760 and 820℃ for more than 80 s, rapid cooling at the rate of more than 30℃/s from the quenching temperature between 620 and 680℃, and overaging lower than 300℃ are beneficial for the mechanical properties of DP steels. An appropriate proportion of the two phases is one of the key factors for the favorable properties of DP steels. If the volume fraction of martensite and, thereby, free dislocations are deficient, the tensile strength and n value of DP steels will decrease, whereas, the yield strength will increase. But if the volume fraction of martensite is excessive to make it become a dominant phase, the yield and tensile strength will increase, whereas, the elongation will decrease obviously. When rapid cooling rate is not fast enough, pearlite or cementite will appear, which will degrade the mechanical properties. Even though martensite is sufficient, if it is decomposed in high temperature tempering, the properties will he unsatisfied.展开更多
TWIP steels with 70% cold-rolled reduction were heated at 500, 600, 700, 800, 900, 1000, and 1100 ℃. Then, the properties before and after heating were examined through tensile and hardness experiments. The microstru...TWIP steels with 70% cold-rolled reduction were heated at 500, 600, 700, 800, 900, 1000, and 1100 ℃. Then, the properties before and after heating were examined through tensile and hardness experiments. The microstructures were also analyzed by optical microscopy and transmission electron microscopy. The relationship between the properties and microstructure was examined as well. Finally, the evolution process of cold-rolled microstructures during heating was discussed in detail. Moreover, some conclusions can be drawn, and the heating evolution characteristics are described.展开更多
The microstructure evolution of different cold rolling reductions (from 0 to 81.6%) was studied by SEM (scanning electron microscopy) and TEM (transmission electron microscope). The study showed that the orienta...The microstructure evolution of different cold rolling reductions (from 0 to 81.6%) was studied by SEM (scanning electron microscopy) and TEM (transmission electron microscope). The study showed that the orientation multiplicity of pearlitic lamellas resulted in inhomogeneous deformation of different pearlitic lamellas, and with the increase of reduction, the microstructure underwent a course of "homogeneity → inhomogeneity → homogeneity". The result of XRD (X-ray diffraction) analysis indicated that cementite did not decompose and dissolve into ferrite; the results of the mechanical property test suggested that the relationship between Rp0.2 (yield strength) and ε (true strain) was in good agreement with Hollomon relationship. With the equation Rp0.2 = 1465ε^0.18, the yield strength of the steel in different reductions could be well predicted.展开更多
This study has evaluated the effect of different levels of cold rolling(from 0 to 50%)on the microstructural,magnetic,and mechanical properties and the corrosion behavior of 316L austenitic stainless steel in Na Cl...This study has evaluated the effect of different levels of cold rolling(from 0 to 50%)on the microstructural,magnetic,and mechanical properties and the corrosion behavior of 316L austenitic stainless steel in Na Cl(1 mol/L)+H_2SO_4(0.5 mol/L)solution.Microstructural examinations using optical microscopy revealed the development of a morphological texture from coaxial to elongated grains during the cold-rolling process.Phase analysis carried out on the basis of X-ray diffraction confirmed the formation of the ferromagneticα′-martensite phase under the stresses applied during cold rolling.This finding is in agreement with magnetic measurements using a vibrating sample magnetometer.Mechanical properties determined by tensile and Vickers microhardness tests demonstrated an upward trend in the hardness-to-yield strength ratio with increasing cold-rolling percentage,representing a reduction in the material’s work-hardening ability.Uniform and localized corrosion parameters were estimated via potentiodynamic polarization corrosion tests and electrochemical impedance spectroscopy.In contrast to the uniform corrosion,wherein the corrosion current density increased with increasing cold-working degree because of the high density of microstructural defects,the passive potential range and breakdown potential increased by cold working,showing greater resistance to pit nucleation.Although pits were formed,the cold-rolled material repassivation tendency decreased because of the broader hysteresis anodic loop,as confirmed experimentally by observation of the microscopic features after electrochemical cyclic polarization evaluations.展开更多
Single cold rolling and double cold rolling were applied to hot rolled strips with different reduction ratios. The evolutions of { 100}, { 111} and Goss face texture during double rolling were investigated by comparin...Single cold rolling and double cold rolling were applied to hot rolled strips with different reduction ratios. The evolutions of { 100}, { 111} and Goss face texture during double rolling were investigated by comparing the orientation distribution function (ODF) of the double rolled sample with that of the single rolled one. The double cold rolling texture is characterized by a higher γ-texture and a lower α-texture, and the { 111}〈112〉 component is improved remarkably. Based on the TEM observation and mechanical properties test, it is found that the reduction ratio assignment significantly affects the texture variation, as-annealing microstructures, and properties of the double cold rolled samples. These results may provide a theoretical guide for the industrial production of double cold rolled IF steel.展开更多
The influence of cold rolling reduction on microstructure and mechanical properties of the twinning induced plasticity(TWIP) steel with a chemical composition of Fe-20Mn-3Si-3Al-0.045 C has been investigated.Tensile t...The influence of cold rolling reduction on microstructure and mechanical properties of the twinning induced plasticity(TWIP) steel with a chemical composition of Fe-20Mn-3Si-3Al-0.045 C has been investigated.Tensile tests were carried out to explore the mechanical properties of TWIP steel with different cold rolling reductions.The microstructures were observed by optical microscopy and transmission electron microscopy(TEM).The misorientation and the development of recrystallization texture in TWIP steel sheets were investigated by Electron Back Scatter Diffraction(EBSD) technique.The results indicated that the steel exhibited attractively mechanical properties when cold rolling reduction was about 10%.The tensile strength of the steel with a rolling reduction of 10%is higher than 900 MPa and the yield strength is about 800 MPa,while the elongation is above 35%.The microstructure is composed of austenitic matrix and deformation twins at room temperature,at the same time,a significant amount of deformation twins,stacking faults and dislocations are observed by TEM.TEM observations showed the presence of deformation twinning in the sample at low rolling reduction.As the strain increases the volume fraction of twins increases.Mechanical twins play a dominant role during deformation and result in excellent mechanical properties for the investigated steel.By TEM observation,the possible deformation mechanisms can be suggested as:with the increasing strain,formation of the twin will gradually play a more important role during deformation.The interaction between twins and dislocations enhances the strain hardening rate in the sample.Consequently,the necking is delayed and a good ductility is obtained.Twins were always observed in the region with high density of dislocation and faults,suggesting that the interaction among blocked dislocations and faults as well as deformation twins promote the increase in material strength.EBSD observation showed that the textures has evolved according to the following trend:the brass orientation {110}〈112〉and Goss orientation {110}〈001〉are dominant at every strain level,those intensities increase with increasing strain,while with the increase of the strain level,the change of S orientation {123}〈634〉was not obviously.展开更多
The effects of annealing temperature(with the annealing time being constant at 1 h) on the microstructure, ordering, residual stress, mechanical properties, and subsequent cold rolling workability of Fe-6.5wt%Si ele...The effects of annealing temperature(with the annealing time being constant at 1 h) on the microstructure, ordering, residual stress, mechanical properties, and subsequent cold rolling workability of Fe-6.5wt%Si electrical steel with columnar grains were investigated, where the steel was warm rolled at 500℃ with a reduction of 95%. The results show that recrystallization began to occur in the sample annealed at 575℃ and that full recrystallization occurred in the sample annealed at 625℃. When the annealing temperature was 500℃ or greater, the extent of reordering in the sample was high, which reduced the room-temperature plasticity. However, annealing at temperatures below 300℃ did not significantly reduce the residual tensile stress on the edge of the warm rolled samples. Considering the comprehensive effects of annealing temperature on the recrystallization, reordering, residual stress, and mechanical properties of the warm rolled Fe-6.5wt%Si electrical steel with columnar grains, the appropriate annealing temperature range is 300℃-400℃. Unlike the serious edge cracks that appeared in the sample after direct cold rolling, the annealed samples could be cold rolled to a total reduction of more than 71.4% without the formation of obvious edge cracks, and bright-surface Fe-6.5wt%Si electrical steel strips with a thickness less than 0.1 mm could be fabricated by cold rolling.展开更多
The tensile strength and ductility of a high nitrogen nickel-free austenitic stainless steel with solution and cold rolling treatment were investigated by performing tensile tests at different strain rates and at room...The tensile strength and ductility of a high nitrogen nickel-free austenitic stainless steel with solution and cold rolling treatment were investigated by performing tensile tests at different strain rates and at room temperature. The tensile tests demonstrated that this steel exhibits a significant strain rate and cold rolling dependence of the tensile strength and ductility.With the increase of the strain rate from 10^-4s^-1to 1 s^-1, the yield strength and ultimate tensile strength increase and the uniform elongation and total elongation decrease. The analysis of the double logarithmic stress–strain curves showed that this steel exhibits a two-stage strain hardening behavior, which can be well examined and analyzed by using the Ludwigson equation. The strain hardening exponents at low and high strain regions(n2and n1) and the transition strain(εL) decrease with increasing strain rate and the increase of cold rolling RA. Based on the analysis results of the stress–strain curves, the transmission electron microscopy characterization of the microstructure and the scanning electron microscopy observation of the deformation surfaces, the significant strain rate and cold rolling dependence of the strength and ductility of this steel were discussed and connected with the variation in the work hardening and dislocation activity with strain rate and cold rolling.展开更多
Effect of controlled rolling and cooling process on the mechanical properties of low carbon cold forging steel was investigated for different processing parameters of a laboratory hot rolling mill. The results show th...Effect of controlled rolling and cooling process on the mechanical properties of low carbon cold forging steel was investigated for different processing parameters of a laboratory hot rolling mill. The results show that the specimens with fast cooling after hot rolling exhibit very good mechanical properties, and the improvement of the mechanical properties can be attributed mainly to the ferrite-grain refinement. The mechanical properties increase with decreasing final cooling temperature within the range from 670 ℃ to 570 ℃ due to the finer interlamellar spacing of pearlite colony. The specimen with fast cooling after low temperature rolling shows the highest values of the mechanical properties. The effect of the ferrite grain size on the mechanical properties was greater than that of pearlite morphology in the present study. The mechanical properties of specimens by controlled rolling and cooling process without thermal treatment were greatly superior to that of the same specimens by the conventional rolling, and their tensile strength reached 490 MPa grade even in the case of low temperature rolling without controlled rolling. It might be expected to realize the substitution medium-carbon by low-carbon for 490 MPa grade cold forging steel with controlled rolling and cooling process.展开更多
The microstructure evolution of 1 000 MPa cold rolled dual-phase (DP) steel at the initial heating stages of the continuous annealing process was analyzed. The effects of different overaging temperatures on the micros...The microstructure evolution of 1 000 MPa cold rolled dual-phase (DP) steel at the initial heating stages of the continuous annealing process was analyzed. The effects of different overaging temperatures on the microstructures and mechanical properties of 1 000 MPa cold rolled DP steel were investigated using a Gleeble-3500 thermal/mechanical simulator. The experimental results show that ferrite recovery and recrystallization, pearlite dissolution and austenite nucleation and growth take place in the annealing process of ultra-high strength cold rolled DP steel. When being annealed at 800 ℃ for 80 s, the tensile strength and total elongation of DP steel can reach 1 150 MPa and 13%, respectively. The microstructure of DP steel mainly consists of a mixture of ferrite and martensite. The steel exhibits low yield strength and continuous yielding which is commonly attributed to mobile dislocations introduced during cooling process from the intercritical annealing temperature.展开更多
With a complicated composition, large rolling sludge has been a focal point concerning neither at home nor abroad have any technologies suitable for bulk utilization of stainless steel cold- production and serious dam...With a complicated composition, large rolling sludge has been a focal point concerning neither at home nor abroad have any technologies suitable for bulk utilization of stainless steel cold- production and serious damage to the environment, stainless steel cold- environmental protection for stainless steel enterprises. Up to now, come into being that are not only proper, safe and economical but also rolling sludge. Based on the characteristics of the stainless steel cold- rolling sludge, orthogonal experiments were carried out on pellet proportioning and high-temperature roasting, and major metallurgical properties of sludge pellets were also tested. As the results show, pellets with 30% addition of cold-rolling sludge are qualified regarding their compressive strength, chemical composition and major metallurgical properties. No adverse impact happens to the blast furnace operation when sludge pellets account for 10% of the blast furnace raw materials. Therefore, the technical route applied in this paper is proved simple, feasible and environmentally friendly for cold-rolling sludge treatment.展开更多
The influence of cold rolling reduction on microstructure and mechanical properties of the TWIP (ttwinning induced plasticity) steel was investigated. The results' indicated that the steel had better comprehensive ...The influence of cold rolling reduction on microstructure and mechanical properties of the TWIP (ttwinning induced plasticity) steel was investigated. The results' indicated that the steel had better comprehensive mechanical properties when cold rolling reduction was about 65.0% and the annealing temperature was 1000℃. The tensile strength of the steel is about 640MPa and the yield strength is higher than 255MPa, while the elongation is' above 82%. The microstructure is composed of austenitic matrix and annealing twins at room temperature, at the same time, a significant amount of annealing twins and stacking faults' are observed by transmission electron microscopy (TEM). Mechanical twins play a dominant role during deformation, and result in exceUent mechanical properties.展开更多
This study researches cold rolled ultra high strength martensitic steel processed by water quenching. It is found that both the quenching and overageing temperatures greatly influence the mechanical properties of mart...This study researches cold rolled ultra high strength martensitic steel processed by water quenching. It is found that both the quenching and overageing temperatures greatly influence the mechanical properties of martensitic steel. A tensile strength of 1500 MPa can be obtained from 0.2% C-1.8% Mn steel by soaking at 840℃,quenching at 700℃ and overageing at 200℃ for several minutes. The continuous cooling transformation (CCT) diagram reveals that full martensite can be obtained at a cooling rate of 100℃/s or higher; and at a cooling rate of 3 - 10℃/s,austenite barely decomposes at 700℃. For steel with 0.2% carbon and less manganese, austenite decomposition occurs before it is cooled to 700℃ at a cooling rate of 3 - 10℃/s, which leads to lower tensile strength. It is possible to reduce the manganese content of the 1500 MPa martensitic steel by increasing the quenching temperature. To increase the quenching temperature,the control of flatness during water quenching becomes a major concern.展开更多
Cold-rolled advanced high-strength steel sheets have become the material of choice for the automotive industry because of their unique attributes of high strength and balanced mechanical properties.High-hydrogen gas j...Cold-rolled advanced high-strength steel sheets have become the material of choice for the automotive industry because of their unique attributes of high strength and balanced mechanical properties.High-hydrogen gas jet cooling and water quenching are the most commonly used ultrafast cooling technologies for producing martensite-containing high-strength steel sheets.The water quenching technology ensures the fastest industrial cooling rate of 1 000 K/s;therefore,it has the highest potential with respect to saving alloys.In this study,the water quenching of a C-Mn-containing steel sheet is simulated during continuous annealing to investigate the effect of water quenching and tempering parameters on its mechanical properties.The results reveal that at low quenching temperatures,the strength of the steel sheet decreases as the soaking temperature increases.However,at high quenching temperatures,a high soaking temperature corresponds to increased strength after quenching,regardless of whether the material was austenitized in the single austenite zone or the inter-critical zone.Therefore,a high quenching temperature always results in a high strength and a high yield ratio after quenching.Low-temperature overaging(tempering) considerably influences the yield strength and yield ratio,and the extent of this influence is correlated with the soaking temperature.展开更多
Many advanced technologies have been applied in developing the automatic measuring device for testing transverse thickness difference of cold-rolling steel sheet,such as the technologies of automatic control,sensor me...Many advanced technologies have been applied in developing the automatic measuring device for testing transverse thickness difference of cold-rolling steel sheet,such as the technologies of automatic control,sensor measurement,marking identification,photographic location,computer application and information transmission.This measuring device can measure the transverse thickness difference of the steel plate accurately and quickly,with a high detection level of automation.It is an effective detection equipment for transverse thickness control of steel plate.Horizontal width of steel plate measuring 0.8-1.4 m, horizontal measurement point positioning accuracy±0.02 mm,thickness range 0.2-2.0 mm, measurement accuracy within±1μm.展开更多
Cold-rolled martensitic steel sheets produced on continuous annealing lines with water quenching facility,have advantages of high strength and low alloying element contents.These are in good accordance with the trend ...Cold-rolled martensitic steel sheets produced on continuous annealing lines with water quenching facility,have advantages of high strength and low alloying element contents.These are in good accordance with the trend of light-weighting and fuel saving for automotive steel.In this article,a cold-rolled martensitic steel is studied to investigate the effect of annealing parameters on its mechanical properties.It is found that the quenching temperature and the slow cooling speed as well as the overageing temperature have significant influence on the strength of the experimental steel.The temperature zone at which the austenite decomposition is slow or has not started may be chosen as the quenching temperature to ensure the steel’s strength stability.The slow cooling speed also influences the steel’s strength greatly.A high cooling rate will lead to significantly higher strength.Tempering would decrease the steel’s tensile strength but would increase its yield strength.展开更多
Cold rolled martensitic sheet steels are achieving more and more applications in car-making because of their ultra-high strength and potential for weight reduction. The relatively low plasticity of ultra-high strength...Cold rolled martensitic sheet steels are achieving more and more applications in car-making because of their ultra-high strength and potential for weight reduction. The relatively low plasticity of ultra-high strength martensitic steels might be a drawback for the applications in the aspects of forming and safety protection function and should be significantly noted. A 1 500 MPa grade cold rolled martensitic sheet steel has been studied to investigate the bendability at 90 degree bending and impact toughness as well as fracture surface morphology at various temperatures. Some discussions have been made basing upon the experiment data to get some understanding on the performance of the materials under various conditions and on how to make use of this kind of ultra high strength steel properly.展开更多
In accordance with experimental results about the annealing microstructure and texture of cold-rolled deep- drawing sheet based on the compact strip production (CSP) process, a two-dimensional cellular automation si...In accordance with experimental results about the annealing microstructure and texture of cold-rolled deep- drawing sheet based on the compact strip production (CSP) process, a two-dimensional cellular automation simulation model, considering real space and time scale, was established to simulate recrystallization and grain growth during the actual batch annealing process. The simulation results show that pancaked grains form during recrystallization. (111} advantageous texture components become the main parts of the recrystallization texture. After grain growth, the pancaked grains coarsen gradually. The content of (111} advantageous texture components in the annealing texture increases from 55vo1% to 65vo1%; meanwhile, the contents of {112}〈110〉 and {100}〈110〉 texture components decrease by 4% and 8%, respectively, compared with the recrystallization texture. The simulation results of microstructure and texture evolution are also consistent with the experimental ones, proving the accuracy and usefulness of the model.展开更多
Cold-rolled martensitic steel sheets are becoming widely applied in the automotive industry because of their ultra-high strength,which may result in satisfactory weight reduction. The grades of martensitic steel sheet...Cold-rolled martensitic steel sheets are becoming widely applied in the automotive industry because of their ultra-high strength,which may result in satisfactory weight reduction. The grades of martensitic steel sheets are classified based on their tensile strength,which ranges from 980 to 1 700 MPa. The main applications include a series of structural parts of uniform cross-section or simple shape,such as bumper beams,door beams and door sills,etc. The study and development of cold-rolled martensitic steel sheets date back to 2007 in Baosteel,and some grades became commercially available in 2009. By 2015,Baosteel had commercially supplied thousands of tons of these steel sheets with tensile strength up to 1 400 MPa. Currently,1 500 MPa martensitic steel sheet is commercially available and 1 700 MPa martensitic steel sheet has been successfully produced. The process technology and application guides of Basoteel 's cold-rolled martensitic steels are summarized and analyzed in order to assist ongoing research and ensure correct applications of these ultra-high strength steel sheets.展开更多
文摘Aluminum killed cold rolled steel used for automobiles was welded in this paper by using CO 2 laser with wavelength 10.6μm.The experiment shows that high quality of welding can be realized at welding speed of 4 500mm/min by optimizing the parameters.The strength and hardness of laser welded joints for aluminum killed cold rolled steel increased compared to those of the base metal while the formability decreased.Forming limit diagram of joint material indicated that the laser weld seam should avoid the maximum deformation area of automobile parts during the designing period for the position of weld seam.
文摘A cold rolled dual phase (DP) steel with the C-Si-Mn alloy system was trial-produced in the laboratory, utilizing a Gleeble-3800 thermal simulator. The effects of continuous annealing parameters on the mechanical properties and microstructures of the DP steel were investigated by mechanical testing and microstructure observation. The results show that soaking between 760 and 820℃ for more than 80 s, rapid cooling at the rate of more than 30℃/s from the quenching temperature between 620 and 680℃, and overaging lower than 300℃ are beneficial for the mechanical properties of DP steels. An appropriate proportion of the two phases is one of the key factors for the favorable properties of DP steels. If the volume fraction of martensite and, thereby, free dislocations are deficient, the tensile strength and n value of DP steels will decrease, whereas, the yield strength will increase. But if the volume fraction of martensite is excessive to make it become a dominant phase, the yield and tensile strength will increase, whereas, the elongation will decrease obviously. When rapid cooling rate is not fast enough, pearlite or cementite will appear, which will degrade the mechanical properties. Even though martensite is sufficient, if it is decomposed in high temperature tempering, the properties will he unsatisfied.
基金Funded by the National Natural Science Foundation o f China(51201154)the Natural Science Foundation of Shanxi Province(2014011015-1)
文摘TWIP steels with 70% cold-rolled reduction were heated at 500, 600, 700, 800, 900, 1000, and 1100 ℃. Then, the properties before and after heating were examined through tensile and hardness experiments. The microstructures were also analyzed by optical microscopy and transmission electron microscopy. The relationship between the properties and microstructure was examined as well. Finally, the evolution process of cold-rolled microstructures during heating was discussed in detail. Moreover, some conclusions can be drawn, and the heating evolution characteristics are described.
文摘The microstructure evolution of different cold rolling reductions (from 0 to 81.6%) was studied by SEM (scanning electron microscopy) and TEM (transmission electron microscope). The study showed that the orientation multiplicity of pearlitic lamellas resulted in inhomogeneous deformation of different pearlitic lamellas, and with the increase of reduction, the microstructure underwent a course of "homogeneity → inhomogeneity → homogeneity". The result of XRD (X-ray diffraction) analysis indicated that cementite did not decompose and dissolve into ferrite; the results of the mechanical property test suggested that the relationship between Rp0.2 (yield strength) and ε (true strain) was in good agreement with Hollomon relationship. With the equation Rp0.2 = 1465ε^0.18, the yield strength of the steel in different reductions could be well predicted.
基金Shahid Chamran University of Ahvaz for supporting this research
文摘This study has evaluated the effect of different levels of cold rolling(from 0 to 50%)on the microstructural,magnetic,and mechanical properties and the corrosion behavior of 316L austenitic stainless steel in Na Cl(1 mol/L)+H_2SO_4(0.5 mol/L)solution.Microstructural examinations using optical microscopy revealed the development of a morphological texture from coaxial to elongated grains during the cold-rolling process.Phase analysis carried out on the basis of X-ray diffraction confirmed the formation of the ferromagneticα′-martensite phase under the stresses applied during cold rolling.This finding is in agreement with magnetic measurements using a vibrating sample magnetometer.Mechanical properties determined by tensile and Vickers microhardness tests demonstrated an upward trend in the hardness-to-yield strength ratio with increasing cold-rolling percentage,representing a reduction in the material’s work-hardening ability.Uniform and localized corrosion parameters were estimated via potentiodynamic polarization corrosion tests and electrochemical impedance spectroscopy.In contrast to the uniform corrosion,wherein the corrosion current density increased with increasing cold-working degree because of the high density of microstructural defects,the passive potential range and breakdown potential increased by cold working,showing greater resistance to pit nucleation.Although pits were formed,the cold-rolled material repassivation tendency decreased because of the broader hysteresis anodic loop,as confirmed experimentally by observation of the microscopic features after electrochemical cyclic polarization evaluations.
文摘Single cold rolling and double cold rolling were applied to hot rolled strips with different reduction ratios. The evolutions of { 100}, { 111} and Goss face texture during double rolling were investigated by comparing the orientation distribution function (ODF) of the double rolled sample with that of the single rolled one. The double cold rolling texture is characterized by a higher γ-texture and a lower α-texture, and the { 111}〈112〉 component is improved remarkably. Based on the TEM observation and mechanical properties test, it is found that the reduction ratio assignment significantly affects the texture variation, as-annealing microstructures, and properties of the double cold rolled samples. These results may provide a theoretical guide for the industrial production of double cold rolled IF steel.
文摘The influence of cold rolling reduction on microstructure and mechanical properties of the twinning induced plasticity(TWIP) steel with a chemical composition of Fe-20Mn-3Si-3Al-0.045 C has been investigated.Tensile tests were carried out to explore the mechanical properties of TWIP steel with different cold rolling reductions.The microstructures were observed by optical microscopy and transmission electron microscopy(TEM).The misorientation and the development of recrystallization texture in TWIP steel sheets were investigated by Electron Back Scatter Diffraction(EBSD) technique.The results indicated that the steel exhibited attractively mechanical properties when cold rolling reduction was about 10%.The tensile strength of the steel with a rolling reduction of 10%is higher than 900 MPa and the yield strength is about 800 MPa,while the elongation is above 35%.The microstructure is composed of austenitic matrix and deformation twins at room temperature,at the same time,a significant amount of deformation twins,stacking faults and dislocations are observed by TEM.TEM observations showed the presence of deformation twinning in the sample at low rolling reduction.As the strain increases the volume fraction of twins increases.Mechanical twins play a dominant role during deformation and result in excellent mechanical properties for the investigated steel.By TEM observation,the possible deformation mechanisms can be suggested as:with the increasing strain,formation of the twin will gradually play a more important role during deformation.The interaction between twins and dislocations enhances the strain hardening rate in the sample.Consequently,the necking is delayed and a good ductility is obtained.Twins were always observed in the region with high density of dislocation and faults,suggesting that the interaction among blocked dislocations and faults as well as deformation twins promote the increase in material strength.EBSD observation showed that the textures has evolved according to the following trend:the brass orientation {110}〈112〉and Goss orientation {110}〈001〉are dominant at every strain level,those intensities increase with increasing strain,while with the increase of the strain level,the change of S orientation {123}〈634〉was not obviously.
基金financially supported by the National Basic Research Program of China (No. 2011CB606300)the National High Technology Research and Development Program of China (No. 2012AA03A505)the China Postdoctoral Science Foundation (No. 2013T60110)
文摘The effects of annealing temperature(with the annealing time being constant at 1 h) on the microstructure, ordering, residual stress, mechanical properties, and subsequent cold rolling workability of Fe-6.5wt%Si electrical steel with columnar grains were investigated, where the steel was warm rolled at 500℃ with a reduction of 95%. The results show that recrystallization began to occur in the sample annealed at 575℃ and that full recrystallization occurred in the sample annealed at 625℃. When the annealing temperature was 500℃ or greater, the extent of reordering in the sample was high, which reduced the room-temperature plasticity. However, annealing at temperatures below 300℃ did not significantly reduce the residual tensile stress on the edge of the warm rolled samples. Considering the comprehensive effects of annealing temperature on the recrystallization, reordering, residual stress, and mechanical properties of the warm rolled Fe-6.5wt%Si electrical steel with columnar grains, the appropriate annealing temperature range is 300℃-400℃. Unlike the serious edge cracks that appeared in the sample after direct cold rolling, the annealed samples could be cold rolled to a total reduction of more than 71.4% without the formation of obvious edge cracks, and bright-surface Fe-6.5wt%Si electrical steel strips with a thickness less than 0.1 mm could be fabricated by cold rolling.
基金Project supported by the National Natural Science Foundations of China(Grant Nos.51371089 and 51401083)
文摘The tensile strength and ductility of a high nitrogen nickel-free austenitic stainless steel with solution and cold rolling treatment were investigated by performing tensile tests at different strain rates and at room temperature. The tensile tests demonstrated that this steel exhibits a significant strain rate and cold rolling dependence of the tensile strength and ductility.With the increase of the strain rate from 10^-4s^-1to 1 s^-1, the yield strength and ultimate tensile strength increase and the uniform elongation and total elongation decrease. The analysis of the double logarithmic stress–strain curves showed that this steel exhibits a two-stage strain hardening behavior, which can be well examined and analyzed by using the Ludwigson equation. The strain hardening exponents at low and high strain regions(n2and n1) and the transition strain(εL) decrease with increasing strain rate and the increase of cold rolling RA. Based on the analysis results of the stress–strain curves, the transmission electron microscopy characterization of the microstructure and the scanning electron microscopy observation of the deformation surfaces, the significant strain rate and cold rolling dependence of the strength and ductility of this steel were discussed and connected with the variation in the work hardening and dislocation activity with strain rate and cold rolling.
基金Funded by Shenyang City Application Basic Research Project (No. 1071198-1-00)
文摘Effect of controlled rolling and cooling process on the mechanical properties of low carbon cold forging steel was investigated for different processing parameters of a laboratory hot rolling mill. The results show that the specimens with fast cooling after hot rolling exhibit very good mechanical properties, and the improvement of the mechanical properties can be attributed mainly to the ferrite-grain refinement. The mechanical properties increase with decreasing final cooling temperature within the range from 670 ℃ to 570 ℃ due to the finer interlamellar spacing of pearlite colony. The specimen with fast cooling after low temperature rolling shows the highest values of the mechanical properties. The effect of the ferrite grain size on the mechanical properties was greater than that of pearlite morphology in the present study. The mechanical properties of specimens by controlled rolling and cooling process without thermal treatment were greatly superior to that of the same specimens by the conventional rolling, and their tensile strength reached 490 MPa grade even in the case of low temperature rolling without controlled rolling. It might be expected to realize the substitution medium-carbon by low-carbon for 490 MPa grade cold forging steel with controlled rolling and cooling process.
基金Project(2006BAE03A06) supported by the National Key Technology R&D Program during the 11th Five-Year Plan Period
文摘The microstructure evolution of 1 000 MPa cold rolled dual-phase (DP) steel at the initial heating stages of the continuous annealing process was analyzed. The effects of different overaging temperatures on the microstructures and mechanical properties of 1 000 MPa cold rolled DP steel were investigated using a Gleeble-3500 thermal/mechanical simulator. The experimental results show that ferrite recovery and recrystallization, pearlite dissolution and austenite nucleation and growth take place in the annealing process of ultra-high strength cold rolled DP steel. When being annealed at 800 ℃ for 80 s, the tensile strength and total elongation of DP steel can reach 1 150 MPa and 13%, respectively. The microstructure of DP steel mainly consists of a mixture of ferrite and martensite. The steel exhibits low yield strength and continuous yielding which is commonly attributed to mobile dislocations introduced during cooling process from the intercritical annealing temperature.
文摘With a complicated composition, large rolling sludge has been a focal point concerning neither at home nor abroad have any technologies suitable for bulk utilization of stainless steel cold- production and serious damage to the environment, stainless steel cold- environmental protection for stainless steel enterprises. Up to now, come into being that are not only proper, safe and economical but also rolling sludge. Based on the characteristics of the stainless steel cold- rolling sludge, orthogonal experiments were carried out on pellet proportioning and high-temperature roasting, and major metallurgical properties of sludge pellets were also tested. As the results show, pellets with 30% addition of cold-rolling sludge are qualified regarding their compressive strength, chemical composition and major metallurgical properties. No adverse impact happens to the blast furnace operation when sludge pellets account for 10% of the blast furnace raw materials. Therefore, the technical route applied in this paper is proved simple, feasible and environmentally friendly for cold-rolling sludge treatment.
基金the National Natural Science Foundation of China (No. 50575022) Specialized Research Foundation for the Doctoral Program of Higher Education (No. 20040008024).
文摘The influence of cold rolling reduction on microstructure and mechanical properties of the TWIP (ttwinning induced plasticity) steel was investigated. The results' indicated that the steel had better comprehensive mechanical properties when cold rolling reduction was about 65.0% and the annealing temperature was 1000℃. The tensile strength of the steel is about 640MPa and the yield strength is higher than 255MPa, while the elongation is' above 82%. The microstructure is composed of austenitic matrix and annealing twins at room temperature, at the same time, a significant amount of annealing twins and stacking faults' are observed by transmission electron microscopy (TEM). Mechanical twins play a dominant role during deformation, and result in exceUent mechanical properties.
文摘This study researches cold rolled ultra high strength martensitic steel processed by water quenching. It is found that both the quenching and overageing temperatures greatly influence the mechanical properties of martensitic steel. A tensile strength of 1500 MPa can be obtained from 0.2% C-1.8% Mn steel by soaking at 840℃,quenching at 700℃ and overageing at 200℃ for several minutes. The continuous cooling transformation (CCT) diagram reveals that full martensite can be obtained at a cooling rate of 100℃/s or higher; and at a cooling rate of 3 - 10℃/s,austenite barely decomposes at 700℃. For steel with 0.2% carbon and less manganese, austenite decomposition occurs before it is cooled to 700℃ at a cooling rate of 3 - 10℃/s, which leads to lower tensile strength. It is possible to reduce the manganese content of the 1500 MPa martensitic steel by increasing the quenching temperature. To increase the quenching temperature,the control of flatness during water quenching becomes a major concern.
文摘Cold-rolled advanced high-strength steel sheets have become the material of choice for the automotive industry because of their unique attributes of high strength and balanced mechanical properties.High-hydrogen gas jet cooling and water quenching are the most commonly used ultrafast cooling technologies for producing martensite-containing high-strength steel sheets.The water quenching technology ensures the fastest industrial cooling rate of 1 000 K/s;therefore,it has the highest potential with respect to saving alloys.In this study,the water quenching of a C-Mn-containing steel sheet is simulated during continuous annealing to investigate the effect of water quenching and tempering parameters on its mechanical properties.The results reveal that at low quenching temperatures,the strength of the steel sheet decreases as the soaking temperature increases.However,at high quenching temperatures,a high soaking temperature corresponds to increased strength after quenching,regardless of whether the material was austenitized in the single austenite zone or the inter-critical zone.Therefore,a high quenching temperature always results in a high strength and a high yield ratio after quenching.Low-temperature overaging(tempering) considerably influences the yield strength and yield ratio,and the extent of this influence is correlated with the soaking temperature.
文摘Many advanced technologies have been applied in developing the automatic measuring device for testing transverse thickness difference of cold-rolling steel sheet,such as the technologies of automatic control,sensor measurement,marking identification,photographic location,computer application and information transmission.This measuring device can measure the transverse thickness difference of the steel plate accurately and quickly,with a high detection level of automation.It is an effective detection equipment for transverse thickness control of steel plate.Horizontal width of steel plate measuring 0.8-1.4 m, horizontal measurement point positioning accuracy±0.02 mm,thickness range 0.2-2.0 mm, measurement accuracy within±1μm.
文摘Cold-rolled martensitic steel sheets produced on continuous annealing lines with water quenching facility,have advantages of high strength and low alloying element contents.These are in good accordance with the trend of light-weighting and fuel saving for automotive steel.In this article,a cold-rolled martensitic steel is studied to investigate the effect of annealing parameters on its mechanical properties.It is found that the quenching temperature and the slow cooling speed as well as the overageing temperature have significant influence on the strength of the experimental steel.The temperature zone at which the austenite decomposition is slow or has not started may be chosen as the quenching temperature to ensure the steel’s strength stability.The slow cooling speed also influences the steel’s strength greatly.A high cooling rate will lead to significantly higher strength.Tempering would decrease the steel’s tensile strength but would increase its yield strength.
文摘Cold rolled martensitic sheet steels are achieving more and more applications in car-making because of their ultra-high strength and potential for weight reduction. The relatively low plasticity of ultra-high strength martensitic steels might be a drawback for the applications in the aspects of forming and safety protection function and should be significantly noted. A 1 500 MPa grade cold rolled martensitic sheet steel has been studied to investigate the bendability at 90 degree bending and impact toughness as well as fracture surface morphology at various temperatures. Some discussions have been made basing upon the experiment data to get some understanding on the performance of the materials under various conditions and on how to make use of this kind of ultra high strength steel properly.
文摘In accordance with experimental results about the annealing microstructure and texture of cold-rolled deep- drawing sheet based on the compact strip production (CSP) process, a two-dimensional cellular automation simulation model, considering real space and time scale, was established to simulate recrystallization and grain growth during the actual batch annealing process. The simulation results show that pancaked grains form during recrystallization. (111} advantageous texture components become the main parts of the recrystallization texture. After grain growth, the pancaked grains coarsen gradually. The content of (111} advantageous texture components in the annealing texture increases from 55vo1% to 65vo1%; meanwhile, the contents of {112}〈110〉 and {100}〈110〉 texture components decrease by 4% and 8%, respectively, compared with the recrystallization texture. The simulation results of microstructure and texture evolution are also consistent with the experimental ones, proving the accuracy and usefulness of the model.
文摘Cold-rolled martensitic steel sheets are becoming widely applied in the automotive industry because of their ultra-high strength,which may result in satisfactory weight reduction. The grades of martensitic steel sheets are classified based on their tensile strength,which ranges from 980 to 1 700 MPa. The main applications include a series of structural parts of uniform cross-section or simple shape,such as bumper beams,door beams and door sills,etc. The study and development of cold-rolled martensitic steel sheets date back to 2007 in Baosteel,and some grades became commercially available in 2009. By 2015,Baosteel had commercially supplied thousands of tons of these steel sheets with tensile strength up to 1 400 MPa. Currently,1 500 MPa martensitic steel sheet is commercially available and 1 700 MPa martensitic steel sheet has been successfully produced. The process technology and application guides of Basoteel 's cold-rolled martensitic steels are summarized and analyzed in order to assist ongoing research and ensure correct applications of these ultra-high strength steel sheets.