Five phospholipids in human placenta were determined by phosphorus 31 nuclear magnetic resonance(^(31)P NMR)spectroscopy and thin-layer chromatography(TLC) scanning combined with the corrective method of absorbance pr...Five phospholipids in human placenta were determined by phosphorus 31 nuclear magnetic resonance(^(31)P NMR)spectroscopy and thin-layer chromatography(TLC) scanning combined with the corrective method of absorbance proportional coefficient. The NMR spectrometer used this investigation was a Bruker AM-500 spectrometer operating at 202.4 MHz for ^(31)P chemical shifts are relative to 85% phosphoric acid. TIC was carried out by silica gel H plate developed in chloroform-methanol-glacial acetic acid-ethanol-water(25:4:6:2:0.5),with Vaskovsky reagent as colour -developing agent of phospholipids.展开更多
Wave simulation performance and its quality are key factors to reflect the overall capacity and level of an ocean engineering basin. They include wave simulating and absorbing capacity of reflected waves. In order to ...Wave simulation performance and its quality are key factors to reflect the overall capacity and level of an ocean engineering basin. They include wave simulating and absorbing capacity of reflected waves. In order to reduce the influence of reflected waves, various wave absorbing devices are equipped in ocean engineering basins across the world. The experimental investigation into the performance of combined cambered-type wave absorbing beach(CCTWAB) with damping bars equipped in Deepwater Offshore Basin is conducted. The experiment adopts the two-point method. The reflection coefficients are calculated by the method, in which the incident and reflected waves can be separated from the physically simulated composite waves with different periods and wave heights in the time domain. The experimental results indicate that in the range of normal wave heights and periods for model tests, the CCTWAB with damping bars is excellent in eliminating the reflected waves.展开更多
文摘Five phospholipids in human placenta were determined by phosphorus 31 nuclear magnetic resonance(^(31)P NMR)spectroscopy and thin-layer chromatography(TLC) scanning combined with the corrective method of absorbance proportional coefficient. The NMR spectrometer used this investigation was a Bruker AM-500 spectrometer operating at 202.4 MHz for ^(31)P chemical shifts are relative to 85% phosphoric acid. TIC was carried out by silica gel H plate developed in chloroform-methanol-glacial acetic acid-ethanol-water(25:4:6:2:0.5),with Vaskovsky reagent as colour -developing agent of phospholipids.
基金the National Natural Science Foundation of China(No.51239007)the SMC Morningstar Young Scholars Award Scheme of Shanghai Jiao Tong University
文摘Wave simulation performance and its quality are key factors to reflect the overall capacity and level of an ocean engineering basin. They include wave simulating and absorbing capacity of reflected waves. In order to reduce the influence of reflected waves, various wave absorbing devices are equipped in ocean engineering basins across the world. The experimental investigation into the performance of combined cambered-type wave absorbing beach(CCTWAB) with damping bars equipped in Deepwater Offshore Basin is conducted. The experiment adopts the two-point method. The reflection coefficients are calculated by the method, in which the incident and reflected waves can be separated from the physically simulated composite waves with different periods and wave heights in the time domain. The experimental results indicate that in the range of normal wave heights and periods for model tests, the CCTWAB with damping bars is excellent in eliminating the reflected waves.