MHz cut-off frequency and permeability mechanism of iron-based soft magnetic composites

The lack of soft magnetic composites with high power density in MHz frequency range has become an obstacle in the efficient operation of the electrical and electronic equipments.Here,a promising method to increase the cut-off frequency of iron-based soft magnetic composites to hundreds of MHz is reported.The cut-off frequency is increased from 10 MHz to 1 GHz by modulating the height of the ring,the distribution of particles,and the particle size.The mechanism of cut-off frequency and permeability is the coherent rotation of domain modulated by inhomogeneous field due to the eddy current effect.An empirical formula for the cut-off frequency in a magnetic ring composed of iron-based particles is established from experimental data.This work provides an effective approach to fabricate soft magnetic composites with a cut-off frequency in hundreds of MHz.

Combined control of fluid adsorption capacity and initial permeability on coal permeability

The variations of strain and permeability of coal were systematically studied through the physical simulation of N2 and water injection.The effects of fluid adsorption capacity and initial permeability on strain,permeability and the dominant effect of pore pressure were discussed.The adsorption strain and strain rate of coal during water injection are significantly higher than those during N2 injection.An edge of free adsorption exists in the early phase of N2 and water injection,which is related to fluid saturation.Within this boundary,the strain rate and pore pressure are independent.Moreover,the injec-tion time of initial stage accounts for about 20%of the total injection time,but the strain accounts for 70%of the total strain.For water injection,this boundary is about half of water saturation of coal.Besides,the influence of pore pressure on permeability is complex,which is controlled by adsorption capacity and initial permeability of coal.When the initial permeability is large enough,the effect of adsorption strain on permeability is relatively weak,and the promoting effect of pore pressure on fluid migration is dominant.Therefore,the permeability increases with increasing pore pressure.When the initial permeability is relatively low,the pore pressure may have a dominant role in promoting fluid migration for the fluid with weak adsorption capacity.However,for the fluid with strong adsorption capacity,the adsorption strain caused by pore pressure may play a leading role,and the permeability reduces first and then ascends with increasing pore pressure.

Effect of negative permeability on elastic wave propagation in magnetoelastic multilayered composites

With the advent of left-handed magnetic materials, it is desirable to develop high-performance wave devices based on their novel properties of wave propagation. This letter reports the special properties of elastic wave propagation in magnetoelastic multilayered composites with negative permeability as compared to those in counterpart structures with positive permeability. These novel properties of elastic waves are discerned from the diversified dispersion curves, which represent the propagation and attenuation characteristics of elastic waves. To compute these dispersion curves, the method of reverberation-ray matrix is extended for the analysis of elastic waves in magnetoelastic multilayered composites. Although only the results of a single piezomagnetic and a binary magnetoelastic layers with mechanically free and magnetically short surfaces as well as perfect interface are illustrated in the numerical examples, the analysis is applicable to magnetoelastic multilayered structures with other kinds of boundaries/interfaces.

NANOCRYSTALLINE STRUCTURE AND INITIAL PERMEABILITY OF ANNEALED Fe_(73.5)Cu_(1)W_(3)Si_(13.5)B_(9) Alloy

The nanocrystalline structure of annealed Fe73.5 Cu1 W3Si13.5B9 alloy has been investigated by using the XRD and the TEM methods. The relation between the initial permeability and the microstructure of the annealed alloy has been discussed. The crystalline phase in annealed Fe73.5 Cu1 W3Si13.5B9 alloy is the α-Fe(Si) phase with DO3 superstructure. The volume fraction, Si content and degree of order of the αFe(Si) phase increase with increasing annealing temperature. In the temperature range of 490-570℃, the α-Fe(Si) phase has a size of 13 nm, and its grain number increases as the annealing temperature is increased. The DO3 ordered region in the α-Fe(Si) grain is spherical approximately, and its size increases as the annealing temperature increases. The size of the DO3 ordered region is 12.8 nm at the temperature of 570℃,which is close to that of the α-Fe(Si) grain. There is obvious change in the structure of the residual amorphous phase during annealing, and the nearest atomic distance and the short-range order of residual amorphous phase reach maximum and minimum at 530℃, respectively. The initial permeability of annealed Fe73.5 Cu1 W3Si13.5 B9 alloy is not only dependent on the size, volume fraction and Si content of the α-Fe(Si) phase but also related to the structure state of the residual amorphous phase.

Rolling contact fatigue nondestructive testing system for a bearing inner ring based on initial permeability

Due to the fact that rolling contact fatigue is not easily detected, and residual life is not easily evaluated in the early stage of bearing life, a nondestructive testing method based on initial permeability is proposed. By analyzing the crack propagation mechanism, a fatigue state detection system based on differential signals is designed. A simulation model of the detection of the inner ring of the pulse signal is established by using the electromagnetic field simulation software. The effects of the height of the coil, the inner and outer diameter, the number of coil turns, the diameter and the height of the ferrite core of the probe on the differential value of the detection signal are simulated. The parameter combination of the maximum difference value of the signal is used as the structural size of the sensor, and the detection sensor is designed and fabricated. Moreover, the bearing fatigue test system is designed, and the bearing is tested. The results show that the system has good detection ability for rolling contact fatigue and verifies the mechanism and trend of crack propagation in the inner ring of the bearing.

High permeability and bimodal resonance structure of flaky soft magnetic composite materials

We establish a theoretical bimodal model for the complex permeability of flaky soft magnetic composite materials to explain the variability of their initial permeability.The new model is motivated by finding the two natural resonance peaks to be inconsistent with the combination of the domain wall resonance and the natural resonance.In the derivation of the model,two relationships are explored:the first one is the relationship between the number of magnetic domains and the permeability,and the second one is the relationship between the natural resonance and the domain wall resonance.This reveals that the ball milling causes the number of magnetic domains to increase and the maximum initial permeability to exist after 10 h of ball milling.An experiment is conducted to demonstrate the reliability of the proposed model.The experimental results are in good agreement with the theoretical calculations.This new model is of great significance for studying the mechanism and applications of the resonance loss for soft magnetic composite materials in high frequency fields.

Complex Permittivity and Permeability Studies Viewing Antenna Applications of NBR-Based Composites Comprising Conductive Fillers

The work presents studies on the complex permittivity and permeability of composites based on acrylonitrile butadiene rubber containing combinations of conductive fillers which include carbon black and nickel powder. The properties of those composites, containing each of the fillers at the same amount were compared. The permittivity and permeability values of the composites are influenced remarkably by their morphology and structure as well as by the morphological and structural specifics of both fillers. As electron scanning microscopy studies confirm, those parameters are predetermined by the nature of the composites studied—particle size, particles arrangement in the matrix and their tendency to clustering. Last but not least matrix-filler interface phenomena also impact the characteristics in question. The possibilities for applications of the composites in antennae have been studied, in particular, as substrates and insulating layers in flexible antennae for body centric communications (BCCs). The research results allow the conclusion that these materials can find such applications indeed. Composites of higher conductivity can be used where surface waves are generated to provide on-body communications, while composites of lower conductivity may be used for antennae that will be on the body of a person and will transmit to and receive from other antennas that are not on the body of the same person (off-body communications). It is clear that one can engineer the properties of antennae substrates at microwave frequencies by adjusting the filler content and the type of filler and thus control and tailor the antenna performance specific for a particular application.

Postbuckling of Marine Stifened Composite Plates with Initial Geometric Imperfections Using Progressive Failure Analysis

This work explores the postbuckling behavior of a marine stifened composite plate in the presence of initial imperfections.The imperfection shapes are derived from buckling mode shapes and their combinations.Thereafter,these imperfection shapes are applied to the model,and nonlinear large defection fnite element and progressive failure analyses are performed in ANSYS 18.2 software.The Hashin failure criterion is employed to model the progressive failure in the stifened composite plate.The efect of the initial geometric imperfection on the stifened composite plate is investigated by considering various imperfection patterns and magnitudes.Results show that when the magnitude of the imperfection is 20 mm,the ultimate strength of the stifened composite plate decreases by 31%.Moreover,global imperfection shapes are found to be fundamental in determining the ultimate strength of stifened composite plates and their postbuckling.

A Study on the Initial Fracture Behavior of CF/GF Intra-Hybrid Woven Fabric Reinforced Composites

In this paper, woven fabrics of glass fiber/carbon fiber intra-hybrid in plain structure were used to fabricate fiber reinforced plastic (FRP) composite by hand lay-up method. The investigation on tensile property was carried out on specimens in 7 orientations including 0°/5°/15°/75°/85°/90° in previous works. With the specimen parameters and experimental data, FEM model was built by the software of Marc. By combining the experimental results and finite element analysis, the modulus was simulated and calculated at the first stage. Then interfacial stress of the 0 degree and 90 degree was also calculated. By the initial fracture stress data from experiment as well as the simulation value of interfacial strength of 0 and 90 degree, the initial fracture stress of the off-axial specimens wascalculated and predicted. The result shows that the interfacial strength of the glass fiber bundle is higher than that of the carbon fiber bundle in transverse direction. By using the interfacial strength and according to the Von Mises yielding criterion, the initial fracture stress was predicted, which can be a contribution to the design or predict of the material properties.

Determination Method on Initial Pretension of Cables in Steel Mega Frame and Prestressed Composite Bracing Structure

Determining initial pretension values of pre-stressed cables is one of the key problems for a steel mega frame and pre-stressed composite bracing structure.Through the mechanical analysis of the composite bracing under vertical loading,the critical factors deciding the initial pretention value were found.According to these factors,a rule for the initial pretension value was put forward.The determination equations were acquired based on the principle of force equilibrium at nodes.The numerical results indicate that the internal force disequilibrium in composite bracings resulted from symmetrical load can be eliminated only in a symmetrical way,so that initial pretention values are decided only by vertical loads.The influencing coefficient leveling method,taking into account interactions between story and story,is accurate and feasible.

Self-biased magnetoelectric responses in magnetostrictive/piezoelectric composites with different high-permeability alloys

We comparatively investigate the influence of various high-permeability alloys on the hysteretic and remanent res- onant magnetoelectric （ME） response in a composite of magnetostrictive nickel （Ni） and piezoelectric Pb（Zrl_x, Tix）O3 （PZT）. In order to implement this comparative research, Co-based amorphous alloy （CoSiB）, Fe-based nanocrystalline alloy （FeCuNbSiB） and Fe-based amorphous alloy （FeSiB） are used according to different magnetostriction （2s） and saturation magnetization （μtoMs） characteristics. The bending and longitudinal resonant ME voltage coefficients （αME,b and αME,1） are observed comparatively for CoSiB/Ni/PZT, FeCuNbSiB/Ni/PZT, and FeSiB/Ni/PZT composites. The experimental data indicate that the FeSiB/Ni/PZT composite has the largest remanent self-biased aME,b and aME,1 due to the largest magnetic grading of λs and μ0Ms in the FeSiB/Ni layer. When the number of FeSiB foils is four, the maximum remanent aME,b and aME,I at zero bias magnetic field are 57.8 V/cm·Oe and 107.6 V/cm·Oe, respectively. It is recommended that the high-permeability alloy is supposed to have larger λs and μ0Ms for obtaining a larger remanent self-biased ME responses in ME composite with high-permeability alloy.

Magnetic Hysteresis and Complex Initial Permeability of Cr³⁺Substituted Mn-Zn Ferrites

The impact of Cr3+ ion on the magnetic properties of Mn0.50Zn0.50CrxFe2-xO4 (with x = 0.0, 0.1, 0.2, 0.3, 0.4 and 0.5) has been studied. Ferrite samples were synthesized by combustion method and sintered at various temperatures (1250°C, 1300°C and 1350°C). The structural properties were investigated by means of X-ray diffraction patterns and indicated that the samples possess single phase cubic spinel structure. The lattice parameter decreases with the increase in Cr3+ content, as the ionic radius of Cr3+ ion is smaller than that of Fe3+. The average grain size (D), bulk density (ρB) and initial permeability (μi’ )decreases with increase in Cr3+ content whereas porosity follows its opposite trend. The ρB was found to increase with increase in Cr3+ content as the sintering temperature (Ts) is increased from 1250°C to 1350°C. The Ts affects the densification, grain growth and (μi’ ) of the samples. The (μi’ ) strongly depends on average grain size, density and intragranular porosity. The B-H loops of the compositions were measured at room temperature. The saturation magnetization (Ms), coercivity (Hc) and hysteresis losses were studied as a function of Cr3+ content. The Ms was found to decrease with the increase of Cr3+ content, which is attributed to the dilution of A-B interaction.

Influence of Overlay Placement and Fabric Architecture of Non-crimp Fabrics on In-plane and Transverse Permeability in Liquid Composite Molding

To study the resin flow and the permeability in fabric preforms during the liquid composite molding( LCM) process,influences of stitch and overlay placement styles on the internal flow behavior in-plane and transverse were investigated. The permeability tests were carried using unidirectional and biaxial noncrimp carbon fabric( NCF) by linear capacitance sensors and ultrasound monitor system. The results indicate that the internal flow behavior and permeability in plane with different stitch and overlay placement styles are significantly different. When flow channels formed by stitches penetrate along the fiber direction,the permeability is high in one direction, which makes the in-plane principle permeabilities K_1 and K_2 significantly different. When there is an angle between the flow channel and fiber direction,the in-plane principle permeabilities on all directions are nearly the same and the flow process is close to isotropy. As to transverse permeability,the exist of flow channels on thickness influences it greatly and it is about 1-2 orders of magnitude lower in unidirectional fabric than that in biaxial NCF.

Fracture Toughness Studies of Polypropylene- Clay Nanocomposites and Glass Fibre Reinfoerced Polypropylene Composites

In this paper, a comparative study on the fracture toughness of woven glass fibre reinforced polypropylene, chopped glass fibre reinforced polypropylene and nanoclay filled polypropylene composites is presented. Nanoclays (Cloisite 15A) of 1 wt. % to 5 wt. % were filled in polypropylene (PP) matrix and they were subjected to fracture toughness stu-dies. The specimen with 5 wt. % nanoclay showed 1.75 times and 3 times improvement in critical stress intensity factor (KIC) and strain energy release rate (GIC), respectively, over virgin PP. On the other hand, 3 wt. % nanoclay PP composites showed superior crack containment properties. These structural changes of composite specimens were examined using Transmission Electron Microscopy (TEM) and X-ray diffraction (XRD) methods. It showed that exfoli-ated nanocomposite structures were formed up to 3 wt. % nanoclay, whereas, intercalated nanocomposite structures formed above 3 wt. % nanoclay in the PP matrix. Furthermore, the woven fibre reinforced PP composites demonstrated superior crack resistant properties than that of clay filled nanocomposites and chopped fibre PP composites. However, KIC and GIC values for woven fibre composites were lesser than that of chopped fibre composites. Moreover, KIC and GIC values for both nanoclay filled PP composites and woven fibre composites are comparable even though the clay filled PP demonstrated catastrophic failure. Also, the crack propagation rate of PP-nanoclay composites is comparable to that of chopped fibre composites.

Numerical simulation of the blast wave of a multilayer composite charge

The numerical simulation of a blast wave of a multilayer composite charge is investigated.A calculation model of the near-field explosion and far-field propagation of the shock wave of a composite charge is established using the AUTODYN finite element program.Results of the near-field and far-field calculations of the shock wave respectively converge at cell sizes of 0.25-0.5 cm and 1-3 cm.The Euler--fluxcorrected transport solver is found to be suitable for the far-field calculation after mapping.A numerical simulation is conducted to study the formation,propagation,and interaction of the shock wave of the composite charge for different initiation modes.It is found that the initiation mode obviously affects the shock-wave waveform and pressure distribution of the composite charge.Additionally,it is found that the area of the overpressure distribution is greatest for internal and external simultaneous initiation,and the peak pressure of the shock wave exponentially decays,fitting the calculation formula of the peak overpressure attenuation under different initiation modes,which is obtained and verified by experiment.The difference between numerical and experimental results is less than 10%,and the peak overpressure of both internal and external initiation is 56.12% higher than that of central single-point initiation.

Damage Initiation and Propagation in Composites Subjected to Low-Velocity Impact:Experimental Results,3D Dynamic Damage Model,and FEM Simulations

A three-dimensional dynamic damage model that fits both small and large damage sizes is developed to predict impact damage initiation and propagation for each lamina of T300-carbon/epoxy laminations.First,13 specimens of the same lamination sequence are subjected to three different impact energies(10 J,15 J,and 20 J).After the impact,the laminates are inspected by the naked eye to observe the damage in the outer layers,and subsequently X-rayed to detect the inner damage.Next,the stress analysis of laminates subjected to impact loading is presented,based on the Hertz contact law and virtual displacement principle.Based on the analysis results,a three-dimensional dynamic damage model is proposed,including the Hou failure criteria and Camanho stiffness degradation model,to predict the impact damage shape and area.The numerical predictions of the damage shape and area show a relatively reasonable agreement with the experiments.Finally,the impact damage initiation and propagation for each lamina are investigated using this damage model,and the results improve the understanding of the impact process.

The absorbing properties of Fe_(73.5) Cu_1 Nb_3Si_(13.5)B_9 amorphous powder/S-glass fiber-reinforced epoxy composite panels

Fe73.5Cu1Nb3Si13.5B9 （or FeCuNbSiB） powder/ S-glass fiber-reinforced epoxy composite panels were pre- pared by mold pressing method. Metallographic analysis shows that the amorphous powders are evenly distributed between the layers of S-glass fibers. The effects of the Fe- CuNbSiB powder mass fraction on the complex permittivity, complex permeability, and microwave absorption of the composite panels have been studied in the frequency range of 2.6-18.0 GHz. The complex permittivity of the composite panels with different mass fractions of the FeCuNbSiB powders shows several peaks in the 2.6-18.0 GHz fre- quency range. The complex permeability of the composites decreases with the increasing frequency in the frequency range of 8-18 GHz. The composite with FeCuNbSiB/epoxy mass ratio of 2.5：1.0 has excellent microwave absorption properties of a minimum reflection loss value -30.5 dB at 10.93 GHz for a thickness of 2 mm. A reflection loss exceeding -10 dB can be obtained in a broad frequency range of 3.2-18.0 GHz with a thickness of 1.15-5.00 mm. For the FeCuNbSiB composites, the magnetic loss is the dominant term for microwave absorption. The FeCuNbSiB powders are a possible candidate for high-performance microwave absorption filler.

Effect of a Slight Interfacial Reaction on Mechanical Properties of SiCp/Al Composites

A slight interfacial reaction in squeeze-cast SiCp/6061AI composites has been studied. It is found that this kind of reaction has a particular effect on the mechanical properties of the composites. The results of fie-cure tests show that this reaction in the composites obviously increases the elastic properties, but is not beneficial to the fracture strength and ductility.This phenomenon can be interpreted in terms of two different micromechanisms which have been analyzed using TEM and HREM observations, acoustic emission (AE) technique and SEM fractography. In addition, a new method of SiC surface modification which can control the interface state is initially presented.

Experimental study on explosion dispersion process of a multi-layer composite charge under different initiation modes

The influe nce of initiation modes on the explosive dispersion process of the multi-layer co mposite charge(MCC) was studied.Overpressure sensors and high-speed photography system were used to investigate the energy release process of an MCC with a specific structure.The shock wave pressure and explosive dispersion characteristics of the MCC under different initiation modes were compared.The forming and expanding process of the shock wave of the composite charge under different initiation modes was determined.The separation position of the shock wave and fireball interface was determined.The calculation formulas of the shock radius and overpressure of the composite charge are presented.The radius of the shock wave of the composite charge was significantly affected by the initiation mode.Moreover,the development process of the composite explosive fireball under different initiation modes was analyzed,the variation rules of the composite charge dispersion radius and fireball dispersion velocity with time were obtained under the different initiation modes,the explosion energy release rate of composite charge under simultaneous initiation modes was the highest,and the peak overpressure under the simultaneous initiation mode was 1.61 times that of central single-point initiation.

Ion-transport characteristics of new-old concrete composite system

New-old concrete composite system usually exists in concrete repairing structure.In the present work,series of experiments were carried out to investigate permeability and ion diffusion properties of new-old concrete composite by measuring 6-hour coulomb charge and chloride diffusivity.The interrelation among transport properties of new-old composites,new,and old concretes was also discussed.Results indicate that the permeability and chloride diffusivity of new-old concrete composite system closely interrelate to the corresponding new concrete and old concrete.The interfacial transition zone between new concrete and old concrete greatly influences the transport property of new-old concrete system.Compared with the corresponding new concrete and old concrete lower permeability and diffusivity values for the new-old concrete composites can be achieved by choosing suitable new concrete.It is possible to design the tailor-made new-old concrete composite system for repair given the transport property.