In this study, compounded surface modification technology-high current pulsed electron beam (HCPEB) + micro-plasma oxidation (MPO) was applied to treat ZK60 Mg alloys. The characteristics of the microstructure of...In this study, compounded surface modification technology-high current pulsed electron beam (HCPEB) + micro-plasma oxidation (MPO) was applied to treat ZK60 Mg alloys. The characteristics of the microstructure of ZK60 Mg alloy after single MPO and HCPEB+MPO compounded treatment were investigated by SEM. The results showed that the density of the ceramic layer of HCPEB+MPO-treated ZK60 Mg alloy was improved and defects were reduced compared to that under MPO treatment alone. Surface modified layer of ZK60 Mg alloys treated by HCPEB+MPO was divided into three zones, namely the top loose ceramic zone, middle compact zone and inside HCPEB-induced melted zone. Corrosion resistance of ZK60 Mg alloy before and after the compounded surface modification was measured in a solution of 3.5% NaCl by potentiodynamic polarization curves. It was found that the corrosion current density of ZK60 Mg alloys could be reduced by about three orders of magnitude, from 311μA/cm^2 of the original sample to 0.2μA/cm^2 of the HCPEB+MPO-treated sample. This indicates the great application potential of the HCPEB+MPO compounded surface modification technology in improving the corrosion resistance of ZK60 Mg alloys in the future.展开更多
The surface composite modification of the 7050 aluminum alloy friction stir-welded joints was performed by shot peening(SP)/multiple rotation rolling(MRR)and MRR/SP,and the fatigue performance of the nugget zone(NZ)wa...The surface composite modification of the 7050 aluminum alloy friction stir-welded joints was performed by shot peening(SP)/multiple rotation rolling(MRR)and MRR/SP,and the fatigue performance of the nugget zone(NZ)was investigated.The results demonstrated that the fatigue life of SP/MRR samples is longer than that of MRR/SP.On the plane 150μm below the surface.The grains with high angle grain boundary account for 71.5%and 34.3%for MRR/SP and SP/MRR samples,respectively.The crack propagation path of the MRR/SP is transgranular and intergranular,and it is intergranular for the MRR/SP.Multitudinous fatigue striations and some voids appeared at the fracture during the stable crack propagation stage.However,fatigue striations for SP/MRR are with smaller spacing,fewer holes,and smaller size under SP/MRR compared with fatigue fracture of MRR/SP.The differences in fatigue properties and fracture characteristics of the NZ are related to the microstructure after the two combined surface modifications.展开更多
基金supported by Liaoning BaiQianWan Talents Program of China (No. 2008921028)Doctoral Fund of Ministry of Education of China (No. 200801451082)
文摘In this study, compounded surface modification technology-high current pulsed electron beam (HCPEB) + micro-plasma oxidation (MPO) was applied to treat ZK60 Mg alloys. The characteristics of the microstructure of ZK60 Mg alloy after single MPO and HCPEB+MPO compounded treatment were investigated by SEM. The results showed that the density of the ceramic layer of HCPEB+MPO-treated ZK60 Mg alloy was improved and defects were reduced compared to that under MPO treatment alone. Surface modified layer of ZK60 Mg alloys treated by HCPEB+MPO was divided into three zones, namely the top loose ceramic zone, middle compact zone and inside HCPEB-induced melted zone. Corrosion resistance of ZK60 Mg alloy before and after the compounded surface modification was measured in a solution of 3.5% NaCl by potentiodynamic polarization curves. It was found that the corrosion current density of ZK60 Mg alloys could be reduced by about three orders of magnitude, from 311μA/cm^2 of the original sample to 0.2μA/cm^2 of the HCPEB+MPO-treated sample. This indicates the great application potential of the HCPEB+MPO compounded surface modification technology in improving the corrosion resistance of ZK60 Mg alloys in the future.
基金supported by the National Natural Science Foundation of China(Grants 51865028)the Gansu Provincial Science and Technology Planning Project(Grant No.20YF8GA056).
文摘The surface composite modification of the 7050 aluminum alloy friction stir-welded joints was performed by shot peening(SP)/multiple rotation rolling(MRR)and MRR/SP,and the fatigue performance of the nugget zone(NZ)was investigated.The results demonstrated that the fatigue life of SP/MRR samples is longer than that of MRR/SP.On the plane 150μm below the surface.The grains with high angle grain boundary account for 71.5%and 34.3%for MRR/SP and SP/MRR samples,respectively.The crack propagation path of the MRR/SP is transgranular and intergranular,and it is intergranular for the MRR/SP.Multitudinous fatigue striations and some voids appeared at the fracture during the stable crack propagation stage.However,fatigue striations for SP/MRR are with smaller spacing,fewer holes,and smaller size under SP/MRR compared with fatigue fracture of MRR/SP.The differences in fatigue properties and fracture characteristics of the NZ are related to the microstructure after the two combined surface modifications.