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Construction of Molecular Biology and Experiment Case Library for Graduate Students
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作者 Huanying PANG Miao XIE +3 位作者 Shuanghu CAI Yu HUANG Yucong HUANG Jichang JIAN 《Asian Agricultural Research》 2024年第8期47-49,共3页
Molecular Biology and Experiment is considered fundamental for graduate students specializing in aquaculture at Guangdong Ocean University.This discipline focuses on the examination of the structure and function of ma... Molecular Biology and Experiment is considered fundamental for graduate students specializing in aquaculture at Guangdong Ocean University.This discipline focuses on the examination of the structure and function of macromolecules,including proteins and nucleic acids.Moreover,it elucidates biological phenomena and principles at the molecular level,making it an essential foundational course for students pursuing various biology majors.As a foundational course for the basic application of aquaculture,Molecular Biology and Experiment requires guidance through numerous examples and cases.However,there are several challenges to address in developing the case library.Consequently,a case library has been established to meet the course requirements of Molecular Biology and Experiment for modern graduate students,with the central goal of reforming the educational model of higher education institutions and enhancing the effectiveness and quality of talent development.This strategy is designed to nurture highly skilled professionals who can address the current needs of the industry. 展开更多
关键词 Case LIBRARY Molecular biology and EXPERIMENT AQUACULTURE major
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Simulation Experiments of Land Surface Physical Processes and Ecological Effect over Different Underlying Surface 被引量:1
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作者 LIU Shu-hua~(1,2), JIANG Hao-yu, HU Fei~2 LIU Hui-zhi~2 LIANG Fu-ming~1, WANG Jiang-hua~1(1. Group of Atmosphere Boundary Layer and turbulence, Ministry Laboratory of Storm and Drought Flood Damage, Department of Atmospheric Sciences the School of Physics Peking University, Beijing 100871, China 2. State Key Laboratories of Atmosphere Physics and Chemistry, Institute of Atmospheric Physics, Chinese Academy of Science, Beijing 100029, China) 《地球科学进展》 CAS CSCD 2004年第S1期15-20,共6页
Based on the existing Land Surface Physical Process Models(Deardorff, Dickinson, LIU, Noilhan, Seller, ZHAO), a Comprehensive Land Surface Physical Process Model (CLSPPM) is developed by considering the different phys... Based on the existing Land Surface Physical Process Models(Deardorff, Dickinson, LIU, Noilhan, Seller, ZHAO), a Comprehensive Land Surface Physical Process Model (CLSPPM) is developed by considering the different physical processes of the earth's surface-vegetation-atmosphere system more completely. Compared with SiB and BATS, which are famous for their detailed parameterizations of physical variables, this simplified model is more convenient and saves much more computation time. Though simple, the feas... 展开更多
关键词 comprehensive land surface Physical process model (CLSPPM) Simulation experiment Land surface physical process Ecological effect.
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基于CarSim/Simulink的计算机控制系统综合实验设计
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作者 闻继伟 陈珺 +1 位作者 栾小丽 徐琛 《实验室研究与探索》 CAS 北大核心 2024年第3期73-77,共5页
针对计算机控制系统课程中控制算法设计与仿真实现,设计了基于CarSim/Simulink的控制综合实验方案。以4轮独立驱动小车为对象,要求学生熟悉其基本工作原理,并在非线性动力学模型基础上,进行局部线性近似,设计反馈控制器,模拟小车控制。... 针对计算机控制系统课程中控制算法设计与仿真实现,设计了基于CarSim/Simulink的控制综合实验方案。以4轮独立驱动小车为对象,要求学生熟悉其基本工作原理,并在非线性动力学模型基础上,进行局部线性近似,设计反馈控制器,模拟小车控制。使用CarSim仿真软件可直观地模拟调整4轮独立驱动小车的质量、质心位置和转动惯量等,实现个性化选择,搭建车辆模型;与Simulink接口互通,在Simulink中完成控制算法。实验设计旨在使学生夯实计算机控制系统的理论基础,并逐步过渡到控制工程,理论联系实际,培养其解决复杂工程问题的能力。 展开更多
关键词 CarSim/Simulink联合仿真 计算机控制系统 反馈控制 综合实验
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Reaction degree of composition B explosive with multi-layered compound structure protection subjected to detonation loading 被引量:4
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作者 Jia-yun Liu Yong-xiang Dong +3 位作者 Xuan-yi An Ping Ye Qi-tian Sun Qian Gao 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2021年第2期315-326,共12页
The explosive reaction degree and protection from explosions are concerns in the military field.In this work,the reaction degree of the composition B explosive was investigated experimentally.Multi-layered compound st... The explosive reaction degree and protection from explosions are concerns in the military field.In this work,the reaction degree of the composition B explosive was investigated experimentally.Multi-layered compound structures were used as barriers to weaken the blast loads.A comprehensive experiment using a high-speed camera and image processing techniques,side witness plates,and bottom witness plates was presented.Using the experimental fragment velocities,fragment piercing patterns,and damage characteristics,the reaction degree of the explosive impeded by different multi-layered compound structures could be precisely differentiated.Reaction parameters of the explosive obstructed by compound structures were obtained by theoretical analysis and numerical simulations.Unlike the common method in which the explosive reaction degree is only distinguished based on the initial pressure amplitude transmitted into the explosive,a following shock wave reflected from the side steel casing was also considered.Different detonation growth paths in the explosive formed.Therefore,all these shock wave propagation characteristics must be considered to analyze the explosive response impeded by compound structures. 展开更多
关键词 Reaction degree Explosive protection Compound structure comprehensive experiment
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锆基MOF光催化制过氧化氢的综合化学实验设计
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作者 任颜卫 翟祺祥 《广东化工》 CAS 2024年第11期176-178,共3页
为了加强科研成果向实验教学转化和培养学生科研创新能力,设计基于金属有机框架(MOF)材料的光催化制过氧化氢(H_(2)O_(2))综合化学实验。以双氨基功能化联苯二甲酸为配体,四氯化锆为金属盐,苯甲酸为调节剂,通过溶剂热法合成锆基MOF催化... 为了加强科研成果向实验教学转化和培养学生科研创新能力,设计基于金属有机框架(MOF)材料的光催化制过氧化氢(H_(2)O_(2))综合化学实验。以双氨基功能化联苯二甲酸为配体,四氯化锆为金属盐,苯甲酸为调节剂,通过溶剂热法合成锆基MOF催化剂UiO-67-(NH_(2))_(2)。利用PXRD和UV-DRS对样品结构和可见光吸收性能进行表征。以蓝光LED为光源,探究光源功率、催化剂浓度和反应时间对光催化制H_(2)O_(2)效率的影响。采用罗丹明B为模拟污染物,验证所制H_(2)O_(2)溶液的降解污染物性能。该综合实验涉及MOF合成及表征、仪器测试、数据分析等多个环节,不仅加深学生对化学、材料和环境等多学科基础知识的综合理解,还能激发学生的学习积极性和培养学生的创新能力。 展开更多
关键词 综合化学实验 金属有机框架 光催化 过氧化氢 污染物降解
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Solar Radiation Pressure Modeling and Application of BDS Satellites 被引量:7
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作者 Qiuli CHEN Hui YANG +2 位作者 Zhonggui CHEN Haihong WANG Chen WANG 《Journal of Geodesy and Geoinformation Science》 2020年第2期45-52,共8页
Solar radiation pressure(SRP)model is the basis of high precise orbit determination and positioning of navigation satellites.At present,it is common to see the study of SRP model of BDS satellites.However,the establis... Solar radiation pressure(SRP)model is the basis of high precise orbit determination and positioning of navigation satellites.At present,it is common to see the study of SRP model of BDS satellites.However,the establishment and application of a comprehensive analytical SRP model based on satellite physical parameters are rare.Different from other conservative forces and non-conservative forces,SRP is closely related to the satellite’s physical parameters and in-orbit state.On the basis of the physical mechanism of solar radiation,BDS satellite physical parameters,in-orbit attitude control mode,and so on,a comprehensive analytical model has been studied in this paper.Based on precise ephemeris and satellite laser ranging(SLR)data,the precision of a comprehensive analytical model has been verified.And the precision of orbit determination is at the decimeter level using this comprehensive analytical SRP model.According to the satellite conservation theorem of angular momentum and change of in-orbit telemetry parameters,the difference between a comprehensive analytical model and the actual in-orbit interference force has been analyzed and calculated.The addition of empirical items on the comprehensive analytical model has been proposed.SLR validations demonstrated that the orbit precision of BDS C08 and C10 can be achieved at 0.078 m and 0.084 m respectively.Compared with using the improved CODE empirical model,precision orbit accuracy of them has increased by 0.021 m and 0.045 m respectively. 展开更多
关键词 BDS satellite solar radiation pressure comprehensive analytical model experience correction item precise orbit determination
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COMPREHENSIVE MATHEMATICAL MODEL OF MICROCIRCULATORY DYNAMICS (Ⅰ)——BASIC THEORY
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作者 郭仲三 肖帆 +2 位作者 郭四稳 伍岳庆 古乐野 《Applied Mathematics and Mechanics(English Edition)》 SCIE EI 1999年第9期1014-1022,共9页
Under the basis of physiological data, a nonlinear and unsteady comprehensive mathematical model of microcirculatory dynamics with distributed parameters is developed. Hemodynamics, interstitium dynamics, lymph dynami... Under the basis of physiological data, a nonlinear and unsteady comprehensive mathematical model of microcirculatory dynamics with distributed parameters is developed. Hemodynamics, interstitium dynamics, lymph dynamics, dynamics of protein transport, oxygen dynamics, dynamics of heat transfer, and myogenic and metabolic regulation procedures are included. The interactions between these factors were comprehensively exhibited. The influences of arteriolar vasomotion and nonlinear viscoelasticity of blood in arteriole are considered. A simplified vessel network consisting of arteriole, open and reserved capillaries, venule, initial lymphatics and arteriole_venule anastomose is adopted as the geometrical model. This kind of comprehensive mathematical model is helpful in analyzing clinical data and developing a “numerical experiment method” in microcirculation research. 展开更多
关键词 microcirculatory system comprehensive mathematical model inTERACTION numerical experiment
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Seminar教学法在“机器人工程综合应用实验”课程教学中的应用 被引量:1
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作者 段振霞 刘银华 《上海理工大学学报(社会科学版)》 2024年第1期77-82,共6页
“机器人工程综合应用实验”课程是一门多学科交叉的综合性实践类课程,在实际教学过程中,该课程主要以传统的教学模式为主,即教师在课堂上讲解实验原理和实验步骤指导学生完成实验项目,上述授课方式限制了学生学习的自主性和主动性。将S... “机器人工程综合应用实验”课程是一门多学科交叉的综合性实践类课程,在实际教学过程中,该课程主要以传统的教学模式为主,即教师在课堂上讲解实验原理和实验步骤指导学生完成实验项目,上述授课方式限制了学生学习的自主性和主动性。将Seminar教学法引入传统课堂,结合实际教学案例探究该教学模式的应用效果,通过教学实践过程分析其优势与劣势,并针对存在问题给出相应建议。实践证明,在“机器人工程综合应用实验”课程中应用Seminar教学法,可以充分调动学生的课堂积极性,激发学生的创新精神和批判性精神,同时也能提高教师的授课质量和授课水平,研究成果对其他课程引入Seminar教学法的应用实践具有一定借鉴意义。 展开更多
关键词 SEMinAR教学法 机器人工程综合应用实验 教学应用 教学效果
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Global Comprehensive Sensitivity Analysis of Arch Dam Construction Parameters Based on Orthogonal Experiment 被引量:1
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作者 Denghua Zhong Zhiqiang Chu +3 位作者 Bingyu Ren Mengqi Zhao Tao Guan Wenshuai Song 《Transactions of Tianjin University》 EI CAS 2017年第5期427-433,共7页
The construction of arch dams exhibits high uncertainty. Sensitivity analysis of construction parameters is important for the design and optimization of dam construction duration. However, current research cannot full... The construction of arch dams exhibits high uncertainty. Sensitivity analysis of construction parameters is important for the design and optimization of dam construction duration. However, current research cannot fully consider the combined influences of multiple parameters on the total construction. To effectively analyze the duration of arch dam construction, this study proposes a global comprehensive sensitivity analysis method in view of the whole process of arch dam construction based on an orthogonal experiment. This method could comprehensively consider the influence of the construction parameters that may lead to the uncertainty of construction duration. In addition, this method is able to identify the key parameters that may have a significant effect on duration uncertainty and sums up the general rules of combined parameters’ interaction effect, which provides a scientific basis for reasonable optimization of the duration of dam construction. © 2017, Tianjin University and Springer-Verlag GmbH Germany. 展开更多
关键词 Arch dams ARCHES DAMS Uncertainty analysis
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Comprehensive experiment and evaluation on safety due to fully-mechanized mining under the Xitian River at Linxin Mine
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作者 来兴平 任奋华 蔡美峰 《Journal of Coal Science & Engineering(China)》 2004年第2期34-36,共3页
L3414 mechanized mining working face (No.14 coal seam) of Lingxin Mine is under the Xitian River.The mining disturbed zone where rock properties and conditions have been changed due to mining, the safety and environme... L3414 mechanized mining working face (No.14 coal seam) of Lingxin Mine is under the Xitian River.The mining disturbed zone where rock properties and conditions have been changed due to mining, the safety and environmental protection were con- cemed greatly. Based on engineering geological environment of L3414 working face and mining factors, the color bore-bole TV inspecting, leakage of drilling fluid monitoring, simulation experiment, numerical computing, in-situ ground stress measurement and subsidence measurement, etal, these programs contribute to the formation of a scientific basis for control water safe mining and normal mining or environmental protection in the condition of existing fully-mechanized mining. 展开更多
关键词 comprehensive experiment and evaluation existing mining method control water safe mining environmental protection
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A retrospective view on the history of natural sciences in XX-XXI
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作者 Vladislav Sergeyevich Olkhovsky 《Natural Science》 2010年第3期228-245,共18页
The presented paper is dedicated to a new ret-rospective view on the history of natural sci-ences in XX-XXI cc, partially including the sci-ence philosophy (mainly, the problems of the scientific realism, i.e. the cor... The presented paper is dedicated to a new ret-rospective view on the history of natural sci-ences in XX-XXI cc, partially including the sci-ence philosophy (mainly, the problems of the scientific realism, i.e. the correspondence of science to reality) and also a novel scheme for different classes of sciences with different ob-jects and paradigms. There are analyzed the chosen “great” and “grand” problems of phys-ics (including the comprehension of quantum mechanics, with a recently elaborated new chapter, connected with time as a quantum obs- ervable and time analysis of quantum processes) and also of natural sciences as a whole. The particular attention is paid to the interpretation questions and slightly to the aspects, inevitably connected with the world- views of the res- earchers (which do often constitute a part of the interpretation questions). 展开更多
关键词 SCIENCE history SCIENCE realism paradigm PROBLEM of interpretation and comprehension of QUANTUM mechanics the WAVE-FUNCTION collapse the Einstein-Podolsky-Rosen paradox TIME as a QUANTUM observable canonically conjugated to energy maximal hermitian TIME operator TIME analysis of QUANTUM processes relationship be-tween physics and biology PROBLEM of origin of biologic life REDUCTIONISM cosmologic PROBLEM Big Bang anthropic principle
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基于“芳酸结构形貌调控的Zn-MOFs制备表征”构建无机化学综合实验
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作者 吴若雨 查如艳 +1 位作者 李春涯 王炎英 《广州化工》 CAS 2024年第19期180-182,189,共4页
金属有机框架化合物(MOFs)是有机配体与金属离子或金属簇通过配位键组装而成的具有分子内孔隙结构的有机-无机杂化材料,具有比表面积大、孔隙率高、孔径可调、稳定性好等特征,在催化、能源、药物输送及传感等领域广泛应用。MOFs的物性... 金属有机框架化合物(MOFs)是有机配体与金属离子或金属簇通过配位键组装而成的具有分子内孔隙结构的有机-无机杂化材料,具有比表面积大、孔隙率高、孔径可调、稳定性好等特征,在催化、能源、药物输送及传感等领域广泛应用。MOFs的物性特征与其形貌及组成密切相关,故形貌调控至关重要。本文以对苯二甲酸、均苯三甲酸、2,6-萘二羧酸为有机配体,以锌离子为金属中心,采用室温沉淀法制备Zn-MOFs纳米材料体系,基于有机配体调控Zn-MOFs形貌。采用扫描电子显微镜表征其形貌,X-射线衍射光谱表征其晶体结构,红外光谱表征化学组成,紫外可见吸收光谱表征其光谱特性,并修饰至玻碳电极表面,构建光电化学界面,考察三种Zn-MOFs纳米材料的光电转换性能。通过该综合实验,有助于延伸无机化学金属配合物之理论基础,拓展光电化学及化学修饰电极知识领域,有利于强化科研创新意识、提升材料制备及表征相关实验技能、建立数据处理与结果分析的思维模式,有助于培养学生立志创新、勇于探索之精神。 展开更多
关键词 无机化学 综合实验 有机金属框架 锌配合物 形貌调控 芳香多酸
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综合创新实验:功能化COFs在锂硫电池中的应用
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作者 杨延琴 古国贤 韩禄 《广州化工》 CAS 2024年第1期227-231,共5页
将碳纳米管作为载体,通过1,3,5-均苯三甲醛与3,8-二氨基-6-苯基菲啶在乙酸存在下的可逆席夫碱反应,合成了一种碳纳米管支撑的共价有机骨架复合材料(COF@CNT)。并用1,3-丙磺酸内酯将其功能化,进一步得到两性离子功能化的共价有机骨架复... 将碳纳米管作为载体,通过1,3,5-均苯三甲醛与3,8-二氨基-6-苯基菲啶在乙酸存在下的可逆席夫碱反应,合成了一种碳纳米管支撑的共价有机骨架复合材料(COF@CNT)。并用1,3-丙磺酸内酯将其功能化,进一步得到两性离子功能化的共价有机骨架复合材料(ZW-COF@CNT)。将该复合材料作为正极的硫宿主材料组装到锂硫电池中,研究其对电化学性能的影响。本实验涉及抽滤、真空干燥、纽扣电池组装等操作过程,也包括材料表征、电池性能测试等分析过程。 展开更多
关键词 综合创新实验 共价有机骨架 锂硫电池 穿梭效应
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基于Matlab/Simulink的幅度调制与解调综合实验设计 被引量:21
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作者 李露 史振威 周付根 《实验室研究与探索》 CAS 北大核心 2011年第1期96-99,193,共5页
针对数字信号处理实验课程教学中存在的内容单一、知识点零散等问题,以巩固学生理论知识,提高学生实际动手能力为目的,利用Matlab/Simulink软件平台,对"数字信号处理"课程的综合性实验设计进行了探讨和研究。在课程中引入信... 针对数字信号处理实验课程教学中存在的内容单一、知识点零散等问题,以巩固学生理论知识,提高学生实际动手能力为目的,利用Matlab/Simulink软件平台,对"数字信号处理"课程的综合性实验设计进行了探讨和研究。在课程中引入信号的幅度调制与解调综合实验,使学生在了解调制解调基本原理的基础上,灵活运用所学到的数字信号处理知识,如频谱分析、滤波器设计等分析问题和解决问题,并直观地观察实验结果,以此调动学生学习的积极性、自主性和创造性,达到培养学生独立思考、善于创造、综合应用知识的能力。 展开更多
关键词 数字信号处理 综合实验 MATLAB SIMULinK
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基于Linux的智能家居控制系统综合实验设计 被引量:7
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作者 王伟 韩雪 +1 位作者 高照玲 马永刚 《实验技术与管理》 CAS 北大核心 2020年第1期159-162,166,共5页
为提高学生工程实践和创新能力、促进理论教学和实验教学紧密结合,针对嵌入式Linux相关课程,以智能家居控制系统为例,介绍了综合实验设计思路和设计内容,给出阶段性成果。应用表明,基于Linux的智能家居控制系统综合实验设计,在实验教学... 为提高学生工程实践和创新能力、促进理论教学和实验教学紧密结合,针对嵌入式Linux相关课程,以智能家居控制系统为例,介绍了综合实验设计思路和设计内容,给出阶段性成果。应用表明,基于Linux的智能家居控制系统综合实验设计,在实验教学、学生兴趣、学生应用实践能力和创新能力培养和提升等方面都有很好的效果。 展开更多
关键词 智能控制 ARM LinUX 综合实验
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迷你临床演练评量(Mini-CEX)在细胞生物实验教学中的应用 被引量:4
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作者 董静 郑立红 +4 位作者 陈萍 刘丹 吕艳欣 梅庆步 张明龙 《中国继续医学教育》 2016年第36期9-10,共2页
将迷你临床演练评量(Mini-CEX)教学方法应用于《细胞生物学》的实验教学中,针对学生被动灌输的习惯及知识运用时的生搬硬套问题,根据课程特点进行教学方法改革,提高学生的自主学习性和参与度。迅速提高学生的操作能力,利用个性化反馈弥... 将迷你临床演练评量(Mini-CEX)教学方法应用于《细胞生物学》的实验教学中,针对学生被动灌输的习惯及知识运用时的生搬硬套问题,根据课程特点进行教学方法改革,提高学生的自主学习性和参与度。迅速提高学生的操作能力,利用个性化反馈弥补知识框架中的薄弱点,培养学生的综合能力。并设计Mini-CEX评价表及调查问卷,总结反馈意见,实现以考促学、教学相长。现以教学互动理论为依据,旨在提高细胞生物学教学的质量。 展开更多
关键词 MinI-CEX 细胞生物学 以考促学 综合能力
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综合性和创新性实验的设计与实践—Biginelli反应 被引量:12
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作者 王书文 曹玮 李明 《实验室研究与探索》 CAS 2007年第1期100-102,共3页
在室温离子液体作催化剂的条件下,利用苯甲醛、尿素和乙酰乙酸乙酯3组分缩合反应,一锅煮的方法制备3,4-二氢嘧啶-2-酮衍生物。本实验是学生基础实验延伸,并且在学生实验结果统计分析的基础上,分析了本科学生综合创新能力。
关键词 综合和设计性实验 离子液体 BIGinELLI反应 3 4-二氢嘧啶-2(1H)-酮 创新能力
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医学细胞生物学实验教学引入Mini-CEX评价模式的探析 被引量:3
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作者 董静 郑立红 +3 位作者 陈萍 刘丹 吕艳欣 张明龙 《继续医学教育》 2017年第7期59-60,共2页
目的探讨迷你临床演练评量(Mini-CEX)教学模式应用到细胞生物学实验教学中的可行性。方法结合课程特点,采用Mini-CEX教学模式,以考促学,通过教学实践活动给予学生客观综合评价及反馈意见。并对开展Mini-CEX教学模式的实验组和传统教学... 目的探讨迷你临床演练评量(Mini-CEX)教学模式应用到细胞生物学实验教学中的可行性。方法结合课程特点,采用Mini-CEX教学模式,以考促学,通过教学实践活动给予学生客观综合评价及反馈意见。并对开展Mini-CEX教学模式的实验组和传统教学模式的空白对照组分别进行问卷调查。结果开展Mini-CEX教学模式的实验组综合成绩高于空白对照组,学生满意度高,结果差异有统计学意义(P<0.05)。结论 Mini-CEX评价模式应用于医学细胞生物学实验课教学具有可行性,可有效提高教学效果。 展开更多
关键词 迷你临床演练评量 医学细胞生物学 实验教学
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Intel IPP在数字图像处理综合实验中的应用 被引量:3
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作者 滕升华 王芳 +1 位作者 赵增顺 孙农亮 《实验室科学》 2016年第5期76-79,共4页
综合实验是"数字图像处理"教学的重要实践环节,要确保实验质量必须精心组织实验内容、采取有效可行的实验形式。依据数字图像处理课程的特点,阐述了综合实验设计的基本原则;分析不同编程工具的特点及在实验应用中存在的问题,... 综合实验是"数字图像处理"教学的重要实践环节,要确保实验质量必须精心组织实验内容、采取有效可行的实验形式。依据数字图像处理课程的特点,阐述了综合实验设计的基本原则;分析不同编程工具的特点及在实验应用中存在的问题,提出采用C++结合Intel IPP的实验编程方式,并以旧电影去模糊为例对IPP的具体应用进行了探讨。引入IPP丰富了数字图像处理的实验形式,更有助于引导学生利用图像处理知识解决实际问题。 展开更多
关键词 综合实验 数字图像处理 英特尔集成性能基元
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“一锅煮”制备Biginelli和Hantzsch两种产物及其结构分析 被引量:1
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作者 王书文 郭维斯 罗世忠 《化工高等教育》 2019年第2期84-88,共5页
苯甲醛、尿素和乙酰乙酸乙酯三组分"一锅煮"可以同时制备Biginelli和Hantzsch两种产物。教学中通过改变催化剂种类、反应物料比、反应溶剂等条件,引导学生探讨反应条件的改变对总产率及两种异构体比例的影响。实验中通过薄层... 苯甲醛、尿素和乙酰乙酸乙酯三组分"一锅煮"可以同时制备Biginelli和Hantzsch两种产物。教学中通过改变催化剂种类、反应物料比、反应溶剂等条件,引导学生探讨反应条件的改变对总产率及两种异构体比例的影响。实验中通过薄层色谱来跟踪反应进程,通过柱色谱分离混合物,最后通过熔点、红外光谱对合成的化合物进行结构表征。本实验集无机化学、有机化学、基础分析化学和仪器分析于一体,具有很强的实用性和可操作性,可作为有机化学实验中的综合性、设计性实验开设。 展开更多
关键词 综合性、设计性实验 Biginelli产物 Hantzsch产物 结构表征
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