Mechanical properties of AISI 1045 ceramic coated materials by nano indentation and crack opening displacement method

Abstract： An effective approach was conducted for estimating fracture toughness using the crack opening displacement （COD） method for plasma enhanced chemical vapor deposition （PECVD） coating materials. For this evaluation, an elastoplastic analysis was used to estimate critical COD values for single edge notched bending （SENB） specimens. The relationship between fracture toughness （Kic） and critical COD for SENB specimens was obtained. Microstructure of the interface between AleO3-TiO2 composite ceramic coatings and AISI 1045 steel substrates was studied by using scanning electron microscope （SEM）. Chemical compositions were clarified by energy-dispersive X-ray spectroscopy （EDS）. The results show that the interface between of Al203-TiO2 and substrate has mechanical combining. The nanohardness of the coatings can reach 1 200 GPa examined by nanoindentation. The Klc was calculated according to this relationship from critical COD. The bending process produces a significant relationship of COD independent of the axial force applied. Fractographic analysis was conducted to determine the crack length. From the physical analysis of nanoindentation curves, the elastic modulus of 1045/AI2O3-TiO2 is 180 GPa for the 50 μm film. The highest value of fracture toughness for 1045/A1203-TiO2-250 μm is 348 MPa·mv2.

Effect of Coarse Aggregate Size on and Crack Opening in Normal and Relationship between Stress High Strength Concretes

Fine and coarse aggregates play an important role in the fracture of concrete. However, quantitative information available on the effect of the coarse aggregate size on the fracture properties of concrete is still limited. In the present paper, the effect of coarse aggregate size （single grade of 5～10, 10～16, 16～20 and 20～25 mm） on stress-crack opening （σ-w） relation in normal and high strength concretes （compressive strength of 40 and 80 MPa, respectively） was studied. The investigation was based on three-point bending tests implemented by fictitious crack analysis. The result shows that coarse aggregate size and cement matrix strength significantly influence the shape of σ-w curve. For a given total aggregate content, in normal strength concrete, smaller size of aggregate leads to a high tensile strength and a sharp stress drop after the peak stress. The smaller the coarse aggregate, the steeper the σ-w curve. By contrast, in high strength concrete, the effect of aggregate size on σ-w relation almost vanishes. A similar σ-w relation is obtained for the concrete except for the case of 20～25 mm coarse aggregate size. The stress drop after the peak stress is more significant for high strength concrete than that for normal strength concrete. Meanwhile, the smaller the coarse aggregate size, the higher the flexural strength. Fracture energy and characteristic length increase with increasing coarse aggregate size in both normal and high strength concretes.

Repairing of RC T-Section Beams with Opening by CFRP for Cracks and Ultimate Torque

The repair of reinforced concrete(RC)beams with carbon fiber reinforced polymers(CFRP)is experimentally investigated in this study.The four T-section reinforced reactive powder concrete beams with many locations of circular opening were repaired by CFRP and investigated under pure torsion.The repairing beams were tested to obtain the effect of the amount of CFRP laminate on beams cracking and ultimate torque behavior,angle of twist and failure modes.The results obtained from the adopted repairing technique showed a significant effect of external high strength CFRP laminates on effectively restore of section solid of 85%of crack torsional strength effectively restored.In addition,the results show that effectively restoring of section opening by 82%-80%of crack torsional strength,and the adopted repairing technique gives a good strength to the beams.

Critical crack tip opening displacement of different strength concrete

Critical crack tip opening displacement (CTODc) of concrete using experimental and analytical evaluation with seven different compressive strengths ranging from 30 up to 150 MPa was studied based on two types of fracture tests:three-point bending (TPB) and wedge splitting (WS).In the tests,the values of CTODc were experimentally recorded using a novel technique,in which fiber Bragg grating (FBG) sensors were used,and two traditional techniques,in which strain gauges and clip gauges were deployed.The values of CTODc of tested concrete were also predicted using two existing analytical formulae proposed by JENQ & SHAH and XU,respectively.It is found that the values of CTODc obtained by both experimental measurements and analytical formulae exhibit a negligible variation as the compressive strength of concrete increases,and the test geometry adopted has little impact on the value of CTODc.Regarding the experimental measurement of CTODc,the clip gauge method generally leads to a larger value of CTODc and shows a more significant scatter as compared with the other two methods,while the strain gauge method leads to a slightly lower CTODc as compared with the FBG sensor method.The analytical formula proposed by JENQ and SHAH is found to generally lead to an overestimation,while the analytical formula proposed by XU shows a good accuracy.

Effect of loading rates on crack propagating speed,fracture toughness and energy release rate using single-cleavage trapezoidal open specimen under impact loads

The former studies indicate that loading rates significantly affect dynamic behavior of brittle materials,for instance,the dynamic compressive and tensile strength increase with loading rates.However,there still are many unknown or partially unknown aspects.For example,whether loading rates have effect on crack dynamic propagating behavior(propagation toughness,velocity and arrest,etc).To further explore the effect of loading rates on crack dynamic responses,a large-size single-cleavage trapezoidal open(SCTO)specimen was proposed,and impacting tests using the SCTO specimen under drop plate impact were conducted.Crack propagation gauges(CPGs)were employed in measuring impact loads,crack propagation time and velocities.In order to verify the testing result,the corresponding numerical model was established using explicit dynamic software AUTODYN,and the simulation result is basically consistent with the experimental results.The ABAQUS software was used to calculate the dynamic SIFs.The universal function was calculated by fractal method.The experimental-numerical method was employed in determining initiation toughness and propagation toughness.The results indicate that crack propagating velocities,dynamic fracture toughness and energy release rates increase with loading rates;crack delayed initiation time decreases with loading rates.

RIPP Opens a New Route for Catalytic Cracking of Heavy Oil

On January 19,2021 the project“The ring-opening cracking technology of naphthenic-base heavy oil for increasing high-octane gasoline production”undertaken by the SINOPEC Research Institute of Petroleum Processing(RIPP)as the leading institution has passed the review and appraisal.The experts attending the appraisal meeting have unanimously recognized that this project has made remarkable progress through bringing forth new ideas in improving the ring-opening cracking process of naphthenic-base heavy oil to form a SINOPEC’s new platform of catalytic cracking technology with independent intellectual property rights and free operation rights.

Analytical solution for the effective elastic properties of rocks with the tilted penny-shaped cracks in the transversely isotropic background

Seismic prediction of cracks is of great significance in many disciplines,for which the rock physics model is indispensable.However,up to now,multitudinous analytical models focus primarily on the cracked rock with the isotropic background,while the explicit model for the cracked rock with the anisotropic background is rarely investigated in spite of such case being often encountered in the earth.Hence,we first studied dependences of the crack opening displacement tensors on the crack dip angle in the coordinate systems formed by symmetry planes of the crack and the background anisotropy,respectively,by forty groups of numerical experiments.Based on the conclusion from the experiments,the analytical solution was derived for the effective elastic properties of the rock with the inclined penny-shaped cracks in the transversely isotropic background.Further,we comprehensively analyzed,according to the developed model,effects of the crack dip angle,background anisotropy,filling fluid and crack density on the effective elastic properties of the cracked rock.The analysis results indicate that the dip angle and background anisotropy can significantly either enhance or weaken the anisotropy degrees of the P-and SH-wave velocities,whereas they have relatively small effects on the SV-wave velocity anisotropy.Moreover,the filling fluid can increase the stiffness coefficients related to the compressional modulus by reducing crack compliance parameters,while its effects on shear coefficients depend on the crack dip angle.The increasing crack density reduces velocities of the dry rock,and decreasing rates of the velocities are affected by the crack dip angle.By comparing with exact numerical results and experimental data,it was demonstrated that the proposed model can achieve high-precision estimations of stiffness coefficients.Moreover,the assumption of the weakly anisotropic background results in the consistency between the proposed model and Hudson's published theory for the orthorhombic rock.

CLOSED-FORM WEIGHT FUNCTION FOR EDGE CRACK PROBLEMS

An accurate crack surface opening displacement formula for edge cracks in finite bodies has been derived,and was subsequently used to develop wide-range closed-form weight functions for edge cracks. The analytical weight function is general and can be easily used to determine accurate stress intensity factors and crack surface opening displacements for arbitrarily loaded edge cracks with high efficiency.Examples have been given for problems of edge crack(s)with a number of typical load conditions for illustration.

Seismic stability analysis of concrete gravity dams with penetrated cracks

The seismic stability of a cracked dam was examined in this study. Geometric nonlinearity and large deformations, as well as the contact condition at the crack site, were taken into consideration. The location of penetrated cracks was first identified using the concrete plastic-damage model based on the nonlinear finite element method （FEM）. Then, the hard contact algorithm was used to simulate the crack interaction in the normal direction, and the Coloumb friction model was used to simulate the crack interaction in the tangential direction. After verification of numerical models through a case study, the seismic stability of the Koyna Dam with two types of penetrated cracks is discussed in detail with different seismic peak accelerations, and the collapse processes of the cracked dam are also presented. The results show that the stability of the dam with two types of penetrated cracks can be ensured in an earthquake with a magnitude of the original Koyna earthquake, and the cracked dam has a large earthquake-resistant margin. The failure processes of the cracked dam in strong earthquakes can be divided into two stages： the sliding stage and the overturning stage. The sliding stage ends near the peak acceleration, and the top block slides a long distance along the crack before the collapse occurs. The maximum sliding displacement of the top block will decrease with an increasing friction coefficient at the crack site.

Modeling of Fatigue Crack Growth Closure Considering the Integrative Effect of Cyclic Stress Ratio,Specimen Thickness and Poisson's Ratio

Key components of large structures in aeronautics industry are required to be made light and have long enough fatigue lives.It is of vital importance to estimate the fatigue life of these structures accurately.Since the FCG process is affected by various factors,no universal model exists due to the complexity of the mechanisms.Most of the existing models are obtained by fitting the experimental data and could hardly describe the integrative effect of most existing factors simultaneously.In order to account for the integrative effect of specimen parameters,material property and loading conditions on FCG process,a new model named integrative influence factor model（IIF） is proposed based on the plasticity-induced crack closure theory.Accordingly to the predictions of crack opening ratio（γ） and effective stress intensity factor range ratio（U） with different material under various loading conditions,predictions of γ and U by the IIF model are completely identical to the theoretical results from the plane stress state to the plane strain state when Poisson＇s ratio equals 1/3.When Poisson＇s ratio equals 0.3,predictions of γ and U by the IIF model are larger than the predictions by the existing model,and more close to the theoretical results.In addition,it describes the influence of R ratios on γ and U effectively in the whole region from-1.0 to 1.0.Moreover,several sets of test data of FCG rates in 5 kinds of aluminum alloys with various specimen thicknesses under different loading conditions are used to validate the IIF model,most of the test data are situated on the predicted curves or between the two curves that represent the specimen with different thicknesses under the same stress ratio.Some of the test data slightly departure from the predictions by the IIF model due to the surface roughness and errors in measurement.Besides,based on the analysis of the physical rule of crack opening ratios,a relative thickness of specimen is defined to describe the influence of material property,specimen thickness and so forth on FCG characteristics conveniently.In conclusion,the relative thickness of specimen simplifies the expression of FCG characteristic and provides a general parameter to analyze the fatigue characteristics of different materials with various thicknesses under different loading conditions.The IIF model describes the integrative effect of existing influence factors explicitly and quantitatively,and provides a helpful tool for fatigue property estimation of practical component and experiment design.

Strip-coalesced interior zone model for two unequal collinear cracks weakening piezoelectric media

In this paper, a mathematical strip-saturation model is proposed for a poled transversely isotropic piezoelectric plate weakened by two impermeable unequal-collinear hairline straight cracks. Remotely applied in-plane unidirectional electromechanical loads open the cracks in mode-I such that the saturation zone developed at the interior tips of cracks gets coalesced. The developed saturation zones are arrested by distributing over their rims in-plane normal cohesive electrical displacement. The problem is solved using the Stroh formalism and the complex variable technique. The expressions are derived for the stress intensity factors （SIFs）, the lengths of the saturation zones developed, the crack opening displacement （COD）, and the energy release rate. An illustrative numerical case study is presented for the poled PZT-5H ceramic to investigate the effect of prescribed electromechanical loads on parameters affecting crack arrest. Also, the effect of different lengths of cracks on the SIFs and the local energy release rate （LERR） has been studied. The results obtained are graphically presented and analyzed.

SLOW PROPAGATION OF FATIGUE CRACK NEAR THRESHOLD

The effect of pearlite interlamellar spacing(d)from 0.31 to 0.77 μm of T8 steel on fatigue crack propagation near threshold has been investigated at different stress ratios(R).The closure stress intensity factor(K_(cl)),the threshold value(ΔK_(th))and crack tip opening dis- placement range(ΔCOD)were measured.The results show that pearlite interlamellar spac- ing in this range has no effect on K_(cl),but has effect on the threshold value in low stress ratio. The threshold value is higher for materials with larger interlamellar spacing.No matter what the stress ratio is,during the propagation near threshold,the propagation rate will be the same,provieded the crack tip opening displacement range is the same. Metallurgical examinations were also carried out to show that the crack propagation path is sensitive to mierostructure.The crack always propagates along either boundary of pearlite colony or ferrite lamellar in pearlite.

Solution of stress intensity factors of multiple cracks in plane elasticity with eigen COD formulation of boundary integral equation

The concept of eigen crack opening displacement （COD） can be defined as the COD of a crack in infinite plate under the tractions acting on the crack surface. By introducing this concept, the eigen COD formulation of boundary integral equation is proposed in this paper, together with the solution procedures for multiple crack problems in plane elasticity. With the proposed approach, the multiple crack problems can be solved with the conventional displacement discontinuity boundary integral equations in an iterative fashion with a small size of system matrix as that in the numerical Green’s function （NGF） approach but without the trouble to determine the complementary solutions since the standard boundary element discretization on the crack surface is no longer required with the proposed approach. Some numerical examples computing the stress intensity factors are presented and compared with those in literature to show the accuracy and the effectiveness of the proposed approach.

Digital image correlation based high-speed crack tip locatingmethod and its application

Based on a digital image correlation（DIC）method with the measurements of a high speed crack＇s displacement and strain fields,a technique to accurately and automatically locate its crack tip has been developed.The crack tip is identified by finding the abrupt jump on the opening（or dislocation）curve of a point on the trace of the crack propagation,while the opening is measured through a virtual extensometer technique and the abrupt jump is identified by finding the peak on the curve.The method was verified using a specially designed experiment and applied to measure the critical crack tip opening angle of a rock sample.Because the involvement of analytical models has been avoided and then the good performance could be ensured for low resolution speckle images,this technique is expected to be very useful in the quantitative study of high speed cracks in experiments using high speed cameras.

PERIODICAL INTERFACIAL CRACKS IN ANISOTROPIC ELASTOPLASTIC MEDIA

By using Fourier transformation the boundary problem of periodical interfacial cracks in anisotropic elastoplastic bimaterial was transformed into a set of dual integral equations and then it was further reduced by means of definite integral transformation into a group of singular equations. Closed form of its solution was obtained and three corresponding problems of isotropic bimaterial, of a single anisotropic material and of a bimaterial of isotropy- anisotropy were treated as the specific cases. The plastic zone length of the crack tip and crack openning displacement ( COD) decline as the smaller yield limit of the two bonded materials rises, and they were also determined by crack length and the space between two neighboring cracks . In addition , COD also relates it with moduli of the materials .

Stability analysis of the sliding process of the west slope in Buzhaoba Open-Pit Mine

To study the stability of the west slope in Buzhaoba Open-Pit Mine and determine the aging stability coefficient during slide mass development, the deformation band of the west slope and the slide mass structure of the 34,600 profile are obtained on the basis of hydrology, geology, and monitoring data.The residual thrust method is utilized to calculate the stability coefficients, which are 1.225 and 1.00 under sound and transfixion conditions, respectively. According to the rock damage and fragmentation and the principle of mechanical parameter degradation, the mechanical models of the slide mass development of the hard and soft rock slopes are established. An integrated model for calculating the slope stability coefficient is built considering water, vibration, and other external factors that pertain to the structural plane damage mechanism and the generating mechanism of the sliding mass. The change curve of the stability coefficient in the slide mass development is obtained from the relevant analyses,and afterwards, the stability control measures are proposed. The analysis results indicate that in the cracking stage of the hard rock, the slope stability coefficient decreases linearly with the increase in the length Lbof the hard rock crack zone. The linear slope is positively correlated to rock cohesion c. In the transfixion stage of the soft rock, the decrease speed of the stability coefficient is positively correlated to the residual strength of the soft rock. When the slope is stable, the stability coefficient is in a quadratic-linear relationship with the decreased height Dh of the side slope and in a linear relationship with anchoring force P.

Engineering critical assessment on welding flaws of the X65 UOE girth weld based on CRACKWISE

Focused on the girth weld of a φ762 x 28.6 mm （X65） offshore UOE pipe, the fracture toughness properties at different weld joint positions were tested. Meanwhile,the largest size of different cracks under service condition was calculated by using CRACKWISE. The service life of the UOE pipe with postulated crack-like flaws was calculated by considering various fatigue factors, such as vibrations caused by ocean current and fluctuations of inner pressure. The assessment process and results can be used to direct the repair of weld flaws laid in pipes or to assess the reliability of in-serving pipes.

Mechanistic Insights into the Catalytic Cracking of Cyclohexane

Although naphthenes have long been identified as important feedstock components for the production of light olefins and aromatics in fluid catalytic cracking units,their cacking mechanism and microscopic reaction networks,such as activation modes,ring-opening paths,and the production of aromatics,remain debated.In this context,we reported experimental and computational work aimed at elucidating the reaction network of naphthenes in fluid catalytic cracking using cyclohexane as the model naphthene.First,the main reactions for the formation of highly selective and value-added products such as light olefins and aromatics were discussed.Then,the proportions of cyclohexane activation via(i)the non-classical carbonium mechanism and(ii)the classical carbenium mechanism were analyzed by data fitting methods,which revealed that around 32.6%of cyclohexane was initiated by path(i),and the remaining naphthene was activated by path(ii).Moreover,our DFT results showed that the ring opening of cyclohexane through pathway(i)was more difficult than that through path(ii),and ring opening followed by the ring contraction of cyclohexane carbenium ions was the most energetically favorable route among the different ring-opening ways.

Numerical Comparison Research on the Solution of Stress Intensity Factors of Multiple Crack Problems

A newly developed approach without crack surface discretization for modeling 2D solids with large number of cracks in linear elastic fracture mechanics is proposed with the eigen crack opening displacement (COD) boundary integral equations in this paper. The eigen COD is defined as a crack in an infinite domain under fictitious traction acting on the crack surface. Respect to the computational accuracies and efficiencies, the multiple crack problems in finite and infinite plates are solved and compared numerically using three different kinds of boundary integral equations (BIEs): 1) the dual BIEs require crack surface discretization;2) the BIEs with numerical Green’s functions (NGF) without crack surface discretization, but have to solve a complementary matrix;3) the eigen crack opening displacement (COD) BIEs in the present paper. With the concept of eigen COD, the multiple crack problems can be solved by using a conventional displacement discontinuity boundary integral equation in an iterative fashion with a small size of system matrix as that in the NGF approach, but without troubles to determine the complementary matrix. Solution of the stress intensity factors of multiple crack problems is solved and compared in some numerical examples using the above three computational algorithms. Numerical results clearly demonstrate the numerical models of eigen COD BIEs have much higher efficiency, providing a newly numerical technique for multiple crack problems. Not only the accuracy and efficiency of computation can be guaranteed, but also the overall properties and local details can be obtained. In conclusion, the numerical models of eigen COD BIEs realize the simulations for multiple crack problems with large quantity of cracks.

A Straightforward Direct Traction Boundary Integral Method for Two-Dimensional Crack Problems Simulation of Linear Elastic Materials

This paper presents a direct traction boundary integral equation method(DTBIEM)for two-dimensional crack problems of materials.The traction boundary integral equation was collocated on both the external boundary and either side of the crack surfaces.The displacements and tractions were used as unknowns on the external boundary,while the relative crack opening displacement(RCOD)was chosen as unknowns on either side of crack surfaces to keep the single-domain merit.Only one side of the crack surfaces was concerned and needed to be discretized,thus the proposed method resulted in a smaller system of algebraic equations compared with the dual boundary element method(DBEM).A new set of crack-tip shape functions was constructed to represent the strain field singularity exactly,and the SIFs were evaluated by the extrapolation of the RCOD.Numerical examples for both straight and curved cracks are given to validate the accuracy and efficiency of the presented method.