Cryogenic strength,ductility and toughness of AI-Li alloy 8090 were found to be superior to those at ambient temperature,and up to optima at about 20 K.Different aging regimes may only influence on its cryogenic yield...Cryogenic strength,ductility and toughness of AI-Li alloy 8090 were found to be superior to those at ambient temperature,and up to optima at about 20 K.Different aging regimes may only influence on its cryogenic yield strength and elongation.展开更多
The influence of soaking time in deep cryogenic treatment on the tensile and impact properties of low-alloy medium-carbon HY-TUF steel was investigated in this study. Microstructural studies based on phase distributio...The influence of soaking time in deep cryogenic treatment on the tensile and impact properties of low-alloy medium-carbon HY-TUF steel was investigated in this study. Microstructural studies based on phase distribution mapping by electron backscatter diffraction show that the deep cryogenic process causes a decrease in the content of retained austenite and an increase in the volume fraction of η-carbide with increasing soaking time up to 48 h. The decrease in the content of retained austenite from ~1.23vol% to 0.48vol% suggests an isothermal martensitic transformation at 77 K. The η-type precipitates formed in deep cryogenic-treated martensite over 48 h have the Hirotsu and Nagakura orientation relation with the martensitic matrix. Furthermore, a high coherency between η-carbide and the martensitic matrix is observed by high-resolution transmission electron microscopy. The variations in macrohardness, yield strength, ultimate tensile strength, and ductility with soaking time in the deep cryogenic process show a peak/plateau trend.展开更多
The effect of Mn content on the microstructure and cryogenic mechanical properties of a 7% Ni steel was investigated within the Mn content range from 0.13% to 0.36%. The microstructure of the steel as determined by op...The effect of Mn content on the microstructure and cryogenic mechanical properties of a 7% Ni steel was investigated within the Mn content range from 0.13% to 0.36%. The microstructure of the steel as determined by optical microscopy, scanning electron microscopy, transmission electron microscopy, electron backscattering diffraction and X-ray diffraction was presented, and the low-temperature mechanical properties were given. The size of prior austenite grain did not change a lot as Mn content increased. Film-like reversed austenite, having high stability, was found mainly in the specimens with lower Mn content; however, in the specimen with the highest Mn content, the role of Mn was not obvious in stabilizing reversed austenite. Besides, with increasing Mn content, the amount of reversed austenite at grain boundaries gradually decreased. The variable Mn content had a significant effect on cryogenic toughness~ but not apparent on cryogenic tensile strength or yield strength. An excellent combination of cryogenic tensile and impact properties was obtained when Mn content of steel was 0.13%.展开更多
The influence of Nb content on the microstructure and cryogenic mechanical properties of a 7%Ni steel was investigated within the Nb content range from 0 to 0.05%. The microstructure was characterized by optical micro...The influence of Nb content on the microstructure and cryogenic mechanical properties of a 7%Ni steel was investigated within the Nb content range from 0 to 0.05%. The microstructure was characterized by optical microscope, scanning electron microscope, transmission electron microscopy and X-ray diffraction, and the low-temperature mechanical property tests were conducted. The Nb addition can effectively refine the prior austenite grains and microstructure of the steel. Fine niobium precipitates with a diameter of about 10-50 nm were observed. They tend to be spherical and locate mainly in the vicinity of grain boundaries. Although there are considerable amounts of reversed austenite forming at grain boundaries in the specimen containing the highest Nb content, no Nb element was detected in such reversed austenite, which implies that Nb element did not affect the formation of the reversed austenite directly. Mechanical test results suggest that the strength of the 7%Ni steel is not simply in relation to the prior austenite grain size, but also depends on the amount of reversed austenite. On the other hand, the grain refinement, enhanced with increasing Nb content, has a good effect on cryogenic toughness.展开更多
To further improve the mechanical performance of a new alloyed austempered ductile iron(ADI), deep cryogenic treatment(DCT) has been adopted to investigate the effect of DCT time on the microstructure and mechanic...To further improve the mechanical performance of a new alloyed austempered ductile iron(ADI), deep cryogenic treatment(DCT) has been adopted to investigate the effect of DCT time on the microstructure and mechanical behaviors of the alloyed ADI Fe-3.55 C-1.97 Si-3.79 Ni-0.71 Cu-0.92 Mo-0.64 Cr-0.36 Mn-0.30 V(in wt.%). With increasing the DCT time, more austenite transformed to martensite and very fine carbides precipitated in martensite in the extended period of DCT. The amount of austenite decreased in alloyed ductile irons, while that of martensite and carbide precipitation increased. The alloyed ADI after DCT for 6 h had the highest hardness and compressive strength, which can be attributed to the formation of more plate-like martensite and the finely precipitated carbides. There was a gradual decrease in hardness and compressive strength with increasing the DCT time to 12 h because of the dissolution of M3 C carbide. After tempering, there was a decrease in mechanical properties compared to the direct DCT sample, which was caused by the occurrence of Ostwald ripening of precipitated carbides. The optimum wear resistance was achieved for the alloyed ADI after DCT for 6 h. The wear mechanism of the alloyed ADI in associating with DCT is mainly consisted of micro-cutting wear and some plastic deformation wear.展开更多
文摘Cryogenic strength,ductility and toughness of AI-Li alloy 8090 were found to be superior to those at ambient temperature,and up to optima at about 20 K.Different aging regimes may only influence on its cryogenic yield strength and elongation.
文摘The influence of soaking time in deep cryogenic treatment on the tensile and impact properties of low-alloy medium-carbon HY-TUF steel was investigated in this study. Microstructural studies based on phase distribution mapping by electron backscatter diffraction show that the deep cryogenic process causes a decrease in the content of retained austenite and an increase in the volume fraction of η-carbide with increasing soaking time up to 48 h. The decrease in the content of retained austenite from ~1.23vol% to 0.48vol% suggests an isothermal martensitic transformation at 77 K. The η-type precipitates formed in deep cryogenic-treated martensite over 48 h have the Hirotsu and Nagakura orientation relation with the martensitic matrix. Furthermore, a high coherency between η-carbide and the martensitic matrix is observed by high-resolution transmission electron microscopy. The variations in macrohardness, yield strength, ultimate tensile strength, and ductility with soaking time in the deep cryogenic process show a peak/plateau trend.
基金financially supported by Wuhan Iron and Steel(Group)Corp
文摘The effect of Mn content on the microstructure and cryogenic mechanical properties of a 7% Ni steel was investigated within the Mn content range from 0.13% to 0.36%. The microstructure of the steel as determined by optical microscopy, scanning electron microscopy, transmission electron microscopy, electron backscattering diffraction and X-ray diffraction was presented, and the low-temperature mechanical properties were given. The size of prior austenite grain did not change a lot as Mn content increased. Film-like reversed austenite, having high stability, was found mainly in the specimens with lower Mn content; however, in the specimen with the highest Mn content, the role of Mn was not obvious in stabilizing reversed austenite. Besides, with increasing Mn content, the amount of reversed austenite at grain boundaries gradually decreased. The variable Mn content had a significant effect on cryogenic toughness~ but not apparent on cryogenic tensile strength or yield strength. An excellent combination of cryogenic tensile and impact properties was obtained when Mn content of steel was 0.13%.
基金financially supported by Wuhan Iron&Steel Co.,Ltd.
文摘The influence of Nb content on the microstructure and cryogenic mechanical properties of a 7%Ni steel was investigated within the Nb content range from 0 to 0.05%. The microstructure was characterized by optical microscope, scanning electron microscope, transmission electron microscopy and X-ray diffraction, and the low-temperature mechanical property tests were conducted. The Nb addition can effectively refine the prior austenite grains and microstructure of the steel. Fine niobium precipitates with a diameter of about 10-50 nm were observed. They tend to be spherical and locate mainly in the vicinity of grain boundaries. Although there are considerable amounts of reversed austenite forming at grain boundaries in the specimen containing the highest Nb content, no Nb element was detected in such reversed austenite, which implies that Nb element did not affect the formation of the reversed austenite directly. Mechanical test results suggest that the strength of the 7%Ni steel is not simply in relation to the prior austenite grain size, but also depends on the amount of reversed austenite. On the other hand, the grain refinement, enhanced with increasing Nb content, has a good effect on cryogenic toughness.
基金Financial support from the National High Technology Research and Development Program of China(No.2012AA03A508)is greatly appreciated
文摘To further improve the mechanical performance of a new alloyed austempered ductile iron(ADI), deep cryogenic treatment(DCT) has been adopted to investigate the effect of DCT time on the microstructure and mechanical behaviors of the alloyed ADI Fe-3.55 C-1.97 Si-3.79 Ni-0.71 Cu-0.92 Mo-0.64 Cr-0.36 Mn-0.30 V(in wt.%). With increasing the DCT time, more austenite transformed to martensite and very fine carbides precipitated in martensite in the extended period of DCT. The amount of austenite decreased in alloyed ductile irons, while that of martensite and carbide precipitation increased. The alloyed ADI after DCT for 6 h had the highest hardness and compressive strength, which can be attributed to the formation of more plate-like martensite and the finely precipitated carbides. There was a gradual decrease in hardness and compressive strength with increasing the DCT time to 12 h because of the dissolution of M3 C carbide. After tempering, there was a decrease in mechanical properties compared to the direct DCT sample, which was caused by the occurrence of Ostwald ripening of precipitated carbides. The optimum wear resistance was achieved for the alloyed ADI after DCT for 6 h. The wear mechanism of the alloyed ADI in associating with DCT is mainly consisted of micro-cutting wear and some plastic deformation wear.