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Interplay between polarization rotation and crack propagation in PMN-PT relaxor single crystals 被引量:2
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作者 Fei Fang Wenqi Jing Wei Yang 《Theoretical & Applied Mechanics Letters》 CAS 2014年第5期18-23,共6页
Investigations on the interconnection between the polarization rotation and crack propagation are performed for [110J-oriented 74Pb(Mg1/3Nb2/3)O3- 26PbTiO3 relaxor ferroelectric single crystal under electric loading... Investigations on the interconnection between the polarization rotation and crack propagation are performed for [110J-oriented 74Pb(Mg1/3Nb2/3)O3- 26PbTiO3 relaxor ferroelectric single crystal under electric loadings along [001] direction. The crystal is of predominantly monoclinic MA phase with scatter dis- tributed rhombohedral (R) phase under a moderate poling field of 900 V/mm in [00l] direction. With magnitude of 800 V/ram, a through thickness crack is initi- ated near the electrode by electric cycling. Static electric loadings is then imposed to the single crystal. As the applied static electric field increases, domain switch- ing in the monoclinic MA phase and phase transition from MA to R phase occur near the crack. The results indicate that the crack features a conducting one. Whether domain switching or phase transition occurs depends on the intensity of the electric field component that is perpendicular to the applied electric field. 展开更多
关键词 ferroelectric single crystals relaxor crack propagation phase transition re-laibility
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Crack growth behavior of SRR99 single crystal superalloy under thermal fatigue 被引量:2
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作者 LIU Yuan YU Jinjiang +3 位作者 XU Yan SUN Xiaofeng GUAN Hengrong HU Zhuangqi 《Rare Metals》 SCIE EI CAS CSCD 2008年第5期526-530,共5页
The thermal fatigue behavior of a single crystal superalloy SRR99 was investigated. Specimens with V-type notch were tested at the peak temperatures of 900, 1000, and 1100℃. The crack growth curves as a function of t... The thermal fatigue behavior of a single crystal superalloy SRR99 was investigated. Specimens with V-type notch were tested at the peak temperatures of 900, 1000, and 1100℃. The crack growth curves as a function of the number of cycles were plotted. With the increase of peak temperature, the crack initiation life was shortened dramatically. Through optical microscopy (OM) and scanning electron microscopy (SEM) observation, it was found that multiple small cracks nucleated at the notch tip region but only one or two of them continued to develop in the following thermal cycles. The primary cracks generally propagated along a preferential direction. Microstructure changes after thermal fatigue were also discussed on the basis of SEM observation. 展开更多
关键词 single crystal superalloy thermal fatigue crack growth behavior dendrite orientation
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THE NEAR TIP STRESS AND STRAIN FIELDS IN CRACKED SINGLE CRYSTALS
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作者 张永伟 王自强 《Acta Mechanica Sinica》 SCIE EI CAS CSCD 1994年第3期250-259,共10页
The numerical analyses of stationary mathematically sharp Mode I crack in FCC and BCC crystals with elastic-ideally plastic(EIP)and fast hardening saturation(FHS)law are carried out in the present paper.From the calcu... The numerical analyses of stationary mathematically sharp Mode I crack in FCC and BCC crystals with elastic-ideally plastic(EIP)and fast hardening saturation(FHS)law are carried out in the present paper.From the calculated re- sults,it is shown that:for the cases of small strain,EIP crystal cracks,the features of concentrated deformation patterns and the stress state in near-crack tip deforma- tion fields are identical to the earlier analytical solutions,but along the angular sector boundaries,there exist narrow complex stress zones.The overall characteristics of de- formation patterns for the cases of EIP and FHS are similar.The behaviours of crack tip opening can be characterized by crack-tip-opening-displacement(CTOD).For the case of FHS,finite deformation BCC crystal crack,our calculations are qualitatively in agreement with recent experimental observations. 展开更多
关键词 single crystal crack stress field finite element
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Real-time quantitative optical method to study temperature dependence of crack propagation process in colloidal photonic crystal film
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作者 林冬风 徐余颛 +4 位作者 石将建 张瑜 罗艳红 李冬梅 孟庆波 《Chinese Physics B》 SCIE EI CAS CSCD 2015年第7期518-523,共6页
A real-time quantitative optical method to characterize crack propagation in colloidal photonic crystal film(CPCF)is developed based on particle deformation models and previous real-time crack observations. The crac... A real-time quantitative optical method to characterize crack propagation in colloidal photonic crystal film(CPCF)is developed based on particle deformation models and previous real-time crack observations. The crack propagation process and temperature dependence of the crack propagation rate in CPCF are investigated. By this method, the crack propagation rate is found to slow down gradually to zero when cracks become more numerous and dense. Meanwhile, with the temperature increasing, the crack propagation rate constant decreases. The negative temperature dependence of the crack propagation rate is due to the increase of van der Waals attraction, which finally results in the decrease of resultant force. The findings provide new insight into the crack propagation process in CPCF. 展开更多
关键词 colloidal photonic crystal crack propagation TEMPERATURE real-time quantitative optical method
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IN-SITU OBSERVATION OF CRACK PROPAGATION IN PST CRYSTALS OF Ti-49% AlALLOY
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作者 Lu, Yonghao Zhang, Yonggang Chen, Changqi 《中国有色金属学会会刊:英文版》 EI CSCD 1999年第1期65-71,共7页
1INTRODUCTIONγTiAlbasealoyhasbeenofmuchinterestasstructuralmaterialsforelevatedtemperatureaerospaceapplicat... 1INTRODUCTIONγTiAlbasealoyhasbeenofmuchinterestasstructuralmaterialsforelevatedtemperatureaerospaceapplicationsbecauseofitsl... 展开更多
关键词 PST crystal fracture behavior crack PATH TOUGHNESS mechanism
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Exact analytic solutions for an elliptic hole with asymmetric collinear cracks in a one-dimensional hexagonal quasi-crystal 被引量:18
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作者 郭俊宏 刘官厅 《Chinese Physics B》 SCIE EI CAS CSCD 2008年第7期2610-2620,共11页
Using the complex variable function method and the technique of conformal mapping, the anti-plane shear problem of an elliptic hole with asymmetric colfinear cracks in a one-dimensional hexagonal quasi-crystal is solv... Using the complex variable function method and the technique of conformal mapping, the anti-plane shear problem of an elliptic hole with asymmetric colfinear cracks in a one-dimensional hexagonal quasi-crystal is solved, and the exact analytic solutions of the stress intensity factors (SIFs) for mode Ⅲ problem are obtained. Under the limiting conditions, the present results reduce to the Griffith crack and many new results obtained as well, such as the circular hole with asymmetric collinear cracks, the elliptic hole with a straight crack, the mode T crack, the cross crack and so on. As far as the phonon field is concerned, these results, which play an important role in many practical and theoretical applications, are shown to be in good agreement with the classical results. 展开更多
关键词 one-dimensional hexagonal quasi-crystals elliptic hole with asymmetric collinear cracks stress intensity factor complex variable function method
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Effect of Lamellar Orientation on Crack Paths in PST Crystals of γ-TiAl BasedAlloys
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作者 Yonghao Lu Lijie Qiao +1 位作者 Yanbin ining chang Chu(Material Science and Engineering School, University of Science and Technology’ Beijing, Beijing 100083, China) 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 1999年第4期272-276,共5页
The effect of lamellar orientation on crack paths in PST crystals of y-TiAl based alloys was investigated by in-situ SEM technique. The results indicate that the crack paths in PST crystals of y-TiAl based alloys are ... The effect of lamellar orientation on crack paths in PST crystals of y-TiAl based alloys was investigated by in-situ SEM technique. The results indicate that the crack paths in PST crystals of y-TiAl based alloys are strongly dependent on lamellar orientation ofPST crystals, and the differently oriented PST crystals show different nucleation and propagation mechanisms of crack, resulting in different levels of fracture toughness. 展开更多
关键词 γ-TiAl based alloy PST crystal lamellar orientation crack path
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Growth of Casting Microcrack and Micropore in Single-crystal Superalloys Analysed by Three-Dimensional Unit Cell
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作者 Jiansong WAN Zhenzhou LU Zhufeng YUE 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2006年第2期183-189,共7页
Finite element (FE) analysis was employed to investigate the casting microcrack and micropore growth in nickel-base single-crystal superalloys DD3. Based on the finite deformation rate-dependent crystallographic con... Finite element (FE) analysis was employed to investigate the casting microcrack and micropore growth in nickel-base single-crystal superalloys DD3. Based on the finite deformation rate-dependent crystallographic constitutive equation, the simulations of casting microcrack and micropore growth in three-dimensional unit cell model were carried out in a range of parameters including stress triaxiality, Lode parameter and type of activated slip systems. The FE results show that the stress triaxiality has profound effects on growth behavior, and the Lode parameter is also important for the casting microcrack and micropore growth. The type of operative slip systems has remarkable effect on casting microcrack and micropore growth, so the life of single- crystal component is associated with the type of activated slip systems, which is related to Schmid factor and the number of activated slip systems. The growth comparison between microcrack and micropore reveals that when the material is subjected to large deformation, the growth rate of microcrack is faster than that of micropore, i.e. microcrack is more dangerous than micropore; the microcrack is easier to result in brittle fracture than micropore. The stress triaxiality and Lode parameter have strong influence on the growth of microcrack and micropore. 展开更多
关键词 Casting micropore Casting crack Single-crystal superalloys crystallographic constitutive equation
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考虑应力梯度的缺口疲劳分散性研究 被引量:1
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作者 郑战光 谢羿吉 +2 位作者 孙腾 谢昌吉 黄增 《塑性工程学报》 CAS CSCD 北大核心 2024年第1期223-230,共8页
针对缺口部位的微观结构及尺寸导致的疲劳分散差异较大的问题,为准确预测缺口件的疲劳分散性,以矩形截面缺口件为例,采用宏观Chaboche循环塑性本构模型与细观晶体循环塑性本构模型相结合的有限元子模型方法,并考虑缺口效应,提出了以应... 针对缺口部位的微观结构及尺寸导致的疲劳分散差异较大的问题,为准确预测缺口件的疲劳分散性,以矩形截面缺口件为例,采用宏观Chaboche循环塑性本构模型与细观晶体循环塑性本构模型相结合的有限元子模型方法,并考虑缺口效应,提出了以应力梯度影响因子、等效应力与纵向应变为变量的统计标准差作为疲劳指示因子FIP_(notch)。在不同位移载荷、位移载荷比和缺口直径大小情况下将疲劳指示因子FIP_(notch)与经典的Fatemi-Socie疲劳指示因子FIP FS进行疲劳分散性的比较与分析。结果表明:疲劳指示因子FIP_(notch)均能很好地预测不同位移载荷、位移载荷比和缺口直径下的缺口疲劳分散性,且比经典的FIP FS方法有更高的精度与适用性。 展开更多
关键词 疲劳分散性 晶体塑性 裂纹萌生驱动力 疲劳指示因子
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Dislocation Behaviour near the Crack Tip in Bulk Fe-3% Si Single Crystal
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作者 徐永波 哈宽富 +2 位作者 王中光 杨春松 戴忠玲 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 1991年第1期35-39,共5页
An investigation has been made of the disloca- tion distribution and dislocation free zone near the crack tip in bulk Fe-3% Si single crystal during deformation in SEM.It has been found that a number of dislocations w... An investigation has been made of the disloca- tion distribution and dislocation free zone near the crack tip in bulk Fe-3% Si single crystal during deformation in SEM.It has been found that a number of dislocations were emitted from the crack tip during deformation.After that,the dislocations moved rapidly away from the crack tip,which indi- cated that they were strongly repelled by the stress field at the crack tip.Between the crack tip and the plastic zone there is a region of dislocation-free, which is referred to as dislocation-free zone (DFZ). The length of DFZs is roughly estimated 100 μm which is much longer than that found in thin foil specimen.The variation of dislocation density as a function of the distance from the crack tip was measured,which showed that the dislocations are inversely piled up in the plastic zone.The length of DFZs increased with both the length of pre-crack and the amplitude of applied stress. 展开更多
关键词 DISLOCATION crack tip DFZ Fe-3%Si single crystal
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激光定向能量沉积DD405单晶高温合金的裂纹形成机制研究
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作者 李金国 郭以沫 +5 位作者 卢楠楠 朱泓雨 梁静静 张光睿 周亦胄 孙晓峰 《航空制造技术》 CSCD 北大核心 2024年第17期20-29,共10页
采用激光定向能量沉积技术制备了第二代单晶高温合金DD405薄壁结构,通过试验和理论相结合的手段对单晶高温合金在激光定向能量沉积过程中的热裂纹形成机制进行分析和探究。结果表明,热裂纹的形成是由应力集中、液膜稳定性和碳化物析出相... 采用激光定向能量沉积技术制备了第二代单晶高温合金DD405薄壁结构,通过试验和理论相结合的手段对单晶高温合金在激光定向能量沉积过程中的热裂纹形成机制进行分析和探究。结果表明,热裂纹的形成是由应力集中、液膜稳定性和碳化物析出相3个因素所决定的。由于激光定向能量沉积过程的逐层叠加,残余应力随着沉积高度递增,因此沉积区存在高水平的残余拉应力。沉积区的晶界处会出现显著的应力集中,液膜在两侧拉应力作用下发生撕裂导致裂纹萌生。液膜稳定性与相邻晶粒间的晶界角度密切相关,当大角晶界大于40°时,会在拉应力的驱动下形成热裂纹。MC型碳化物析出相通过“钉扎作用”抑制液相补缩及弱化与基体之间结合强度等作用进一步促进了热裂纹形成。 展开更多
关键词 单晶高温合金 热裂纹 激光定向能量沉积 残余应力 薄壁结构
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火电厂锅炉水冷壁焊缝泄漏失效分析 被引量:1
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作者 校林飞 杨占君 +6 位作者 郑准备 张建伟 周宁 何华 谭永生 陈璟 吴宇星 《电焊机》 2024年第4期84-90,共7页
某12Cr1MoV水冷壁对接焊缝中部出现周向裂纹导致泄漏失效,为调查泄漏失效原因,对焊缝进行了宏观检查、磁粉检测、硬度检验、金相分析、全元素分析和能谱分析,并建立模型分四个阶段讨论了水冷壁焊缝泄漏失效的原因。研究表明:焊缝中夹杂... 某12Cr1MoV水冷壁对接焊缝中部出现周向裂纹导致泄漏失效,为调查泄漏失效原因,对焊缝进行了宏观检查、磁粉检测、硬度检验、金相分析、全元素分析和能谱分析,并建立模型分四个阶段讨论了水冷壁焊缝泄漏失效的原因。研究表明:焊缝中夹杂的S元素是焊缝泄漏失效的主要因素,收缩拉应力为偏析在晶界的低熔点共晶物提供了形成沿晶热裂纹的条件,氧气的介入造成热裂纹的局部氧化,实际运行的综合应力使氧化的沿晶热裂纹多点扩展、融合,形成宏观裂纹,最终导致焊缝泄漏失效。 展开更多
关键词 水冷壁 焊缝 泄漏失效 结晶裂纹 元素偏析 低熔点共晶物
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多级孔花状ZSM-5分子筛的合成及其正辛烷催化裂解反应性能研究
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作者 王健捷 束小龙 +5 位作者 肖霞 王鹏 范晓强 孔莲 解则安 赵震 《无机盐工业》 CAS CSCD 北大核心 2024年第8期139-146,共8页
高性能催化剂的研发是石脑油催化裂解制低碳烯烃领域的研究热点。使用双子季胺盐表面活性剂[C_(18)H_(37)-N^(+)(CH_(3))_(2)-C_6H_(12)-N^(+)(CH_(3))_(2)-C_6H_(13)]Br_(2)作为结构导向剂,成功合成了花状ZSM-5分子筛。利用XRD、SEM、N... 高性能催化剂的研发是石脑油催化裂解制低碳烯烃领域的研究热点。使用双子季胺盐表面活性剂[C_(18)H_(37)-N^(+)(CH_(3))_(2)-C_6H_(12)-N^(+)(CH_(3))_(2)-C_6H_(13)]Br_(2)作为结构导向剂,成功合成了花状ZSM-5分子筛。利用XRD、SEM、N_(2)吸附-脱附和NH_(3)-TPD表征技术研究了晶化温度、n(Si)/n(Al)、n(H_(2)O)/n(Si O_(2))和n(Na_(2)O)/n(Si O_(2))等合成条件对ZSM-5分子筛物化性质的影响,并考察其正辛烷催化裂解反应性能。研究结果表明,花状ZSM-5分子筛的优化制备条件为:n(Na_(2)O)∶n(Al_(2)O_(3))∶n(Si O_(2))∶n(C_(18-6-6)Br_(2))∶n(H_(2)O)=5∶1∶100∶10∶4000、晶化时间为72 h、晶化温度为175℃。随着n(Si)/n(Al)的增大,花状分子筛颗粒逐渐团聚;当投料n(Na_(2)O)/n(Si O_(2))高于0.05时,分子筛样品中开始出现其他杂相;随着投料n(H_(2)O)/n(Si O_(2))的增大,分子筛层状形貌逐渐不明显。在催化裂解正辛烷制乙烯和丙烯反应中,经过30 h连续测试,花状ZSM-5分子筛的正辛烷转化率始终保持稳定,乙烯和丙烯总收率从62.0%逐渐增加至64.4%。花状ZSM-5分子筛较高的催化活性和优异的抗积炭稳定性主要归结于其独特的层状形貌和多级孔结构。 展开更多
关键词 低碳烯烃 多级孔 ZSM-5分子筛 催化裂解 晶化条件
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基于声子晶体的声发射波源检测概率研究 被引量:1
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作者 李红豫 曾祥兴 张璐 《振动与冲击》 EI CSCD 北大核心 2024年第7期75-83,共9页
声发射(acoustic emission,AE)检测就是利用采集和分析声发射现象所产生的信号从而实现对材料进行无损评价的技术,该技术具有实时监测并定位破坏源的能力但是由于检测过程中声发射源信号未知,因此评价检测可靠性的检测概率(probability ... 声发射(acoustic emission,AE)检测就是利用采集和分析声发射现象所产生的信号从而实现对材料进行无损评价的技术,该技术具有实时监测并定位破坏源的能力但是由于检测过程中声发射源信号未知,因此评价检测可靠性的检测概率(probability of detection,POD)研究仍然是空白。进一步来说,在利用声发射监测损伤过程时,声发射波源直接决定其检测结果的可靠性,因此波源的检测概率可以成为量化声发射检测有效性的一个重要指标。为了确定声发射波源的检测概率,利用声子晶体(phononic crystals,PCs)的特性,通过部署声子晶体形成物理带隙,滤除噪声信号,从而获得铝合金试件在紧凑拉伸试验下由于疲劳裂缝活动而引起的声发射信号,最终确定声发射源的检测概率及其影响因素。结果表明,检测概率会随着疲劳裂缝扩展而提高,但裂缝长度达到一定值后开始下降,最终趋于一个平稳值,另外通过设置阈值和选择适当的滤波器,能有效提高检测概率,保证声发射评价结构损伤的有效性。该研究对声发射源识别和检测可靠性评价具有重要意义。 展开更多
关键词 声发射(AE) 检测概率(POD) 声子晶体 疲劳裂缝
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拉伸情形下孔洞缺陷对单晶镁裂纹扩展影响的分子动力学模拟
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作者 柯昌锐 蓝永庭 +2 位作者 解远航 丁浩川 华振虎 《机械强度》 CAS CSCD 北大核心 2024年第5期1192-1199,共8页
采用分子动力学方法对预设裂纹和孔洞的单晶镁模型进行了沿C轴拉伸加载的数值模拟,研究在镁晶体中不同位置的孔洞缺陷对裂纹扩展的影响。模拟结果分析表明,在相同特征尺寸下,孔洞会影响单晶镁模型的屈服强度,不同孔洞位置的模型屈服强... 采用分子动力学方法对预设裂纹和孔洞的单晶镁模型进行了沿C轴拉伸加载的数值模拟,研究在镁晶体中不同位置的孔洞缺陷对裂纹扩展的影响。模拟结果分析表明,在相同特征尺寸下,孔洞会影响单晶镁模型的屈服强度,不同孔洞位置的模型屈服强度不同,其中当孔洞位于裂纹[101ˉ0]方向时,模型的屈服强度最低。孔洞能在一定程度上缓解裂纹在该方向上的应力集中,影响裂纹的孪晶扩展速率。裂纹处靠近孔洞侧的孪晶生长速度相对较慢,其中孔洞位于裂纹[101ˉ0]方向时,孪晶生长速度最慢。孔洞对裂纹的扩展方向影响较小,一般情况下裂纹与孔洞合并后沿拉伸方向扩展,整体呈现比较对称的锥面扩展,但孔洞位于裂纹[0001]方向时,裂纹并未与孔洞出现明显的联合现象。 展开更多
关键词 单晶镁 孔洞 裂纹 孪晶 分子动力学
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大型钛合金构件激光熔化沉积制造过程残余应力诱发开裂机理研究
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作者 谢勇 张文奇 +5 位作者 武致军 严振宇 彭深沉 黄鹏 郭宁 周庆军 《航空制造技术》 CSCD 北大核心 2024年第15期55-64,共10页
残余应力诱发开裂问题仍是限制大型构件激光熔化沉积工业化应用的一大瓶颈。因此,探究激光熔化沉积大型复杂构件残余应力的演化规律,以及残余应力诱发裂纹萌生和扩展的微观组织相关性具有重要意义。通过对大型钛合金构件开裂断口形貌分... 残余应力诱发开裂问题仍是限制大型构件激光熔化沉积工业化应用的一大瓶颈。因此,探究激光熔化沉积大型复杂构件残余应力的演化规律,以及残余应力诱发裂纹萌生和扩展的微观组织相关性具有重要意义。通过对大型钛合金构件开裂断口形貌分析及宏观热-力耦合有限元计算,首次发现激光熔化沉积过程独特的热应力三阶段非对称循环加载模式,即稳定循环-突增加载阶段、非线性循环加载阶段及线性循环加载阶段。以热-力耦合计算得到的残余应力为输入,采用耦合损伤的晶体塑性计算研究了3种热应力加载模式对激光熔化沉积特有的网篮组织的破坏程度,发现线性循环加载模式对网篮组织破坏性最大,稳定循环-突增加载模式破坏性次之,非线性循环加载模式破坏性最小。这种热应力加载模式、断口形貌及微观组织分析进一步表明,残余应力诱发开裂现象是由过大的热应力累积、零件的几何特征、热应力加载模式及成形缺陷等多因素协同控制的,而非单一因素影响,这也为从适时消除应力、优化零件结构及工艺参数、减少和抑制缺陷产生等方面系统化控制开裂问题提供了方向。 展开更多
关键词 激光熔化沉积 TC11钛合金 残余应力 裂纹扩展 晶体塑性
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TP321焊接过程产生层间结晶裂纹和表面液化裂纹的原因和预防措施
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作者 王龙己 吴波 赖朝喜 《当代化工》 CAS 2024年第2期486-490,共5页
加氢装置因为高温、高压、临氢的特殊环境,使加热炉进出口、反应器进出口、高压换热器进出口管线不得不选用TP321或者TP347材质。但在装置建设过程中,工期紧、焊接环境差、焊工水平层次不齐、焊材成分和可焊接操作性差、对热输入和层间... 加氢装置因为高温、高压、临氢的特殊环境,使加热炉进出口、反应器进出口、高压换热器进出口管线不得不选用TP321或者TP347材质。但在装置建设过程中,工期紧、焊接环境差、焊工水平层次不齐、焊材成分和可焊接操作性差、对热输入和层间温度控制较苛刻等原因,使得在焊接过程中出现热裂纹等焊接质量问题。为保证TP321材质管道焊接质量,对产生以上质量问题原因进行简要阐述,保证焊接过程合适的热输入、应用合格焊材、保证焊缝组织铁素体含量,从而保证装置试压、开停工过程的安全与稳定性。 展开更多
关键词 加氢装置 TP321 层间结晶裂纹 表面液化裂纹 铁素体 低温共晶体
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基于渗透结晶法的裂缝有效封堵对比研究
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作者 李善超 董婉莹 +2 位作者 葛一鸣 陈川峰 周鹏 《江西建材》 2024年第3期43-44,共2页
文中对比研究了BKN 88渗透结晶自修复剂和Feedar渗透结晶自修复剂宏观的修复效果,利用渗水系数来表征两种自修复剂的修复性能。结果表明,BKN 88渗透结晶自修复剂的修复效果较好。此外,文中研究了自修复剂掺量、开裂时间和裂缝宽度对自... 文中对比研究了BKN 88渗透结晶自修复剂和Feedar渗透结晶自修复剂宏观的修复效果,利用渗水系数来表征两种自修复剂的修复性能。结果表明,BKN 88渗透结晶自修复剂的修复效果较好。此外,文中研究了自修复剂掺量、开裂时间和裂缝宽度对自修复性能的影响。 展开更多
关键词 渗透结晶法 渗水系数 混凝土裂缝
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工艺参数对高温高压合成Ⅱa型培育钻石的影响
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作者 兰昊天 李仁德 +4 位作者 刘文俊 余海洲 范祖华 刘威 周念 《硬质合金》 CAS 2024年第2期97-105,共9页
针对国内采用六面顶压机利用高温高压法合成Ⅱa型培育钻石存在成核晶种粒数少、优晶占比小、生长缺陷多等问题,对合成前期和合成结束后的工艺参数曲线进行了优化。通过调控合成腔体内部的压力和温度,使其在合成腔体中的生长环境稳定,从... 针对国内采用六面顶压机利用高温高压法合成Ⅱa型培育钻石存在成核晶种粒数少、优晶占比小、生长缺陷多等问题,对合成前期和合成结束后的工艺参数曲线进行了优化。通过调控合成腔体内部的压力和温度,使其在合成腔体中的生长环境稳定,从而提高晶种形核生长数和优晶率。结果表明,最优工艺方案为:培育钻石生长阶段的前20h,在低温高压环境下缓慢升温并采取一段时间的保温措施,然后恒功率升温至设定温度,在高温高压下生长3d;在合成结束的2h内,采取分阶段带加热功率低速卸压,能够有效控制裂纹、金属包裹体等缺陷的产生,提高合成晶体品质。最终晶种形核生长数为25颗,优晶占比为92%。 展开更多
关键词 高温高压 Ⅱa型培育钻石 合成阶段 晶种形核生长数 优晶率 裂纹 金属包裹体
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对称热流载荷下一维六方准晶体币状裂纹的热-弹性解析解
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作者 李泓钊 李佩栋 《宁夏大学学报(自然科学版)》 CAS 2024年第2期112-123,共12页
针对一维六方准晶无限体中币状裂纹问题,给出了裂纹面作用对称热流载荷时的解析解.在准晶热-弹性通解的基础上,采用广义势理论方法,得到了准晶体中稳态的三维精确热-弹性场.同时,给出了裂纹所在平面上多个重要物理量的封闭解,其中包括... 针对一维六方准晶无限体中币状裂纹问题,给出了裂纹面作用对称热流载荷时的解析解.在准晶热-弹性通解的基础上,采用广义势理论方法,得到了准晶体中稳态的三维精确热-弹性场.同时,给出了裂纹所在平面上多个重要物理量的封闭解,其中包括裂纹面位移、法向应力、应力强度因子等.通过数值算例,验证了当前解析解的正确性,并分析了三维热-弹性场的分布情况.通过对声子场和相位子场耦合与解耦前后的对比,可知相位子场对结果的影响非常显著.所得解析解可作为针对准晶体断裂问题数值方法(如扩展有限元法)和实验方法(红外热成像无损检测方法)的校核基准. 展开更多
关键词 一维六方准晶 币状裂纹 热流载荷 解析解 势理论方法
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