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Crystal Structure of N-(O-Ethylphenylthionophos-phonyl) N'-(O-p-iodinephenylphenylthionophos-phonyl)thiosemicarbazide
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作者 ZHANG Xin(Department of Chemistry, Tianjin Colege of Education, Tianjin 300050)LIU Xiao-Lan MIAO Zhi-Wei +3 位作者 ZHOU Guang-Yan MIAO Fang-Ming(Institute of Chemical Crystallography, Tianjin Normal University,Tianjin 300074)CAI Jian-Ping JIN Gui-Yu CHEN Ru 《Chinese Journal of Structural Chemistry》 SCIE CAS CSCD 1997年第1期16-19,共4页
The title compound C21,H22,N3O2P2S3I, Mr=633. 44 crystallizes in themonoclinic, space group P21/a, with a= 8. 784 (3), b= 19. 900 (5), c = 16. 022 (4)A, β=98. 40(2)° V=2770. 6 A', Z=4, Dc= 1. 52 g/cm3, F(000... The title compound C21,H22,N3O2P2S3I, Mr=633. 44 crystallizes in themonoclinic, space group P21/a, with a= 8. 784 (3), b= 19. 900 (5), c = 16. 022 (4)A, β=98. 40(2)° V=2770. 6 A', Z=4, Dc= 1. 52 g/cm3, F(000)=1264, μ=125. 45 cm-l, R=0. 078, Rw=0. 067. In the molecule, each P atom is coordinated byO, N, S and C atoms with a distorted tetrahedral coordination configuration. 展开更多
关键词 crystal structure thionophosphonylthiosemicarbazide tetrahedral configuration
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