Anisotropic cyclic deformation behavior of an extruded Mg-3Y alloy sheet with rare earth texture

Mg-RE(magnesium-rare earth)alloys exhibit pronounced in-plane anisotropy of mechanical response under quasi-static monotonic loading resulting from the RE texture,as extensively reported.In this work,an obvious in-plane anisotropy of cyclic deformation behavior was observed in an extruded Mg-3Y alloy sheet during strain-controlled tension-compression low-cycle fatigue(LCF)at room temperature.The extrusion direction(ED)samples displayed better fatigue resistance with almost symmetrical hysteresis loops and longer fatigue life compared with the transverse direction(TD)samples.The influences of texture on the deformation modes,cracking modes,and mechanical behavior of Mg-Y alloy sheets under cyclic loading were studied quantitatively and statistically.The activation of various slip/twinning-detwinning systems was measured at desired fatigue stages via EBSD observations together with in-grain misorientation axes(IGMA)analysis.The results indicate that the activation of deformation modes in the TD sample was featured by the cyclic transition,i.e.,prismatic slip(at the tensile interval)→{10–12}tension twinning(at the compressive reversal)→detwinning+prismatic slip(at the re-tensile reversal).In the case of the ED sample,the cyclic deformation was dominated by the basal slip throughout the fatigue life.For cracking modes,intergranular cracking and persistent slip bands(PSB)cracking were the primary cracking modes in the ED sample while the TD sample showed a high tendency of{10–12}tension twinning cracking(TTW cracking).The underlying mechanisms influencing the activation of various slip/twinning-detwinning systems,as well as cracking modes and cyclic mechanical behavior,were discussed.

CYCLIC DEFORMATION OF FACE CENTERED CUBIC CRYSTALS AND ITS DISLOCATION INTERACTION MODEL——Ⅰ.CYCLIC DEFORMATION OF COPPER CRYSTALS

Cyclic stress-strain responses and dislocation structure of copper single crystals with various tensile axes were systematically studied and compared with each other.Experimental results reveal that the evolution of microscopic dislocation configurations in a crystal and, accordingly,its macroscopic cyclic behaviours are closely related with its orientation.Re- markable secondary slip has been observed in some crystals with orientations well inside the crystallographic triangle, which are usually considered as single-slip ones.Their cyclio behaviours and dislocation structures at saturation are similar to those of their neighbouring multi-slip crystals.These results have constructed the experimental basis for the newly pro- posed dislocation interaction model Jor cyclic deformation of fee crystals,which will be des- cribed in the second part of this article.

EFFECT OF SLIP ORIENTATION ON STRESS RESPONSE,INTERNAL FRICTION AND ULTRASONIC ATTENUATION DURING CYCLIC DEFORMATION IN Al SINGLE CRYSTALS

The variation of cyclic stress,internal friction and ultrasonic attenuation during cyclic deformation and relations among them have been investigated with different slip orientation Al single crystals.The results indicate that the value of cyclic stress σ,internal friction Q^(-1)and ultrasonic attenuation △α depend obviously on the slip orientation.There are large differences in above three parameters for different slip orientation Al crystals.In early stage of fatigue life,σ and △α increase and Q^(-1)decreases with cycles N,and △α reached maxi- mum before σ,while Q^(-1)and σ get the valley and the peak,respectively,at same cycles.

CYCLIC DEFORMATION OF FACE CENTERED CUBIC CRYSTALS AND ITS DISLOCATION INTERACTION MODEL——Ⅱ.DISLOCATION INTERACTION MODEL OF CYCLIC DEFORMATION

A dislocation interaction model has been proposed for cyclic deformation of fcc crystals.Ac- cording to this model,cyclic stress-strain responses and saturation dislocation structures of a crystal are associated with the modes and intensities of dislocation interactions between slip systems active in the crystal; and,hence,may be predicted by the location of its tensile axis in the crystallographic triangle.This model has successfully explained the different behaviours of double-slip crystals and multi-slip behaviours of some crystals with orientations usually con- sidered as single-slip ones.

BAUSCHINGER EFFECT AND DISLOCATION STRUCTURE IN STAINLESS STEEL DURING CYCLIC DEFORMATION

Cyclic deformation in symmetrical push-pull mode was carried out at room temperature in air using a Schenck hydropuls machine.The total strain amplitude which was kept constant dur- ing the test ranged from ±0.004 to±0.012.The 0.2% offset yield stress σ_(0.2f) in tension and σ_(0.2r) in compression and peak stress σ were measured from the stress-strain hysteresis loop at various cycles.The Bauschinger strenghth differential factor(BSDF)was then calcu- lated from σ_(0.2f) and σ_(0.2r).The energy loss △E of each cycle was determined from hysteresis loop areas.These parameters,BSDF,σ and △E,appear to have two distinctively different stages. The dislocation structures were observed using TEM in specimens deformed cyclically,for various cycles.The observation shows that the dislocations pile-up mainly against grain boundaries and there exist large amount of deformation twins.The addition of 0.25 wt-% ni- trogen reduced the stacking fault energy of the alloy significantly.Cross-slip and climb are therefore rather difficult to occur during the cyclic deformation at room temperature,and well-defined dislocation cells and walls can only be seen at the final stage of fatigue.

The Study of Dual-phase Steel after Cyclic Deformation at Various Strain Amplitudes

Low cycle fatigue tests under plastic strain control were carried out with a dual-phase steel containing 23 Vol.-％ martensite. Specimens hardened rapidly at first few cycles followed by a slight softening to saturation stages when cycled at higher strain amplitudes, whereas at lower strain amplitudes the specimens presented continually hardening for a long time until saturation. TEM examination of the saturation dislocation structures show that clusters, parallel walls and cells were found at low, medium and high strain amplitude, respectively. It also has been found that the martensite/ferrite interfaces did not affect the dislocation structures signi- ficantly when a specimen was fatigued at lower strain amplitude. However, the dislocation struc- ture adjacent to the two-phase boundary is dif- ferent to some extent from that in the remote regions in the ferrite when a higher strain amplitude is applied.

Natural overlaying behaviors push the limit of planar cyclic deformation performance in few-layer MoS_(2) nanosheets

As a typical two-dimensional(2D)transition metal dichalcogenides(TMDCs)material with nonzero band gap,MoS_(2)has a wide range of potential applications as building blocks in the field of nanoelectronics.The stability and reliability of the corresponding nanoelectronic devices depend critically on the mechanical performance and cyclic reliability of 2D MoS_(2).Although an in situ technique has been used to analyze the mechanical properties of 2D materials,the cyclic mechanical behavior,that is,fatigue,remains a major challenge in the practical application of the devices.This study was aimed at analyzing the planar cyclic performance and deformation behavior of three-layer MoS_(2)nanosheets(NSs)using an in situ transmission electron microscopy(TEM)variable-amplitude uniaxial low-frequency and cyclic loading-unloading tensile acceleration test.We also elucidated the strengthening effect of the natural overlaying affix fragments(other external NSs)or wrinkle folds(internal folds from the NS itself)on cycling performances and service life of MoS_(2)NSs by delaying the whole process of fatigue crack initiation,propagation,and fracture.The results have been confirmed by molecular dynamics(MDs)simulations.The overlaying enhancement effect effectively ensures the long-term reliability and stability of nanoelectronic devices made of few-layer 2D materials.

Abnormal chemical composition fluctuations in multi-principal-element alloys induced by simple cyclic deformation

High entropy alloys exhibit excellent combination of mechanical properties because of the unique com-position fluctuations,termed as‘concentration wave’.The concentration wave was closely related to mul-tiple aspects,including the fluctuation of local strain energy,local atomic environment,electronegativity,etc.Here we report for the first time that the amplitude of the concentration wave can be mechani-cally tailored under cyclic deformation in a well-known Cantor alloy.Atomic-scale energy-dispersive X-ray spectroscopy(EDS)mapping reveals that cyclic deformation may dynamically induce the clustering of solute atoms with a size of 1-3 nm,thus resulting in a higher concentration wave amplitude.The con-centration wave promotes strong interactions between dislocations and local solute clusters.Aside from the typical Taylor strengthening contribution due to the presence of isolated dislocations,the strength enhancement from the mechanically induced composition fluctuations was quantified to be as high as∼70 MPa,about one-third of the yield strength of the alloy without pre-deformation.This opens up a novel strategy of designing high strength alloys by tailoring solute configurations.

CYCLC DEFORMATION OF Nb SINGLE CRYSTALS

The Nb single crystals of both[321]and[110]orientations have been cyclicly deformed in tension-compression at constant strain rate 8×10^(-4)s^(-1)over a range of plastic strain amplitudes between 10^(-3)and 10^(-4).The cyclic hardening,the changes in shape of crystals and the asymmetry of stress have been studied.The hardening curve can be divided into three stages,i.e.first,rapid-hardening and saturated stage. In the first stage of cyclic hardening curve dominant features of dislocation configura- tions are high density networks and debris loops.In the rapid-hardening stage the main fea- ture is the formation of dislocation bundles.In the saturated a well defined bundle structure fully develops and between them it is filled with only screw dislocations and the imposed strain is accommodated mainly by the motion of screw dislocations travelling to and from between the bundles.Three-dimension cell,two-dimension cell or bundle structures are summarized as the saturated structures of bcc metals.

Fatigue characteristics of sand-cast AZ91D magnesium alloy

The fatigue characteristics of the AZ91D-T6 alloy samples taken from engine blocks have been investigated at 20℃ and elevated temperature(150℃).The fatigue strength and cyclic stress amplitude of the alloy significantly decrease with the increase of the test temperature,although cyclic hardening occurs continuously until failure for both temperatures.With the increase of the temperature,the decreased fatigue life of the alloy tested at the same stress amplitude is mainly attributed to the decreased matrix strength and the increased hysteresis energies.Fatigue failure of the engine blocks made of AZ91D-T6 alloy is mainly controlled by casting defects.For the defect-free specimens,the crack initiation behavior is determined by the single-slip(20℃)and by environment-assisted cyclic slip(150℃)during fatigue,respectively.The low-cycle fatigue lives of the alloy can be predicted using the Coffin-Manson relation and Basquin laws,the three-parameter equation and the energy-based concepts,while the high-cycle fatigue lives of the alloy fitted well with the developed long crack life model and MSF life models.

Fatigue Behaviour of Metal Matrix Composites

Based mainly on the work done at the authors' laboratory in recent years,this paper examines what is currently known about the cyclic deformation and fatigue properties of metal matrix composites, with particular emphasis on discontinuous fiber (whisker or particulate)-reinforced Al composites. The following items are discussed:fatigue strength and life,cyclic deformation and microstructural evolution,microcrack initiation and growth,fatigue crack propagation behaviour.

Addressing the permanent deformation behavior of hot mix asphalt by triaxial cyclic compression testing with cyclic confining pressure

Rutting or permanent deformation is one of the major distress modes of hot mix asphalt in the field. Triaxial cycle compression testing （TCCT） is a standardized and scientifically accepted test method to address this distress mode in the lab and to characterize the resistance to permanent deformation. In most labs and according to EN 12697-25, standard TGCTs are carried out with cyclic axial loading and a constant confining pressure. In road pavements on the other hand, dynamic traffic loading due to passing wheels leads to cyclic confining pressure. In order to bring the TCCT closer to reality, the radial reaction and its phase lag to axial loading in standard TCCTs are analyzed and an enhanced TCCT with cyclic confining pressure is introduced. The cyclic confining pressure takes into account the viscoelastic material response by the radial phase lag to axial phase loading. In a subsequent test program, TCCTs with different confining pressure amplitudes were carried out on two hot mix asphalts. Results from standard and enhanced TCCTs were analyzed, compared and discussed. It is shown that the resistance to permanent deformation in- creases significantly when the viscoelastic material response is taken into account in the TCCT by introducing cyclic confining pressure.

Bauschinger Effect of Mn18Cr18N Austenitic Stainless Steel

The experimental study of Bauschinger effect in Mn18Cr18N austenitic stainless steel was presented by compression-tensile cyclic loading tests with the prestrains ranging from 0.005 to 0.1,which was illustrated utilizing stress-strain curves and analysed by TEM images from aspects of microstructural mechanisms.Moreover,the Bauschinger effect and its associated roundness phenomenon in reverse flow curve with respect to different cycles and cyclic strain amplitudes were evaluated in a quantitative manner.The experimental results indicate that Bauschinger effect is apparent during the test.At smaller cyclic strain amplitude,intergranular backstress is the main source of Bauschinger effect.With further increasing of cycles,dislocation density increases and dislocation movement is hindered in the reverse deformation.Therefore,Bauschinger effect is weakened to some extent.At large cyclic strain amplitude,backstress originating from the dislocation pile-up at grain boundaries and the continuous formation of deformation twins dominate the Bauschinger effect.In addition,the backstress results in the roundness of reverse curve during cyclic loading.The larger value ofΔεp*,the more obvious the roundness of the reverse curve,and the more significant the Bauschinger effect.

Microstructure and low cycle fatigue of a Ti2AlNb-based lightweight alloy

Ti2AlNb-based intermetallic compounds are considered as a new category of promising lightweight aerospace materials due to their balanced mechanical properties.The aim of this study was to evaluate monotonic and cyclic deformation behavior of an as-cast Ti-22A1-20Nb-2V-1Mo-0.25Si(at.%)intermetallic compound in relation to its microstructure.The alloy containing an abundant fine lamellar O-Ti2AlNb phase exhibited a good combination of strength and plasticity,and superb fatigue resistance in comparison with other intermetallic compounds.Cyclic stabilization largely remained except slight cyclic hardening occurring at higher strain amplitudes.While fatigue life could be described using the common Coffin-Mason-Basquin equation,it could be better predicted via a weighted energy-based approach.Fatigue crack growth was characterized mainly by crystallographic cracking,along with fatigue striationlike features being unique to appear in the intermetallics.The results obtained in this study lay the foundation for the safe and durable applications of Ti2AlNb-based lightweight intermetallic compounds.

Effect of heat treatment on strain–controlled fatigue behavior of cast Mg–Nd–Zn–Zr alloy

The influence of heat treatment on the strain-controlled fatigue behavior of cast NZ30 K alloy was investigated. Compared with the as-cast and solutionized（T4） alloys, the peak-aged（T6） and over-aged（T7）counterparts have a higher cyclic stress and a lower plastic strain value due to the precipitation strengthening. The as-cast and T4-treated alloys have a higher fatigue strength/yield strength ratio than the aged alloys, which is mainly attributed to their higher cyclic hardening. Under stress-controlled loading,the aged alloys show lower hysteresis energies than the as-cast and T4-treated counterparts, leading to longer fatigue lifetimes. For the T4-treated alloy, the cyclic hardening and fatigue failure are controlled by the dislocations-slip and twinning, while for both the as-cast and T6-treated counterparts, they are controlled by the dislocation-slip. For the T7-treated alloy, cyclic deformation and failure behavior are mainly dependent on dislocations-slip and grain boundary sliding.

Origin of superior low-cycle fatigue resistance of an interstitial metastable high-entropy alloy

In this study, the deformation behaviors and related microstructural evolutions were investigated in either monotonic or cyclic deformation modes in an interstitial metastable high-entropy alloy. These investigations aimed to reveal the mechanisms underlying the superior low-cycle fatigue(LCF) life of this alloy.A thermomechanical process was applied to induce fine-grained(FG) and coarse-grained(CG) microstructures in Fe–30Mn–10Co–10Cr–0.4C(atomic percentage) alloy. Their superior combination of strength and ductility was attributed to the appearance of deformation-induced ε-martensite and the presence of carbon. The CG alloy showed a greater volume fraction of ε-martensite than the FG alloy in the monotonic deformation mode, and vice versa in the cyclic mode. Such a disparity was interpreted in light of the back-stress effect of the relaxed γ-grain boundaries in the latter mode. Meanwhile, the γ-to-ε phase transformation under cyclic loading at low strain amplitudes(0.4%) barely led to an improved fatigue life as compared with that at higher strain amplitudes(≥ 0.55%). The high reversibility of partial dislocation motions under cyclic loading and delaying the formation of dislocation cells through the martensitic transformation could explain why the alloys investigated in this study exhibited a superior LCF life compared with high-entropy alloys reported in previous studies.

Formability Investigations of High-Strength Dual-Phase Steels

Car manufacturing is always regarded as the key industry behind sheet metal forming, and thus, the requirements of and developments in car manufacturing play a decisive role in the development of sheet metal forming. The automotive industry is faced with contradictory demands and requirements： better performance with lower consumption and less harmful emissions, more safety and comfort; these are extremely difficult to supply simultaneously with conventional materials and conventional manufacturing processes. The fulfillment of these often contradictory requirements is one of the main driving forces in the automotive industry and thus in the material and process developments in sheet metal forming, as well. In recent years, significant developments can be observed in the application of high-strength steels. In this respect, the application of various dual-phase steels is one of the best examples. However, the application of these highstrength steels often leads to formability and manufacturing problems. One formability problem is the springback occurring after sheet metal forming. In the current research, we have dealt mainly with advanced high-strength steels, primarily with dual-phase steels. When applying them, the springback phenomenon is one of the most critical issues. To reduce the tremendous amount of experimental work needed, we also applied numerical simulation using isotropic–kinematic hardening rules. The isotropic–kinematic hardening behavior of a given material in the applied Auto Form numerical package may be characterized with three independent material parameters c, v and K（a detailed explanation of their meaning will be given in the main part of this paper）. However, we found that the material data included in simulation packages for these new high-strength steels are not fully adequate. For the determination of more reliable material parameters and to achieve better simulation results, a new testing device was developed. Numerical simulations were performed using the material parameters determined by the new device to show the sensitivity of springback behavior to these material parameters.