Research on Pressure Tight Sampling Technique of Deep-Sea Shallow Sediment—A New Approach to Gas Hydrate Investigation

Analyzed and calculated are pressure changes and body deformation of the sample inside of the corer in the process of sampling of deep-sea shallow sediment with a non-piston corer for gas hydrate investigation, Two conclusions are drawn： （1） the stress increments associated with the corer through the sampling process do not affect the stabilization of the gas hydrate; （2） the body deformation of the sample is serious and the ＂incremental filling ratio＂ （IFR） is less than unit, For taking samples with in-situ pressure and structure, combining with the design theories of the pressure tight corer, we have designed a kind of piston corer, named the gas hydrate pressure tight piston corer, Several tests on the sea have been conducted. Test results indicate that the piston corer has a good ability of taking sediment samples on the seafloor and maintaining their original in-situ pressure, meeting the requirement of exploration of gas hydrate in deep-sea shallow sediment layers.

The pressure compensation technology of deep-sea sampling based on the real gas state equation

Compressed gas is usually used for the pressure compensation of the deep-sea pressure-maintaining sampler.The pressure and volume of the recovered fluid sample are highly related to the precharged gas. To better understand the behavior of the gas under high pressure, we present a new real gas state equation based on the compression factor Z which was derived from experimental data. Then theoretical calculation method of the pressure and volume of the sample was introduced based on this empirical gas state equation. Finally, the proposed calculation method was well verified by the high-pressure vessel experiment of the sampler under 115 MPa.

Accumulator-Based Deep-Sea Microbe Gastight Sampling Technique

The accumulator is used as a pressure compensation device to realize deep-sea microbe gastight sampling. Four key states of the accumulator are proposed to describe the pressure compensation process and a corresponding mathematical model is established to investigate the relationship between the results of pressure compensation and the parameters of the accumulator. Simulation results show that during the falling process of the sampler, the accumulator＇ s real opening pressure is greater than its precharge pressure; when the sampling depth is 6000 m and the accumulator＇ s precharge pressure is less than 30 MPa, to increase the accumulator＇ s precharge pressure can improve pressure compensation results obviously. Laboratory experiments at 60 MPa show that the acctunulator is an effective and reliable pressure compensation device for deep-sea microbe samplers, The success in sea trial at a depth of 2000 m in the South China Sea shows that the mathematical model and laboratory experiment results are reliable.

Engineering behaviour of in situ cored deep cement mixed marine deposits subjected to undrained and drained shearing

The deep cement mixing(DCM)is used to improve the capacity and reduce the settlement of the soft ground by forming cemented clay columns.The investigation on the mechanical behaviour of the DCM samples is limited to either laboratory-prepared samples or in-situ samples under unconfined compression.In this study,a series of drained and undrained triaxial shearing tests was performed on the in-situ cored DCM samples with high cement content to assess their mechanical behaviours.It is found that the drainage condition affects significantly the stiffness,peak and residual strengths of the DCM samples,which is mainly due to the state of excess pore water pressure at different strain levels,i.e.being positive before the peak deviatoric stress and negative after the peak deviatoric stress,in the undrained tests.The slope of the failure envelope changes obviously with the confining pressures,being steeper at lower stress levels and flatter at higher stress levels.The strength parameters,effective cohesion and friction angle obtained from lower stress levels(c′0 andφ′0)are 400 kPa and 58°,respectively,which are deemed to be true for design in most DCM applications where the in-situ stress levels are normally at lower values of 50-200 kPa.Additionally,the computed tomography(CT)scanning system was adopted to visualize the internal structures of DCM samples.It is found that the clay pockets existing inside the DCM samples due to uneven mixing affect markedly their stress-strain behaviour,which is one of the main reasons for the high variability of the DCM samples.

Strategies on Sample Size Determination and Qualitative and Quantitative Traits Integration to Construct Core Collection of Rice (Oryza sativa)

The development of a core collection could enhance the utilization of germplasm collections in crop improvement programs and simplify their management. Selection of an appropriate sampling strategy is an important prerequisite to construct a core collection with appropriate size in order to adequately represent the genetic spectrum and maximally capture the genetic diversity in available crop collections. The present study was initiated to construct nested core collections to determine the appropriate sample size to represent the genetic diversity of rice landrace collection based on 15 quantitative traits and 34 qualitative traits of 2 262 rice accessions. The results showed that 50-225 nested core collections, whose sampling rate was 2.2%-9.9%, were sufficient to maintain the maximum genetic diversity of the initial collections. Of these, 150 accessions （6.6%） could capture the maximal genetic diversity of the initial collection. Three data types, i.e. qualitative traits （QT1）, quantitative traits （QT2） and integrated qualitative and quantitative traits （QTT）, were compared for their efficiency in constructing core collections based on the weighted pair-group average method combined with stepwise clustering and preferred sampling on adjusted Euclidean distances. Every combining scheme constructed eight rice core collections （225, 200, 175, 150, 125, 100, 75 and 50）. The results showed that the QTT data was the best in constructing a core collection as indicated by the genetic diversity of core collections. A core collection constructed only on the information of QT1 could not represent the initial collection effectively. QTT should be used together to construct a productive core collection.

Simulation of sludge－dredging effects in controlling nutrient release of LakeKasumigaura with large－size core samples

Nutrient release from the dredged and undredged sediments in Lake Kasumigaura were simulated under the laboratory control conditions with large-size core samples. It was found that phosphate and ammonia release fluxes are less in aerobic than those in anaerobic. In different simulated dredged depth, the phosphate release showed large divergence in the anaerobic than in the aerobic. There was a larger accumulated release of phosphate and ammonia at actual dredged (St. B) than the undredged (St. A) in anaerobic condition. This showed that the sludge-dredging was effective of controlling phosphorus and nitrogen release. A preliminary assessment is drawn from the experiments that the sludge-dredging work in Tsuchiura Bay of Lake Kasumigaura can reduce about 15. 9% of phospbate and 56. 2% of anunonia release from the sediments respectively.

Turbidite Events Recorded in Deep-sea Core IR-GC1 off Western Sumatra： Evidence from Grain-size Distribution

Sediment core IR-GC1, from the abyssal basin of the Indian Ocean off Sumatra, may provide important information on depositional events related to earthquakes and tsunamis. In this study, based on a combination of grain-size analysis with lithological studies and oxygen isotope stratigraphy, seven deep-sea turbidite layers were identified, corresponding to seven turbidity events that occurred at 128- 130, 105-107, 98-100, 86-87, 50-53, 37-41 and 20-29 ka. The sediments of the turbidite deposits are characterized by coarse grain sizes, poor sorting, wide kurtosis, bimodal frequency distributions and clear depositional variations. Particle size grading is also an important signature of deep-sea turbidite deposits and can be used as an indicator to identify turbidite layers. Possible triggering mechanisms for the turbidite events include tsunamis, earthquakes, volcanic eruptions and sea-level changes.

Sample Size Determination and Statistical Hypothesis Testing for Core Centration in Press Coated Tablets

A novel statistical approach to evaluate the manufacturing quality of press coated tablets in terms of the centering of their core is presented. We also provide a formula to determine the necessary sample size. This approach is applied to real data.

Frequency and Characteristics of Dust Sediments in Core Samples from Hashylan Wetland, Kermanshah, Iran

Dust phenomenon is one of the biggest environmental problems in arid and semiarid regions. In these areas, lakes and wetlands are natural dust traps and core sampling method can be an appropriate way to assess the phenomenon of the dust. Therefore, the purpose of this study is the study of frequency and characteristics of dust sediments in core samples from Hashilan wetlands, Kermanshah. Four intact core samples were taken from different parts of the Hashilan wetland in Kermanshah. Physical, chemical and micromorphological analysis were done. Also clay mineralogy was performed using X-ray analysis (XRD) and shape of particles was photographed by scanning electron microscope (SEM). Considering that four samples had been taken from different parts of the wetland, the quantitative differences in dust amount are likely due to the location of the samples. The results of XRD and thin sections show that the dominant mineralogical composition of dust particles was clay minerals, quartz and calcite. SEM results for core sample 1 revealed that most particles had the size between 2 to 50 mm which ranged from fine silt to coarse silt. Considering the similarities between SEM images for core sample 1 and those from Kermanshah dust measurement station, it could be said that fine rounded particles detected at top 30 cm of core samples had Aeolian origin. These findings were in accordance with the results from dust measurement and weather station of Kermanshah about increased dust activities in the study area over past 10 years.

基于空间插值的不规则海洋地质样品测试分析数据聚类算法研究

海洋地质调查中获取大量海洋沉积物柱状样样品测试分析数据,样品测试分析目的不同导致柱状样数据采样深度不同,由此造成地质取样数据在三维空间上呈现不规则散点状分布。传统聚类算法无法在三维空间上对此类不规则散点数据进行聚类分析。对此,文章设计了一种基于空间插值的不规则地质样品测试分析数据聚类算法,有效地将三维样品测试分析散点数据降为二维数据后进行聚类分析,本算法较好地解决了地质体中试验测试数据的不均衡性问题,为海洋地质大数据分析提供了基础技术方法。

基于机器学习的水泥基灌浆料强度预测方法

针对采用小直径芯样法准确预测水泥基灌浆料抗压强度的问题,使用压力试验机分别对水泥基灌浆料标准尺寸试块和小直径芯样进行抗压强度试验,并基于试验数据,采用支持向量机回归(SVR)和随机森林回归(RFR)对水泥基灌浆料抗压强度进行回归预测。结果表明:标准尺寸试块均呈正反相接的四角锥体破坏形态,而高径比为0.7和1.0的小直径芯样呈正反相接的圆锥体破坏形态,高径比为1.2的小直径芯样呈斜裂缝剪切破坏形态;标准尺寸试块和小直径芯样的抗压强度值均服从正态分布,且无离群值;随着龄期的增长,标准尺寸试块和小直径芯样的抗压强度提高,且具有早期强度较高的特性;直径46 mm芯样的抗压强度较小,且更易受加工精度的影响;在给定的龄期和直径下,高径比为0.7的芯样抗压强度值最大,抗压强度离散程度最小;RFR预测模型对水泥基灌浆料抗压强度的预测效果更优。所提方法可较准确预测水泥基灌浆料抗压强度,为水泥基灌浆料抗压强度的预测研究提供了参考。

高温小井眼大直径岩心旋转井壁取心仪研制及应用

随着油气勘探开发难度增大,特别是海洋油气勘探开发的不断加大,以及深水井、高温井越来越多,地质方面对电缆测井技术所获取的参数要求也越来越高。为了更好地获取小井眼尺寸井壁岩心样本,助力油气田高效探勘开发,通过对取心仪井下仪器关键零部件电子控制短节和机械液压短节的创新设计与模拟分析,研制了适用于高温、高压、小尺寸井眼的大直径旋转井壁取心仪(MRCT-dumpy)。通过功能测试和5口井作业应用表明,大直径旋转井壁取心仪钻头性能及取心电机性能均得到充分验证,其热管理系统满足作业需要,符合设计要求;该取心仪取心功能正常,最高单趟收获岩心43颗,满足小井眼大直径取心作业要求。该仪器的设计与应用可为后期同类技术的发展提供指导。

基于表型性状分析构建冀北地区马铃薯核心种质

为合理利用和更好保存马铃薯种质资源,本研究以冀北地区保存的502份马铃薯种质资源为材料,调查了26个表型性状,以不同块茎肉色进行分组,设置简单比例、对数比例、平方根比例和多样性比例4种取样方法,5%、10%、15%、20%、25%和30%共6种取样比例,利用2种遗传距离(欧氏距离和马氏距离)和4种聚类方法(类平均法、最长距离法、最短距离法、离差平方和法),探讨最佳取样策略,抽选核心种质。利用遗传多样性特征值、t检验、评价参数和系统聚类等方法对核心种质的表型性状进行评价,以及利用主成分分析对核心种质进行确认。结果表明,平方根比例法能够使核心种质更具代表性,20%为最佳取样比例,欧氏距离优于马氏距离,最优聚类方法为最短距离法,最终抽提出100份马铃薯核心种质,占全部种质的19.92%;核心种质的评价和主成份分析结果表明100份核心种质消除了大部分遗传冗余,保留了所有样本的遗传多样性,具有良好的代表性。本研究为马铃薯种质资源的有效利用和种质创新提供了重要的理论依据和实践基础。

基于表型性状的酸枣核心种质构建

为更好地保存和研究酸枣种质,提高利用效率,以211份酸枣种质为试材,基于表型性状数据,在25%取样比例下,对所有种质进行逐步系统聚类,从遗传距离方法、取样方法、聚类方法和取样比例4个方面探讨酸枣核心种质的最佳取样策略。根据最佳取样策略和3种分组取样方法进行分组取样,并与不分组取样进行比较。结果表明:基于25%取样比例,采用优先取样法、欧氏距离法和可变类平均法构建核心种质效果最佳;在最佳构建策略下筛选总体取样比例,结果表明最佳总体取样比例为25%;不分组取样构建的核心种质Pcore的方差差异百分率(VD)、变异系数变化率(VR)和极差符合率(CR)高于分组取样构建的核心种质Core-L,构建效果更好;定性描述性状保留比例、t检验、符合率检验、主成分分析和样品三维分布图表明构建的核心种质能够消除遗传冗余,能够代表原始种质。基于表型性状筛选出的最佳构建策略为“欧氏距离+可变类平均法+优先取样法+25%取样比例”,经过补充完善,最终得到58份核心种质,具有较高的代表性。本研究成功构建了能够代表原始酸枣种质表型遗传多样性的核心种质,有助于科学、有效地收集和保存酸枣种质资源,为深入挖掘和利用酸枣种质资源提供了科学依据,同时也为选育酸枣良种奠定基础。

基于表型性状构建禾初级核心种质

“禾”是适应贵州黔东南山区峡谷森林中遮荫、泥沼、寒冷、积水等特殊自然生境生长的地方水稻品种。以402份禾种质资源为材料,依据禾颖尖颜色差异将原始种质划分为5组,基于26个表型性状,采用逐步聚类法以6种总体取样规模、4种组内取样比例和2种组内取样方法筛选最佳取样策略,构建禾初级核心种质,并对其进行综合评价。结果表明,10%为最适总体取样规模,组内取样比例法以对数比例法最优,聚类取样法是组内最佳取样方法。在最佳取样策略下,共获得47份禾初级核心种质,占比11.69%,表型保留比例为95.77%。核心种质评价结果表明,构建的核心种质作为原始种质的浓缩能够代表禾原始种质的遗传多样性。

基于ICEEMDAN多尺度熵与NGO-HKELM的转子故障诊断

针对电机转子故障信号非平稳、敏感的故障特征不能有效提取,传统分类器参数智能优化算法存在优化速度慢、调整参数多、易陷入局部最优等问题提出基于ICEEMDAN-MSE-KPCA与NGO-HKELM优化的转子故障诊断方法。首先,采用改进的自适应噪声完全集合经验模态分解(improved complete empirical mode decomposition with adaptive noise,ICEEMDAN)方法对转子振动信号进行分解和重构;计算重构信号的多尺度样本熵(multiscale sample entropy,MSE),形成特征向量,通过核主成分分析(kernel principal component analysis,KPCA)方法对高维的特征向量进行降维;最后,将降维后的特征向量输入北方苍鹰算法(northern goshawk optimization,NGO)优化的混合核极限学习机(hybrid extreme learning machine,HKELM)进行转子故障分类。研究结果表明,基于ICEEMDAN-MSE-KPCA与NGO-HKELM优化的转子故障诊断模型,平均识别准确率可达97.7273%,平均寻优时间为1.0681 s,收敛速度快、准确率高以及分类效果好。

焦虑情绪何时会激发创业努力?一个跨层次双重调节模型

创业者必须投入极大强度的努力,才能带领初创企业度过三年艰难的酝酿期。部分研究指出,情绪是激发创业者持续投入努力的近端驱动力。焦虑作为创业活动中显著存在的日常情绪,关于其在何种情况下能够激发创业努力的研究却略显不足。本文基于社会认知理论,引入核心自我评价和创业身份中心性作为调节变量,探究日常焦虑情绪对创业努力的促进作用。借助体验抽样法,收集了嵌入在44位创业者中的684份有效问卷。跨层回归结果表明,当创业者核心自我评价高时,焦虑情绪积极促进创业努力;当创业者创业身份中心性高时,焦虑情绪积极促进创业努力;当创业者的核心自我评价和创业身份中心性均高时,焦虑情绪最大程度激发创业努力。隔日配对数据结果表明,在核心自我评价和创业认同中心性水平均高的情况下,当日焦虑情绪体验的激励作用可以持续到次日。研究结论不仅丰富了创业情境下焦虑情绪研究,揭开了焦虑与创业努力复杂关系;而且回应了关于情绪能否直接导致行为观点的质疑,丰富了创业努力情感观研究。

化子坪长6储层长岩心CO_(2)驱替实验及数值模拟评价

二氧化碳驱提高石油采收率(CO_(2)-EOR)在我国大部分低渗透、低孔隙度油藏中的应用越来越重要。鉴于国家净零排放目标,在采用二氧化碳驱提高采收率时,二氧化碳封存是另一个重要考虑因素。针对低渗油藏,开展天然岩心长岩心CO_(2)驱替试验,并利用TOGA(TOUGH Oil,Gas,Aqueous)软件建立岩心尺度数值模型开展模型的识别与验证,对模型的有效性及物性参数进行敏感性分析,结果表明,1)根据出口气油比可将二氧化碳驱油与封存划分为未见气(0~100)、极少量气(100~1 000)、气体突破(1 000~10 000)、大量气窜(>10000)四个不同阶段;2)孔隙度、渗透率及非均质性对模拟结果影响较大,在后续实际场地模型中应予以重点关注。研究结果可为实际场地规模模型提供参数依据。

南海东部深层定向井防电测卡“S”井身设计及应用

针对海上油田深层定向电缆测井遇阻遇卡现象较多、录取资料困难的问题,提出了在非目的层井段完成造斜和降斜,并用套管封固,再采用直井段揭开目的层,形成“S”型井眼的设计方案,并通过优化钻井液性能,确保井壁稳定性,优选飞轮代替传统的测井工具扶正器等措施,最终实现资料录取目的,大大降低了电缆测井作业风险,目前已在南海东部推广应用。

关于加强我国实物地质资料统筹保管工作的思考

实物地质资料是地质勘探工作形成的宝贵资源,确保重要实物地质资料安全妥善保管是实现其潜在价值有效保存和高效利用的重要保障,而如何改进日益增长的重要岩芯保管需求和有限的库房建设之间的矛盾,是当前我国实物地质资料保管工作面临的重要问题。笔者等系统总结了近年来我国实物地质资料保管工作在制度建设、库房建设等方面取得的重要成果,分析了当前面临的主要问题,研究并提出了我国实物地质资料统筹保管工作的总体布局、机制建立等方面的建议,为提升我国实物地质资料统筹保管能力提供参考。