The synthesis of photosensitive 1-(3-aminophenyl)-3-(4-aminophenyl)-2-propen-1-one(Ⅵ) was carried out by an adol condensation reaction of 3-acetylacetanilide and 4-acetamidobenzaldehyde using NaOH solution as catalys...The synthesis of photosensitive 1-(3-aminophenyl)-3-(4-aminophenyl)-2-propen-1-one(Ⅵ) was carried out by an adol condensation reaction of 3-acetylacetanilide and 4-acetamidobenzaldehyde using NaOH solution as catalyst with total yield of 61.9%. The optimum synthesis conditions were obtained. The method has the advantages of low cost, high yield and easy operation. The target compound was characterized by elemental analysis, IR and NMR. Its maximal UV-Vis absorption is at 349 nm.展开更多
文摘The synthesis of photosensitive 1-(3-aminophenyl)-3-(4-aminophenyl)-2-propen-1-one(Ⅵ) was carried out by an adol condensation reaction of 3-acetylacetanilide and 4-acetamidobenzaldehyde using NaOH solution as catalyst with total yield of 61.9%. The optimum synthesis conditions were obtained. The method has the advantages of low cost, high yield and easy operation. The target compound was characterized by elemental analysis, IR and NMR. Its maximal UV-Vis absorption is at 349 nm.
