Based on the bulging principle of different ellipticity dies, the methyl vinyl silicone rubber with excellent thermal stability and heat transfer performance was chosen as the viscous medium. The finite element analys...Based on the bulging principle of different ellipticity dies, the methyl vinyl silicone rubber with excellent thermal stability and heat transfer performance was chosen as the viscous medium. The finite element analysis and experiments of viscous warm pressure bulging （VWPB） of AZ31B magnesium alloy were conducted to analyze the influence of different ellipticity dies on the formability of AZ31B magnesium alloy. At the same time, based on the grid strain rule, the forming limit diagram （FLD） of VWPB of AZ31B magnesium alloy was obtained through measuring the strain of bulging specimens. The results showed that at the temperature range of viscous medium thermal stability, the viscous medium can fit the geometry variation of sheet and generate non-uniform pressure field, and as the die ellipticity increases, the difference value of non-uniform pressure reduces. Meanwhile, according to the FLD, the relationship between part complexity and ultimate deformation was investigated.展开更多
The microstructure and mechanical properties of A357 alloy under differential pressure casting process with different casting mould materials were studied. The results show that by using SiO2 resin sand the grain size...The microstructure and mechanical properties of A357 alloy under differential pressure casting process with different casting mould materials were studied. The results show that by using SiO2 resin sand the grain size is biggest and the tensile and elongation are the lowest, while the grain size is the smallest and the tensile strength and elongation are the highest when the chill is used, and the grain size, tensile strength and elongation of A357 alloy with SiC resin sand mould are in the middle. Furthermore, the results also demonstrate that for thin wall castings during differential pressure casting processes the grain size, tensile strength and elongation are different at different positions corresponding to the same casting mould material, while at the position of gating the grain size is the smallest and the tensile strength and elongation have the highest values. At the position of edge the grain size, the tensile strength and elongation take the second place. However, in the middle of the thin wall castings the grain size is coarsest and the tensile strength and elongation are the lowest.展开更多
With the diversification of manufacture methods, joining the same materials with different states becomes indispensable in practical application. In present work, 6061 aluminum alloys with different states were welded...With the diversification of manufacture methods, joining the same materials with different states becomes indispensable in practical application. In present work, 6061 aluminum alloys with different states were welded by laser beam welding （LBW）. The microstructures of welded joint, before and after heat treating, were investigated. The mechanical properties, such as the tensile properties and microhardness , were tested. And the fracture characteristic was observed by means of scanning electron microscope （SEM）. The results show that the 6061 aluminum alloys have superior weldability and the microstructures are different significantly in different states. Besides, the grain boundaries of the joint microstructures become unclear after the heat treating. The strength and the elongations of welded joints could reach to those of the base metal. The tensile fracture occurs in the fusion zone and near 6061-0 alloy. And the fracture presents ductile rupture. Therefore, the LBW is an effective method for 6061 aluminum alloy.展开更多
The microstructure of differently annealed nanocrystalline Fe72.7Cu1Nb1.8Mo2Si13B9.5 alloy was investigated by using Mssbauer spectroscopy and transmission electron microscope. The specimens were isochronally annealed...The microstructure of differently annealed nanocrystalline Fe72.7Cu1Nb1.8Mo2Si13B9.5 alloy was investigated by using Mssbauer spectroscopy and transmission electron microscope. The specimens were isochronally annealed at temperatures between 480℃ and 600℃ for 0.5 h. The experimental results show that the microstructure mainly consists of the nanoscale bcc α-Fe(Si) grains and the residual amorphous matrix phase. A trace paramagnetic phase was found for annealing about above 500℃. The volume fraction of cr-Fe(Si) grain increases with increasing annealing temperature, whereas the average size of grain is almost unchanged above 480℃ up to 580℃. The calculated thickness of the intergranular layer of the residual amorphous matrix clearly decreases with increasing annealing temperature.展开更多
The structures of the bulk amorphous Zr41Ti14Cu12.5Nil0.0Be22.5 alloy have been analyzed in solid, supercooled liquid and liquid with X-ray diffraction. The first coordination sphere radii and the first coordination n...The structures of the bulk amorphous Zr41Ti14Cu12.5Nil0.0Be22.5 alloy have been analyzed in solid, supercooled liquid and liquid with X-ray diffraction. The first coordination sphere radii and the first coordination numbers are 0.312 um, 11.2 in solid state.10.932 nm, 10.932 in supercooled liquid region and 0.305 urn, 11.296 in liquid state. The structures are the same in different states. But it shows some tendency to crystallizing that the first coordination sphere radius and the first coordination number drop in supercooled liquid region.展开更多
The microstructure and the stability of Fe_73.5Cu_1Nb_3Si_13.5B_9 alloy at different stages of phase transformation were investigated through the observation of X-ray difraction and transmission electron microscopy an...The microstructure and the stability of Fe_73.5Cu_1Nb_3Si_13.5B_9 alloy at different stages of phase transformation were investigated through the observation of X-ray difraction and transmission electron microscopy and the measurement of magnetic aftereffect (MAE). It was found that the dependence of the volume fraction of amorphous phase and the MAE in the samples annealed from 450 to 700℃ on the annealing temperature is similar.展开更多
Formation condition of high-entropy alloys with solid solution structure was investigated. Seventeen kinds of the high-entropy alloys with different components were prepared, the influencing factors （the comprehensiv...Formation condition of high-entropy alloys with solid solution structure was investigated. Seventeen kinds of the high-entropy alloys with different components were prepared, the influencing factors （the comprehensive atomic radius difference δ, the mixing enthalpy AH and the mixing entropy AS） of phase composition of the alloys were calculated, and the microstructure and phase compositions of alloys were analyzed by using SEM and XRD. The result shows that only the systems with δ≤2.77 and △H≥-8.8 kJ/mol will form high entropy alloy with simple solid solution. Otherwise, intermetallic compounds will exist in the alloys. So, selection of the type of element has important effects on microstructure and properties of high entropy alloys.展开更多
基金Project(51575364)supported by the National Natural Science Foundation of ChinaProject(2013024014)supported by the Natural Foundation of Liaoning Province,China
文摘Based on the bulging principle of different ellipticity dies, the methyl vinyl silicone rubber with excellent thermal stability and heat transfer performance was chosen as the viscous medium. The finite element analysis and experiments of viscous warm pressure bulging （VWPB） of AZ31B magnesium alloy were conducted to analyze the influence of different ellipticity dies on the formability of AZ31B magnesium alloy. At the same time, based on the grid strain rule, the forming limit diagram （FLD） of VWPB of AZ31B magnesium alloy was obtained through measuring the strain of bulging specimens. The results showed that at the temperature range of viscous medium thermal stability, the viscous medium can fit the geometry variation of sheet and generate non-uniform pressure field, and as the die ellipticity increases, the difference value of non-uniform pressure reduces. Meanwhile, according to the FLD, the relationship between part complexity and ultimate deformation was investigated.
文摘The microstructure and mechanical properties of A357 alloy under differential pressure casting process with different casting mould materials were studied. The results show that by using SiO2 resin sand the grain size is biggest and the tensile and elongation are the lowest, while the grain size is the smallest and the tensile strength and elongation are the highest when the chill is used, and the grain size, tensile strength and elongation of A357 alloy with SiC resin sand mould are in the middle. Furthermore, the results also demonstrate that for thin wall castings during differential pressure casting processes the grain size, tensile strength and elongation are different at different positions corresponding to the same casting mould material, while at the position of gating the grain size is the smallest and the tensile strength and elongation have the highest values. At the position of edge the grain size, the tensile strength and elongation take the second place. However, in the middle of the thin wall castings the grain size is coarsest and the tensile strength and elongation are the lowest.
文摘With the diversification of manufacture methods, joining the same materials with different states becomes indispensable in practical application. In present work, 6061 aluminum alloys with different states were welded by laser beam welding （LBW）. The microstructures of welded joint, before and after heat treating, were investigated. The mechanical properties, such as the tensile properties and microhardness , were tested. And the fracture characteristic was observed by means of scanning electron microscope （SEM）. The results show that the 6061 aluminum alloys have superior weldability and the microstructures are different significantly in different states. Besides, the grain boundaries of the joint microstructures become unclear after the heat treating. The strength and the elongations of welded joints could reach to those of the base metal. The tensile fracture occurs in the fusion zone and near 6061-0 alloy. And the fracture presents ductile rupture. Therefore, the LBW is an effective method for 6061 aluminum alloy.
文摘The microstructure of differently annealed nanocrystalline Fe72.7Cu1Nb1.8Mo2Si13B9.5 alloy was investigated by using Mssbauer spectroscopy and transmission electron microscope. The specimens were isochronally annealed at temperatures between 480℃ and 600℃ for 0.5 h. The experimental results show that the microstructure mainly consists of the nanoscale bcc α-Fe(Si) grains and the residual amorphous matrix phase. A trace paramagnetic phase was found for annealing about above 500℃. The volume fraction of cr-Fe(Si) grain increases with increasing annealing temperature, whereas the average size of grain is almost unchanged above 480℃ up to 580℃. The calculated thickness of the intergranular layer of the residual amorphous matrix clearly decreases with increasing annealing temperature.
文摘The structures of the bulk amorphous Zr41Ti14Cu12.5Nil0.0Be22.5 alloy have been analyzed in solid, supercooled liquid and liquid with X-ray diffraction. The first coordination sphere radii and the first coordination numbers are 0.312 um, 11.2 in solid state.10.932 nm, 10.932 in supercooled liquid region and 0.305 urn, 11.296 in liquid state. The structures are the same in different states. But it shows some tendency to crystallizing that the first coordination sphere radius and the first coordination number drop in supercooled liquid region.
基金National Natural &ience Foundation of China!(No. 59671020).
文摘The microstructure and the stability of Fe_73.5Cu_1Nb_3Si_13.5B_9 alloy at different stages of phase transformation were investigated through the observation of X-ray difraction and transmission electron microscopy and the measurement of magnetic aftereffect (MAE). It was found that the dependence of the volume fraction of amorphous phase and the MAE in the samples annealed from 450 to 700℃ on the annealing temperature is similar.
基金Project(HIT.NSRIF.2009090) supported by Natural Scientific Research Innovation Foundation in Harbin Institute of Technology,China
文摘Formation condition of high-entropy alloys with solid solution structure was investigated. Seventeen kinds of the high-entropy alloys with different components were prepared, the influencing factors （the comprehensive atomic radius difference δ, the mixing enthalpy AH and the mixing entropy AS） of phase composition of the alloys were calculated, and the microstructure and phase compositions of alloys were analyzed by using SEM and XRD. The result shows that only the systems with δ≤2.77 and △H≥-8.8 kJ/mol will form high entropy alloy with simple solid solution. Otherwise, intermetallic compounds will exist in the alloys. So, selection of the type of element has important effects on microstructure and properties of high entropy alloys.
