Accurate measurement of ultrasonic velocity by eliminating the diffraction effect

The accurate measurement method of ultrasonic velocity by the pulse interference method with eliminating the diffraction effect has been investigated in VHF range experimentally. Two silicate glasses were taken as the specimens, their frequency dependences of longitudinal velocities were measured in the frequency range 50-350 MHz, and the phase advances of ultrasonic signals caused by diffraction effect were calculated using A. O. Williams' theoretical expression. For the frequency dependences of longitudinal velocities, the measurement results were in good agreement with the simulation ones in which the phase advances were included. It has been shown that the velocity error due to diffraction effect can be corrected very well by this method.

The magnetic properties and magnetocaloric effects in binary R-T(R = Pr,Gd,Tb,Dy,Ho,Er,Tm;T = Ga,Ni,Co,Cu)intermetallic compounds

In this paper, we review the magnetic properties and magnetocaloric effects（MCE） of binary R–T（R = Pr, Gd, Tb,Dy, Ho, Er, Tm; T = Ga, Ni, Co, Cu） intermetallic compounds（including RGa series, RNi series, R_（12）Co_7 series, R_3 Co series and RCu_2series）, which have been investigated in detail in the past several years. The R–T compounds are studied by means of magnetic measurements, heat capacity measurements, magnetoresistance measurements and neutron powder diffraction measurements. The R–T compounds show complex magnetic transitions and interesting magnetic properties.The types of magnetic transitions are investigated and confirmed in detail by multiple approaches. Especially, most of the R–T compounds undergo more than one magnetic transition, which has significant impact on the magnetocaloric effect of R–T compounds. The MCE of R–T compounds are calculated by different ways and the special shapes of MCE peaks for different compounds are investigated and discussed in detail. To improve the MCE performance of R–T compounds,atoms with large spin（S） and atoms with large total angular momentum（J） are introduced to substitute the related rare earth atoms. With the atom substitution, the maximum of magnetic entropy change（？SM）, refrigerant temperature width（Twidth）or refrigerant capacity（RC） is enlarged for some R–T compounds. In the low temperature range, binary R–T（R = Pr, Gd,Tb, Dy, Ho, Er, Tm; T = Ga, Ni, Co, Cu） intermetallic compounds（including RGa series, RNi series,R_（12）Co_7 series, R_3 Co series and RCu_2series） show excellent performance of MCE, indicating the potential application for gas liquefaction in the future.

Angle Compensation and Asymmetry Effect of Light Diffracted by Millimeter Liquid Surface Slosh Wave

The angle compensation method is adopted to detect sloshing waves by laser diffraction, in the case that the wavelength of the sloshing waves is much greater than that of the incident light. The clear diffraction pattern is observed to be of asymmetry, involving orders, position and interval of the diffraction spots that are discovered during the light grazing incidence. It is found that the larger the angle of incidence is, the more obvious the asymmetry is. The higher the negative diffraction orders are, the smaller the intervals between spots are. On the contrary~ in the positive region, the higher the diffraction orders are, the larger the spot intervals are. The positive interval is larger than that of the same negative diffraction order. If the incident angle reaches 1.558 rad in the experiment, all positive diffraction orders completely vanish. Based on the mechanism of phase modulation and with the Fourier transform method, the relations between the incident angle and position, interval spaces, and orders of diffraction spots are derived theoretically. The theoretical calculations are compared with the experimental data, and the comparison shows that the theoretical calculations are in good agreement with the experimental measurement.

Infrared transition properties of vanadium dioxide thin films across semiconductor-metal transition

Vanadium dioxide thin films were fabricated through annealing vanadium oxide thin films deposited by dual ion beam sputtering. X-ray diffraction （XRD）, atom force microscopy （AFM）, and Fourier transform infrared spectrum （FTIR） were employed to measure the crystalline structure, surface morphology, and infrared optical transmittance. The phase transition properties were characterized by transmittance. The results show that the annealed vanadium oxide thin film is composed of monoclinic VO2, with preferred orientation of （011）. The maximum of transmittance change is beyond 65% as the temperature increases from 20 to 80 C. The reversible changes in optical transmittance against temperature were observed. The change rate of transmittance at short wavelength is higher than that at long wavelength at the same temperature across semiconductor-metal phase transition. This phenomenon was discussed using diffraction effect.

Quantitative measurement of magnetic parameters by electron magnetic chiral dichroism

Electron magnetic circular dichroism opens a new door to explore magnetic properties by transmitted electrons in the transmission electron microscope. However, obtaining quantitative magnetic parameters, such as spin and orbital magnetic moment with element-specificity, goes a long way along with the development and improvement of this technique both in theoretical and experimental aspects. In this review, we will give a detailed description of the quantitative electron magnetic circular dichroism（EMCD） technique to measure magnetic parameters with spin-specificity, element-specificity,site-specificity, and orbital-spin-specificity. The discussion completely contains the procedures from raw experimental data acquisition to final magnetic parameters, together with the related custom code we have developed.

Effect of diffraction on the ultrasonic velocity measuredby the pulse interference method in VHF range

The effect of diffraction on the ultrasonic velocity measured by the pulse interference method has been investigated in VHF range theoretically and experimentally. Two silicate glasses are taken as the specimens, their frequency dependences of longitudinal velocities are measured in the frequency range of 50-350 MHz, and the phase advances of ultrasonic signals caused by diffraction effect are calculated using A. O. Williams' theoretical expression. For the velocity error due to diffraction effect, the experimental results are in good agreement with the theoretical prediction. It has been shown that the velocity error due to diffraction effect is directly proportional to dθ21 (f)/df, whereθ21 (f) is the phase advances difference between the two partial reflection signals used in velocity measurement and f is the ultrasonic frequency.

Asymmetric dynamic phase holographic grating in nematic liquid crystal

A new scheme for recording a dynamic phase grating with an asymmetric profile in C60-doped homeotropically aligned nematic liquid crystal（NLC） was presented.An oblique incidence beam was used to record the thin asymmetric dynamic phase holographic grating.The diffraction efficiency we achieved is more than 40%,exceeding the theoretical limit for symmetric profile gratings.Both facts can be explained by assuming that a grating with an asymmetric saw-tooth profile is formed in the NLC.Finally,physical mechanism and mathematical model for characterizing the asymmetric phase holographic grating were presented,based on the photo-refractive-like（PR-like） effect.

Hydrodynamic scaling and wave force estimation of offshore structures

Offshore structures are generally classified as small-scale structures or large-scale structures.Their wave forces are then estimated by Morison equation and diffraction/radiation theories,respectively.However,the classification criterion is not well quantified.In the present paper,a numerical wave flume is established to simulate the wave forces acting on a fixed and vertical surface-piercing circular cylinder under linear waves.By solving Navier–Stokes equation and Euler equation with free surface involved,respectively,the viscous force and inertia force are separated accurately.The variation of viscous force and inertia force with the cylinder diameter to wave length ratio is discussed in detail.The scale intervals for significant viscous and diffraction effects are given.The error caused by neglecting viscous and diffraction forces is quantitatively analyzed.Based on these analysis,the concept of medium-scale structure is proposed and the classification criteria for small-,medium-and large-scale structures are given.In the meantime,the estimation methods of wave forces for different scales of structures are suggested.

Investigation on the InAs(1–x)Sbx epilayers growth on GaAs(001)substrate by molecular beam epitaxy

Undoped and Be-doped InAs（1–x）Sbx（0 ≤ x ≤ 0.71） epitaxial layers were successfully grown on lattice mismatched semi-insulating Ga As（001） substrate with 2° offcut towards 〈110〉. The effect of the In As buffer layer on the quality of the grown layers was investigated. Moreover, the influence of Sb/In flux ratio on the Sb fraction was examined. Furthermore, we have studied the defects distribution along the depth of the In As Sb epilayers.In addition, the p-type doping of the grown layers was explored. The In As Sb layers were assessed by X-ray diffraction, Nomarski microscopy, high resolution optical microscopy and Hall effect measurement. The In As buffer layer was found to be beneficial for the growth of high quality In As Sb layers. The X-ray analysis revealed a full width at half maximum（FWHM） of 571 arcsec for In As0.87 Sb0.13. It is worth noting here that the Hall concentration（mobility） as low（high） as 5 × 10^（16）cm^（-3）（25000 cm^2 V^（-1）s^（-1）） at room temperature, has been acquired.