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Investigation on the Thermal Conductivity of 3-Dimensional and 4-Directional Braided Composites 被引量:24
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作者 Liu Zhenguo Zhang Haiguo Lu Zixing Li Diansen 《Chinese Journal of Aeronautics》 SCIE EI CAS CSCD 2007年第4期327-331,共5页
It is vital to choose a factual and reasonable micro-structural model of braided composites for improving the calculating precision of thermal property of 3-D braided composites by finite element method (FEM). On th... It is vital to choose a factual and reasonable micro-structural model of braided composites for improving the calculating precision of thermal property of 3-D braided composites by finite element method (FEM). On the basis of new microstructure model of braided composites proposed recently, the model of FEM calculation for thermal conductivity of 3-dimennsional and 4-directional braided composites is set up in this paper. The curves of coefficient of effective thermal conductivity versus fiber volume ratio and interior braiding angle are obtained. Furthermore, comparing the results of FEM with the available experimental data, the reasonability and veracity of calculation are confirmed at the same time. 展开更多
关键词 3-dimennsional and 4-directional braided composites thermal conductivity FEM
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Direct current hopping conductance in one-dimensional diagonal disordered systems
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作者 马松山 徐慧 +1 位作者 刘小良 肖剑荣 《Chinese Physics B》 SCIE EI CAS CSCD 2006年第1期190-194,共5页
Based on a tight-binding disordered model describing a single electron band, we establish a direct current (de) electronic hopping transport conductance model of one-dimensional diagonal disordered systems, and also... Based on a tight-binding disordered model describing a single electron band, we establish a direct current (de) electronic hopping transport conductance model of one-dimensional diagonal disordered systems, and also derive a dc conductance formula. By calculating the dc conductivity, the relationships between electric field and conductivity and between temperature and conductivity are analysed, and the role played by the degree of disorder in electronic transport is studied. The results indicate the conductivity of systems decreasing with the increase of the degree of disorder, characteristics of negative differential dependence of resistance on temperature at, low temperatures in diagonal disordered systems, and the conductivity of systems decreasing with the increase of electric field, featuring the non-Ohm's law conductivity. 展开更多
关键词 direct current hopping conductivity diagonal disordered systems the degree of disorder
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ALTERNATING-DIRECTION MULTISTEP PRECONDITIONED ITERATIVE METHODS FOR SEMICONDUCTOR PROBLEM WITH HEAT-CONDUCTION
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作者 Liu Yunxian(刘蕴贤) 《Numerical Mathematics A Journal of Chinese Universities(English Series)》 SCIE 2002年第1期13-24,共12页
The model of transient behavior of semiconductor with heat-conduction is an initial and boundary problem. Alternating-direction multistep preconditioned iterative methods and theory analyses are given in this paper. E... The model of transient behavior of semiconductor with heat-conduction is an initial and boundary problem. Alternating-direction multistep preconditioned iterative methods and theory analyses are given in this paper. Electric potential equation is approximated by mixed finite element method, concentration and heat-conduction equations are approximated by Galerkin alternating-direction multistep methods. Error estimates of optimal order in L2 are demonstrated. 展开更多
关键词 transient behavior of semiconductor heat-conduction mixed FINITE element alternating-direction multistep.
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Effective Thermal Conductivity for 3D Five-Directional Braided Composites Based on Microstructural Analysis
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作者 ZHAO Xiao MAO Junkui JIANG Hua 《Transactions of Nanjing University of Aeronautics and Astronautics》 EI CSCD 2019年第1期128-138,共11页
A method for predicting effective thermal conductivities(ETCs) of three-dimensional five-directional(3D5D) braided composites is presented. The effective thermal conductivity prediction method contains a digital image... A method for predicting effective thermal conductivities(ETCs) of three-dimensional five-directional(3D5D) braided composites is presented. The effective thermal conductivity prediction method contains a digital image processing technology. Multiple scanning electron microscopy(SEM)images of composites are analyzed to obtain actual microstructural features. These actual microstructural features of 3D5D braided composites are introduced into representative volume element(RVE) modeling. Apart from applying actual microstructural features,compression effects between yarns are considered in the modeling of RVE,making the RVE more realistic. Therefore,the ETC prediction method establishes a representative unit cell model that better reflects the true microstructural characteristics of the 3D5D braided composites. The ETCs are predicted with the finite element method. Then thermal conductivity measurements are carried out for a 3D5D braided composite sample.By comparing the predicted ETC with the measured thermal conductivity, the whole process of the ETC prediction method is proved to be effective and accurate,where a relative error of only 2.9 % is obtained.Furthermore,the effects of microstructural features are investigated,indicating that increasing interior braiding angles and fiber fill factor can lead to higher transverse ETCs. Longitudinal ETCs decrease with increasing interior braiding angles,but increase with increasing fiber fill factor. Finally,the influence of variations of microstructure parameters observed in digital image processing are investigated. To explore the influence of variations in microstructural features on variations in predicted ETCs,the actual probability distributions of microstructural features obtained from the 3D5D braided composite sample are introduced into the ETC investigation. The results show that,compared with the interior braiding angle,variations in the fiber fill factor exhibit more significant effects on variations in ETCs. 展开更多
关键词 EFFECTIVE thermal conductIVITY digital IMAGE processing VARIATION 3D five-directional braided COMPOSITES
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Study of ultrahigh-purity copper billets refined by vacuum melting and directional solidification 被引量:6
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作者 FU Yabo CHEN Jie +3 位作者 LIU Ning LU Yiping LI Tingju YIN Guomao 《Rare Metals》 SCIE EI CAS CSCD 2011年第3期304-309,共6页
The purpose of this paper is to study large-sized copper billets refined with 5N ultrahigh purity after vacuum melting and directional solidifi-cation (VMDS). The precise impurity analysis of copper billets was carr... The purpose of this paper is to study large-sized copper billets refined with 5N ultrahigh purity after vacuum melting and directional solidifi-cation (VMDS). The precise impurity analysis of copper billets was carried out with a glow discharge mass spectrometer (GDMS). The re-sults demonstrate that the total concentration of twenty-two impurities is decreased by 63.1wt.%-66.5 wt.%. Ag, P, S, Na, Mg, Se, Zn, In and Bi are easy to be removed due to lgPimp - lgPCu 1.5, and they can be removed effectively under the vacuum condition of 1650-1700 K for 30 min. The electrical conductivity of 5N copper is higher than that of the raw material as the impurity concentrations decrease. The segrega-tion effect in directional solidification can be remarkable when the equilibrium distribution coefficient (k0) value is less than 0.65 due to the strong affinity of Cu for some metallic and non-metallic impurities. 展开更多
关键词 COPPER REFINING vacuum melting directional solidification electrical conductivity
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Directional solidification and physical properties measurements of the zinc-aluminum eutectic alloy 被引量:3
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作者 S.Engin U.Byük +1 位作者 H.Kaya N.Maraslι 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2011年第6期659-664,共6页
Zn-5wt% Al eutectic alloy was directionally solidified with different growth rates (5.32-250.0μm/s) at a constant temperature gradient of 8.50 K/mm using a Bridgman-type growth apparatus.The values of eutectic spac... Zn-5wt% Al eutectic alloy was directionally solidified with different growth rates (5.32-250.0μm/s) at a constant temperature gradient of 8.50 K/mm using a Bridgman-type growth apparatus.The values of eutectic spacing were measured from transverse sections of the samples.The dependences of the eutectic spacing and undercooling on growth rate are determined as λ=9.21V-0.53 and ΔT=0.0245V0.53,respectively.The results obtained in this work were compared with the Jackson-Hunt eutectic theory and the similar experimental results in the literature.Microhardness of directionally solidified samples was also measured by using a microhardness test device.The dependency of the microhardness on growth rate is found as Hv=115.64V0.13.Afterwards,the electrical resistivity (r) of the casting alloy changes from 40×10-9 to 108×10-9 Ω·m with the temperature rising in the range of 300-630 K.The enthalpy of fusion (ΔH) and specific heat (Cp) for the Zn-Al eutectic alloy are calculated to be 113.37 J/g and 0.309 J/(g·K),respectively by means of differential scanning calorimetry (DSC) from heating trace during the transformation from liquid to solid. 展开更多
关键词 eutectic alloys directional solidification microhardness electrical conductivity enthalpy specific heat
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Electric-Jet Assisted Layer-by-Layer Deposition of Gold Nanoparticles to Prepare Conducting Tracks
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作者 S. R. Samarasinghe Isabel Pastoriza-Santos +4 位作者 M. J. Edirisinghe M. J. Reece Luis Liz-Marzán M. R. Nangrejo Z. Ahmad 《Natural Science》 2009年第2期142-150,共9页
A suspension of 15nm diameter gold nanoparti-cles has been deposited along a line on a silicon substrate with the assistance of a jet generated in an electric field. In order to control the evaporation of the solvent ... A suspension of 15nm diameter gold nanoparti-cles has been deposited along a line on a silicon substrate with the assistance of a jet generated in an electric field. In order to control the evaporation of the solvent used to suspend the gold nanoparticles, a heating device was used to change the substrate temperature. Layer-by- layer deposition enabled the direct writing of gold tracks having an electrical resistivity of 1.8 × 10-7 Ωm, only about an order of magnitude above the electrical resistivity of bulk gold. 展开更多
关键词 Gold ELECTROHYDRODYNAMIC JET direct WRITE Track Electrical conductIVITY
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Mechanical, electrical, and thermal properties of the directionally solidified Bi–Zn–Al ternary eutectic alloy
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作者 M.Sahin E.adrli 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2014年第10期999-1008,共10页
A Bi-2.0Zn-0.2A1 (wt%) ternary eutectic alloy was prepared using a vacuum melting furnace and a casting furnace. The samples were directionally solidified upwards at a constant growth rate (V= 18.4 μm/s) under di... A Bi-2.0Zn-0.2A1 (wt%) ternary eutectic alloy was prepared using a vacuum melting furnace and a casting furnace. The samples were directionally solidified upwards at a constant growth rate (V= 18.4 μm/s) under different temperature gradients (G = 1.15-3.44 K/mm) and at a constant temperature gradient (G = 2.66 K/mm) under different growth rates (V= 8.3-500 μm/s) in a Bridgman-type directional so- lidification furnace. The dependence ofmicrostructure parameter (2) on the solidification parameters (G and V) and that of the microhardness (Hv) on the microstructure and solidification parameters were investigated. The resistivity (ρ) measurements of the studied alloy were per- formed using the standard four-point-probe method, and the temperature coefficient of resistivity (α) was calculated from the ρ-Tcurve. The enthalpy (AH) and the specific heat (Cp) values were determined by differential scanning calorimetry analysis. In addition, the thermal conductivities of samples, obtained using the Wiedemann-Franz and Smith-Palmer equations, were compared with the experimental results. The results revealed that, the thermal conductivity values obtained using the Wiedemarm-Franz and Smith-Palmer equations for the Bi-2.0Zn-0.2Al (wt%) alloy are in the range of 5.2-6.5 W/Km and 15.2-16.4 W/Km, respectively. 展开更多
关键词 ternary eutectic alloys directional solidification MICROHARDNESS electrical resistivity thermal conductivity
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经颅直流电刺激对卒中后传导性失语症患者语言功能的治疗效果研究
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作者 张大华 宋为群 +3 位作者 张甜甜 程亦男 汪洁 赵钰婷 《中国脑血管病杂志》 CAS CSCD 北大核心 2024年第10期678-683,共6页
目的探讨经颅直流电刺激(tDCS)干预左侧大脑外侧裂后部颞顶联合区对卒中后传导性失语症患者语言功能的治疗效果。方法前瞻性连续纳入2021年6月至2024年4月在首都医科大学宣武医院康复医学科治疗的卒中后失语症患者。本研究采用自身交叉... 目的探讨经颅直流电刺激(tDCS)干预左侧大脑外侧裂后部颞顶联合区对卒中后传导性失语症患者语言功能的治疗效果。方法前瞻性连续纳入2021年6月至2024年4月在首都医科大学宣武医院康复医学科治疗的卒中后失语症患者。本研究采用自身交叉随机对照试验,入组患者经西方失语成套测验诊断标准评估为传导性失语。将12例卒中后传导性失语症患者完全随机分为A组(治疗顺序:A期—洗脱期—B期)和B组(治疗顺序:B期—洗脱期—A期),各6例。A期为tDCS真干预联合言语语言训练,B期为tDCS假干预联合言语语言训练,洗脱期仅接受言语语言训练,每期均训练5 d。tDCS阳极为刺激电极,放置于刺激靶点;阴极为参考电极,放置于右侧肩部。tDCS的强度为1.4 mA,真刺激为20 min/次,假刺激仅30 s/次后自动停止,均2次/d,共治疗10次。言语语言训练30 min/次,2次/d,共训练10次。A、B期治疗前和治疗后立即进行复述和视图命名(训练项和非训练项)功能检查,并比较A期与B期治疗前后复述和视图命名(训练项和非训练项)功能评分的差值。结果(1)A组与B组患者性别、年龄、病程、受教育程度的差异均无统计学意义(均P>0.05)。(2)康复治疗前,A组与B组患者复述和视图命名(训练项、非训练项)功能评分的差异均无统计学意义(均P>0.05)。(3)A组与B组内洗脱期治疗前后复述和视图命名(训练项、非训练项)功能评分的差异均无统计学意义(均P>0.05)。(4)与B期治疗前后的差值比较,A期患者治疗前后复述功能、视图命名(训练项)、视图命名(非训练项)功能评分的差值均较高[分别为(6.9±1.4)分比(2.2±1.0)分,t=9.604;(6.2±1.2)分比(1.8±1.1)分,t=9.277;(6.5±1.0)分比(1.5±1.0)分,t=12.247;均P<0.01]。结论初步分析显示,tDCS对左侧大脑外侧裂后部颞顶联合区脑组织的干预可能有助于改善卒中后传导性失语症患者复述和视图命名(训练项和非训练项)能力。本研究样本量较少,结果有待于进一步探讨。 展开更多
关键词 命名不能 失语 传导性 经颅直流电刺激 复述功能 视图命名
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改善剩余污泥厌氧消化产甲烷性能的新策略:导电材料介导微生物种间直接电子传递 被引量:1
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作者 罗进财 王欣芸 +3 位作者 孙鸿 董姗燕 田帅 朱易春 《应用化工》 CAS CSCD 北大核心 2024年第4期918-924,共7页
综述了近年来关于碳基和铁基导电材料促进DIET产甲烷的研究进展,归纳了直接种间电子传递的机制,总结了碳基和铁基导电材料的结构特征、电子传递机理和强化剩余污泥厌氧产甲烷效果。指出了当前研究存在的不足,并对未来的研究方向做出了... 综述了近年来关于碳基和铁基导电材料促进DIET产甲烷的研究进展,归纳了直接种间电子传递的机制,总结了碳基和铁基导电材料的结构特征、电子传递机理和强化剩余污泥厌氧产甲烷效果。指出了当前研究存在的不足,并对未来的研究方向做出了展望。 展开更多
关键词 剩余污泥 厌氧消化 直接种间电子传递 导电材料
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高导热多孔石墨预制体的制备及其性能
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作者 吴海华 魏恒 +4 位作者 吴正佳 郝佳欢 戢运鑫 曾世渝 李思维 《材料热处理学报》 CAS CSCD 北大核心 2024年第2期23-32,共10页
以天然鳞片石墨、酚醛树脂以及中间相碳微球为主要原料,制备多孔石墨预制体,经石墨化处理后再与环氧树脂复合,获得高导热石墨/环氧树脂复合材料。研究了素坯成形密度和粉末组成对多孔石墨预制体X-Y方向的导热性能与孔隙率的影响。结果表... 以天然鳞片石墨、酚醛树脂以及中间相碳微球为主要原料,制备多孔石墨预制体,经石墨化处理后再与环氧树脂复合,获得高导热石墨/环氧树脂复合材料。研究了素坯成形密度和粉末组成对多孔石墨预制体X-Y方向的导热性能与孔隙率的影响。结果表明:预制体内部石墨片定向排列,酚醛树脂与中间相碳微球连接其间,形成定向多孔网络结构,实现高导热、高孔隙与大孔径的协同。当素坯成形密度为1.4 g/cm^(3),天然鳞片石墨、酚醛树脂、中间相碳微球的含量分别为67.5 mass%、17.5 mass%和15 mass%时,多孔石墨预制体X-Y方向导热性能达到286.97 W/(m·K),气孔率达到44.56%;此时,石墨/环氧树脂复合材料X-Y方向导热性能达到116.81 W/(m·K)、抗压强度为26 MPa,在电子封装领域具有潜在的应用前景。 展开更多
关键词 高导热 定向排列结构 天然鳞片石墨 多孔材料制备
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捻度配置对双向包覆纱性能的影响及优化
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作者 王勇 乔启凡 +2 位作者 王宗乾 李长龙 王炜 《棉纺织技术》 CAS 2024年第2期43-50,共8页
为了纺制兼具回弹性和导电性的包覆纱,探讨捻度配置对包覆纱强伸性能和回弹性能的影响。以氨纶、不锈钢丝、棉股线为原料,基于空心锭包缠纺设备,纺制以氨纶为纱芯、不锈钢丝为第一外包覆层、棉股线为第二外包覆层的双向包覆纱。重点分... 为了纺制兼具回弹性和导电性的包覆纱,探讨捻度配置对包覆纱强伸性能和回弹性能的影响。以氨纶、不锈钢丝、棉股线为原料,基于空心锭包缠纺设备,纺制以氨纶为纱芯、不锈钢丝为第一外包覆层、棉股线为第二外包覆层的双向包覆纱。重点分析包缠捻度、外内捻度比等工艺参数对双向包覆纱的强伸性能、回弹性能的影响,利用主成分分析法对试验结果进行综合评判。结果表明:包缠捻度和外内捻度比对双向包覆纱强伸性能影响显著。在设定范围内,当包缠捻度800捻/m、外内捻度比1.0时,双向包覆纱综合质量较优。双向包覆纱在拉伸态下具有优良的导电特性,拓展了其在柔性可拉伸导线和柔弹电加热器件领域的应用范畴。认为:纺制兼具回弹性和导电性的双向包覆纱时,捻度配置是关键参数。 展开更多
关键词 双向包覆纱 强伸性 回弹性 主成分分析 导电性 焦耳热
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热解温度对直写3D打印石墨烯/SiC_(p)/SiC复合材料性能的影响
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作者 唐润 刘洪军 李亚敏 《陶瓷学报》 CAS 北大核心 2024年第5期959-967,共9页
通过在碳化硅前驱体聚碳硅烷(PCS)溶液中加入石墨烯/SiC_(p)复合粉末,获得石墨烯/SiC_(p)/PCS浆料,采用直写3D打印(DIW)和高温烧结相结合制备了石墨烯/SiC_(p)/SiC复合材料。PCS在不同热解温度下具有不同的产物与性能,本文研究了热解温... 通过在碳化硅前驱体聚碳硅烷(PCS)溶液中加入石墨烯/SiC_(p)复合粉末,获得石墨烯/SiC_(p)/PCS浆料,采用直写3D打印(DIW)和高温烧结相结合制备了石墨烯/SiC_(p)/SiC复合材料。PCS在不同热解温度下具有不同的产物与性能,本文研究了热解温度对石墨烯/SiC_(p)/SiC复合材料性能的影响。800℃时PCS转化为非晶SiCxOy,随着温度升高至1500℃,非晶SiCxOy逐渐生成导电性更好的β-SiC与游离碳,石墨烯/SiC_(p)/SiC复合材料的电导率从0.93 S·m^(-1)升高至670 S·m^(-1)。1200℃时,复合材料抗压强度和容积密度分别达到最大的12.3 MPa和1.49 g·cm^(-3)。该研究提供了一种基于PCS浆料的直写3D打印工艺制备高导电轻质多孔石墨烯/SiC_(p)/SiC复合陶瓷的方法。 展开更多
关键词 3D打印 直写成型 热解温度 石墨烯/SiC_(p)/SiC复合材料 抗压强度 电导率
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开绕组BLDCM直接转矩控制电压矢量特性研究
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作者 华文韬 杨建飞 +6 位作者 邱鑫 陈秋仲 刘业 胡伦 周锴 刘畅 陈洪生 《微特电机》 2024年第4期8-15,共8页
基于直接转矩控制(DTC)的开绕组无刷直流电机(BLDCM)具有运行效率高、电压矢量多样、控制结构简单等优点,适用于工业领域。根据共直流母线开绕组BLDCM控制拓扑搭建了相应的数学模型,对该拓扑下电压矢量的特性进行理论分析及分类,并将电... 基于直接转矩控制(DTC)的开绕组无刷直流电机(BLDCM)具有运行效率高、电压矢量多样、控制结构简单等优点,适用于工业领域。根据共直流母线开绕组BLDCM控制拓扑搭建了相应的数学模型,对该拓扑下电压矢量的特性进行理论分析及分类,并将电压幅值不为零的电压矢量分为大、中、小三类。分析结果表明:在相同的运行条件下,大矢量作用下转矩变化率最大,小矢量作用下转矩变化率最小,中矢量居于两者之间。仿真结果验证了理论分析的正确性和控制方法的可行性。 展开更多
关键词 无刷直流电机 开绕组 直接转矩控制 两相导通 电压矢量
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基于二维热传导方程的COB-LED散热器热模拟
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作者 王朝瑞 杨平 +1 位作者 韩帅 徐新营 《电子科技》 2024年第3期68-74,共7页
针对COB-LED(Chip on Board-Light Emitting Diode)散热问题,文中基于二维热传导方程建立了一个可快速计算COB-LED散热器表面热分布的数学模型。为了便于模型求解,采用有限差分法求解该数学模型并选择交替方向隐格式作为其差分格式。根... 针对COB-LED(Chip on Board-Light Emitting Diode)散热问题,文中基于二维热传导方程建立了一个可快速计算COB-LED散热器表面热分布的数学模型。为了便于模型求解,采用有限差分法求解该数学模型并选择交替方向隐格式作为其差分格式。根据模型中的边界条件和初始条件设计COB-LED常温点亮实验,并基于ANSYS有限元分析软件进行仿真分析。通过比较求解结果、仿真结果和实验结果验证该数学模型的合理性。结果表明,求解结果与实验结果中最高温度相对误差约23.57%,且两者的温度变化趋势一致。求解结果与仿真结果中最高温度相对误差约34.84%,且温度分布较为接近,证明了该数学模型的合理性与正确性。 展开更多
关键词 热传导方程 有限差分法 交替方向隐格式 数学模型 LED散热器 温度分布 实验验证 仿真分析
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同步整流器中MOSFET的双向导电特性和整流损耗研究 被引量:53
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作者 胡宗波 张波 《中国电机工程学报》 EI CSCD 北大核心 2002年第3期88-93,共6页
该文从理论和实验上研究了MOSFET的双向导电特性 ,得出了完整的双向漏源电压电流特性曲线 ,为MOSFET在同步整流中的实际应用奠定了理论基础。同步整流效率取决于MOSFET整流损耗 ,为此 ,该文基于MOSFET的等效损耗模型 ,深入研究了MOSFET... 该文从理论和实验上研究了MOSFET的双向导电特性 ,得出了完整的双向漏源电压电流特性曲线 ,为MOSFET在同步整流中的实际应用奠定了理论基础。同步整流效率取决于MOSFET整流损耗 ,为此 ,该文基于MOSFET的等效损耗模型 ,深入研究了MOSFET整流损耗与其参数、栅极驱动电压和开关工作频率的相互关系 ,得到MOSFET同步整流效率曲线。此外 ,文中还对输出大电流时MOSFET整流损耗和肖特基二极管整流损耗进行了比较 ,提出了大电流运行时多管MOSFET并联整流方式。该文的工作对同步整流器中开关频率、栅极驱动电压、单管或多管并联运行方式的选择具有实际指导意义。 展开更多
关键词 同步整流器 MOSFET 双向导电特性 整流损耗
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离子色谱直接电导法检测糖蜜中的甜菜碱 被引量:7
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作者 张晨光 潘见 +1 位作者 黄文平 杨毅 《食品科学》 EI CAS CSCD 北大核心 2012年第2期208-210,共3页
建立甜菜碱的离子色谱直接电导测定法,用于糖蜜中提取甜菜碱的生产工艺。采用WY阳离子交换柱(150mm×4.6mm),柱温30℃,2.0mmol/L甲烷磺酸溶液为流动相,流速1.0mL/min,电导检测池。结果表明,甜菜碱在0.5~50mg/L质量浓度范围内线性... 建立甜菜碱的离子色谱直接电导测定法,用于糖蜜中提取甜菜碱的生产工艺。采用WY阳离子交换柱(150mm×4.6mm),柱温30℃,2.0mmol/L甲烷磺酸溶液为流动相,流速1.0mL/min,电导检测池。结果表明,甜菜碱在0.5~50mg/L质量浓度范围内线性关系良好(r=0.9995),加标回收率在93.5%~99.7%之间,检测限为0.15mg/L。所建方法适用于糖蜜中提取甜菜碱生产工艺中质量控制。 展开更多
关键词 离子色谱 直接电导 糖蜜 甜菜碱
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多模式控温在航天光学遥感器上的应用 被引量:8
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作者 王阳 孟庆亮 郭楠 《航天返回与遥感》 CSCD 2020年第3期79-85,共7页
针对空间高分辨率光学遥感器面临的控温精度不断提高,而功耗资源日益紧缺的突出问题,文章提出了间接辐射控温技术与直接传导控温技术相结合的多模式控温方式,通过热仿真分析,对其控温效果进行研究,并分别与间接辐射控温技术和直接传导... 针对空间高分辨率光学遥感器面临的控温精度不断提高,而功耗资源日益紧缺的突出问题,文章提出了间接辐射控温技术与直接传导控温技术相结合的多模式控温方式,通过热仿真分析,对其控温效果进行研究,并分别与间接辐射控温技术和直接传导控温技术进行了对比。结果表明,采用多模式控温方式,合理设置间接辐射控温辅助结构的控温功率和阈值,并对直接加载于控温对象的主动控温功耗进行优化配置,可以在保证高精度控温效果的同时有效降低热控功耗需求。 展开更多
关键词 间接辐射控温 直接传导控温 热仿真 控温精度 空间相机
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单掺Rb^+和Cs^+的KTP晶体生长及其电导率(英文) 被引量:2
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作者 常新安 臧和贵 +2 位作者 陈学安 肖卫强 张书峰 《人工晶体学报》 EI CAS CSCD 北大核心 2007年第5期1052-1055,共4页
采用高温溶液降温法在掺质浓度均为5mol%的KTP-K6溶液中分别生长了单掺Rb+和Cs+的KTP晶体,发现掺质改变了晶体生长习性,在相应生长体系中掺质Rb+和Cs+的分配系数分别为0.646和0.08,掺质KTP晶体的晶胞参数a0和b0比纯KTP晶体者略有增长。... 采用高温溶液降温法在掺质浓度均为5mol%的KTP-K6溶液中分别生长了单掺Rb+和Cs+的KTP晶体,发现掺质改变了晶体生长习性,在相应生长体系中掺质Rb+和Cs+的分配系数分别为0.646和0.08,掺质KTP晶体的晶胞参数a0和b0比纯KTP晶体者略有增长。通过掺Rb+或Cs+,KTP晶体的c向电导率明显降低,但晶体在350~1100nm范围内的光透过性质未受影响。 展开更多
关键词 掺质KTP晶体 生长习性 分配系数 透过 c向电导率
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离子色谱-直接电导法同时测定常见氨基酸和无机阳离子 被引量:2
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作者 焦扬 杨鹏波 +1 位作者 李春 丛威 《过程工程学报》 CAS CSCD 北大核心 2009年第6期1153-1158,共6页
采用阳离子交换色谱-直接电导法测定部分常见氨基酸和无机阳离子,以酒石酸和吡啶二羧酸溶液为淋洗液,利用阳离子色谱系统等度洗脱,通过对色谱分析条件的优化,无需衍生化即可同时测定谷氨酸、丙氨酸、甲硫氨酸、亮氨酸、苯丙氨酸、赖氨酸... 采用阳离子交换色谱-直接电导法测定部分常见氨基酸和无机阳离子,以酒石酸和吡啶二羧酸溶液为淋洗液,利用阳离子色谱系统等度洗脱,通过对色谱分析条件的优化,无需衍生化即可同时测定谷氨酸、丙氨酸、甲硫氨酸、亮氨酸、苯丙氨酸、赖氨酸及Na+,NH4+,K+,Ca2+和Mg2+.选择12min内出峰的5种氨基酸和3种无机阳离子进行定量分析,结果表明,其相对标准偏差RSDn=5≤4.690%,标准曲线的线性相关系数不低于0.9984,检出限在0.27~10.34mg/L之间.以建立的方法测定味精等电母液中的氨基酸,结果显示,氨基酸的回收率为88.7%~107.2%. 展开更多
关键词 离子色谱 直接电导检测器 氨基酸 无机阳离子
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