In order to improve the properties of corundum based dispersive purging plugs,dispersive purging plug specimens were prepared using tabular corundum(1-0.15 and≤0.15 mm)as the aggregates,tabular corundum(≤0.044 mm)an...In order to improve the properties of corundum based dispersive purging plugs,dispersive purging plug specimens were prepared using tabular corundum(1-0.15 and≤0.15 mm)as the aggregates,tabular corundum(≤0.044 mm)andα-Al_(2)O_(3)micropowder(d_(50)=0.6μm)as the matrix,Secar 71 cement as the binder,introducing different amounts of nano-CaCO_(3),casting into shapes,and firing at different temperatures(1200 or 1600℃)for 4 h.The effects of the nano-CaCO_(3) extra-addition(0,0.5%,1.0%,1.5%and 2.0%,by mass)on the consistency of the castables as well as the properties and microstructure of the dispersive purging plug specimens were studied.The results show that:(1)with the fixed water addition,the consistency of the corundum castables decreases as the nano-CaCO_(3)addition increases;(2)with the increasing nano-CaCO_(3)addition,the bulk density of the specimens fired at different temperatures for 4 h decreases,the apparent porosity,the cold strength and the hot modulus of rupture all increase,the gas permeability does not change significantly;(3)the specimens fired at 1600℃ for 4 h have obviously better cold comprehensive performance than those fired at 1200℃for 4 h;(4)when the nano-CaCO_(3)addition is 1.5%,the comprehensive performance of the specimen is the optimal.展开更多
文摘In order to improve the properties of corundum based dispersive purging plugs,dispersive purging plug specimens were prepared using tabular corundum(1-0.15 and≤0.15 mm)as the aggregates,tabular corundum(≤0.044 mm)andα-Al_(2)O_(3)micropowder(d_(50)=0.6μm)as the matrix,Secar 71 cement as the binder,introducing different amounts of nano-CaCO_(3),casting into shapes,and firing at different temperatures(1200 or 1600℃)for 4 h.The effects of the nano-CaCO_(3) extra-addition(0,0.5%,1.0%,1.5%and 2.0%,by mass)on the consistency of the castables as well as the properties and microstructure of the dispersive purging plug specimens were studied.The results show that:(1)with the fixed water addition,the consistency of the corundum castables decreases as the nano-CaCO_(3)addition increases;(2)with the increasing nano-CaCO_(3)addition,the bulk density of the specimens fired at different temperatures for 4 h decreases,the apparent porosity,the cold strength and the hot modulus of rupture all increase,the gas permeability does not change significantly;(3)the specimens fired at 1600℃ for 4 h have obviously better cold comprehensive performance than those fired at 1200℃for 4 h;(4)when the nano-CaCO_(3)addition is 1.5%,the comprehensive performance of the specimen is the optimal.
