Preparation of Large Area Double Sided YBCO Thin Films by DC Magneton Sputtering

Tc, Jc and Rs properties of large area double sided YBCO thin films deposited on LaAlO3 substrates by direct current sputtering were reported.Film thickness of the obtained thin films is over 300 nm, Tc > 90 K; Rs can be as low as less than 1.0 mΩ(77 K, 10 GHz).Homogenousity of the properties around the plane was studied.Under the measnous distributions.Influences of substrate temperature and Ar and O2 pressures on properties of the double-sided thin films were discussed.

Preparation and Characterization of CeO_2-TiO_2/SnO_2:Sb Films Deposited on Glass Substrates by R.F.Sputtering

CeO2-TiO2 films and CeO2-TiO/SnO2：Sb （6 mol%） double films were deposited on glass substrates by radio-frequency magnetron sputtering （R.F. Sputtering）, using SnO2：Sb（6 mol%） target, and CeO2- TiO2 targets with different molar ratio of CeO2 to TiO2 （CeO2：TiO2-0：1.0; 0.1：0.9; 0.2：0.8; 0.3：0.7; 0.4：0.6; 0.5：0.5; 0.6：0.4; 0.7：0.3; 0.8：0.2; 0.9：0.1; 1.0：0）. The films are characterized by UV-visible transmission and infrared reflection spectra, scanning electron microscopy （SEM）, Raman spectroscopy, X-ray photoelectron spectroscopy （XPS） and X-ray diffraction （XRD）, respectively. The obtained results show that the amorphous phases composed of CeO2-TiO2 play an important role in absorbing UV, there are Ce^3-, Ce^4- and Ti^4- on the surface of the films; the glass substrates coated with CeO2-TiO2 （Ce/Ti=0.5：0.5; 0.6：0.4）/SnO2：Sb（6 mol%） double films show high absorbing UV（〉99）, high visible light transmission （75%） and good infrared reflection （〉70%）. The sheet resistance of the films is 30-50 Ω/□. The glass substrates coated with the double functional films can be used as window glass of buildings, automobile and so on.

Double oxide film defects in Ni-based super-alloy castings

A new class of defects has been recently discovered, which are regarded as double oxide film defects. In this study, a number of Ni-based vacuum-cast test bars were investigated. The fractures in the broken test bars were observed by Scanning Electron Microscopy （SEM）. Energy Dispersive Spectroscopy （EDS）, as well as Wavelength Dispersive Spectroscopy （WDS） were used to characterize the chemical elements of the fracture＇s surface. Observation by SEM revealed the presence of inclusions identified as films that appeared to have initiated the growth of carbides. This study has added to the evidence that oxide film defects do exist in Ni-based super-alloy in certain vacuum casting conditions. It provides a reference for researchers＇ further study on the defects, and provides a possible direction for researchers to improve casting technology so as to remove these defects.

Root distribution and influencing factors of dry-sowing and wet-growing cotton plants under different water conditions

To study the effect of soil water and salt environment factors on the root growth of cotton under different moisture control,three different emergence water volumes(60,105,and 150 m^(3)/hm^(2)),two different frequencies(high frequency and low frequency)and one double film cover winter irrigation control treatment(CK:2250 m^(3)/hm^(2))were set up to analyze the spatial distribution patterns of soil water and salt environment and root density in dry sown and wet emerged cotton fields under diffe-rent moisture control conditions.The results show that the soil water content and water infiltration range gradually become larger with the increase of seedling water quantity,and the larger the seedling water quantity,the higher the soil water content.With the same seedling water quantity,the soil water content of the high-frequency(HF)treatment becomes obviously larger.The soil conductivity of each treatment tends to decrease gradually with the increase of seedling water and drip frequency,among which the distribution of soil conductivity of S6 treatment is closest to that of CK.With the increase in soil depth,the soil conductivity tends to increase first and then decrease.Compared with the low-frequency(LF)treatment,the high-frequency treatment shows a significantly deeper soil salt accumulation layer.The root length density(RLD)of cotton gradually increases with the amount of seedling water and the frequency of dripping.The soil layer of root distribution gradually deepens with the amount of seedling water in the vertical direction,and the RLD value in the horizontal direction is significantly greater in the mulched area than that in the bare area between films.This research can serve as a solid scientific foundation for the use of dry sowing and wet emergence techniques in cotton fields in southern Xinjiang.

Ultraviolet-shielding and conductive double functional films coated on glass substrates by sol-gel process

Ultraviolet-shielding and conductive double functional films were composed of CeO2-TiO2 film and SnO2:Sb film deposited on glass substrates using sol-gel process.Ce(NO3)3·6H2O and Ti(C4H9O4),SnCl4 and SbCl3 were used as precursors of the two different functional films respectively.The CeO2-TiO2 films were deposited on glass substrates by sol-gel dip coating method,and then the SnO2:Sb films with different thickness were deposited on the pre-coated CeO2-TiO2 thin film glass substrates,finally,the substrates coated with double functional films were annealed at different temperatures.The optical and electrical properties of the CeO2-TiO2 films and the double films were measured by UV-Vis spectrometer and four probe resistance measuring instrument.The crystal structures and surface morphology of the films were characterized using XRD and optical microscope,respectively.The obtained results show that the ultraviolet-shielding rate of the glass substrates with CeO2-TiO2 films is not less than 90%,and transmittance in visible lights can reach 65%.With the thickness of the SnO2:Sb film increasing,its conductivity became better,and the surface resistance is about 260 Ω/ when the SnO2:Sb films were deposited 11 cycles of the dip on the pre-coated CeO2-TiO2 glass.The ultraviolet-shielding rate of the glass substrates with double functional films is higher than 97%,and the peak transmittance in the visible lights is 72%.Additionally,with increasing the heat treatment time,the Na+ of the glass substrates diffuses into the films,resulting in the particle size of SnO2 crystal smaller.

Morphology,structure and corrosion resistance of Mg-Al LDH films fabricated in different Al^(3+)concentration solutions

In situ-grown Mg-Al layered double hydroxide(LDH)films were obtained on an anodized AZ31 substrate,with the immersion of sample in different concentrations of Al^(3+)solution.The structure,composition and morphology of LDH films were investigated by X-ray diffraction(XRD),Fourier transform infrared(FTIR)and scanning electronic microscopy(SEM),and the corrosion behavior of LDH films was further studied by electrochemical impedance spectroscopy(EIS).The influence of Al^(3+)concentration on the growth behavior of LDH was also discussed.The results indicated that the nest-like structure of MgAl-LDH film was composed of interconnected MgAl-LDH nanosheets.Besides,the LDH obtained in0.032 mol·L^(-1)Al^(3+)solution,possessing dense laminated structure,could effectively seal the porous surface of anodic oxide film.EIS results revealed that the samples coated with LDH films showed a higher electrochemical impedance,and thus,the corrosion resistance of samples coated with LDH films was signally improved compared with the anodized alloy.

Role of Double Oxide Film Defects in the Formation of Gas Porosity in Commercial Purity and Sr-containing Al Alloys

The role of double oxide film （bifilm） defects in the formation of gas porosity in commercial purity and Srcontaining AI alloys was investigated by means of a reduced pressure test （RPT） technique. The liquid metal was poured from a height into a crucible to introduce oxide defects into the melt. The melt was then subjected to different ＂hydrogen addition＂ and ＂holding in liquid state＂ regimes before RPT samples were taken. The RPT samples were then characterized by determining their porosity parameters and examining the internal surfaces of the pores formed in them by scanning electron microscopy. The results indicated oxide defects as the initiation sites for the growth of gas porosity, both in commercial purity and Sr-containing AI alloys. The results also rejected reduction of the surface tension of the melt, increase in the volumetric shrinkage and reduction in interdendritic feeding as the possible causes of an increase in the porosity content of the AI castings modified with strontium. The change in the composition of the oxide layers of double oxide film defects was suggested to be responsible for this behaviour.

Mechanism analysis and performance improvement of mechanized ridge forming of whole plastic film mulched double ridges

In order to achieve high-performance and mechanization construction standard of whole plastic mulched double ridge seedbed,and to meet its forming process and corresponding agronomic requirements of the mechanized double ridge seedbed,the key working parameters such as the speed of rotary blade group,the thickness of upturned sod and the power consumption of rotary blade group under different parameters were analyzed based on related working performance in ridge forming.Also,the test factors and their range of values were finally determined in this study.Discrete element method(DEM)simulation was applied in the numerical simulation of the mechanized ridge forming process of whole plastic mulched double ridges,and the ridge forming effect and digging resistance variation characteristics of different types of shovels were compared.Taking the forward speed of the combined machine,the penetration angle of the arc-shaped shovel and the depth of rotary tillage as independent variables,and the qualified rate of seedbed tillage as the response value,the mathematical model between the test factors and the qualified rate of the seedbed tillage was established,to explore the influence sequence of the factors on the qualified rate of seedbed tillage,and obtained the following optimal working parameters of the ridge forming device:the advancing velocity of the combined machine of 0.50 m/s,penetration angle of the arc-shaped shovel of 31°,rotary tillage depth of 140 mm,and average qualified rate 95.20%of seedbed tillage in corresponding simulation verification test.Field test showed that the average qualified rate of seedbed tillage in ridge forming device was 93.60%,which was close to that of the simulation results.The actual working condition of the sample machine was basically in line with the simulation process and could relatively precisely reflect the mechanized ridge forming mechanism of whole plastic double ridges.The results showed that the established DEM model and its parameter setting were relatively accurate and reasonable.

Effect of Double Oxide Film Defects on Mechanical Properties of As-Cast C95800 Alloy

The morphology of double oxide film defects and their influence on the tensile mechanical properties of a commercial Cu-Al （C95800） alloy were investigated in this study. Plane castings were produced with two types of pouting systems, and their tensile properties were measured and then analyzed by means of Weibull statistics method. The fracture surfaces of the tensile specimens were examined using scanning electron microscopy equipped with energy-dispersive spectroscopy. A large amount of double oxide film defects were observed on the tensile fractured specimens of the topfilled plane castings, and their chemical composition is identified to be Al2O3. Weibull statistics analyses showed that the double oxide film defects significantly reduce mechanical properties of the castings investigated. Furthermore, the ultimate tensile strength is more obviously deteriorated by double oxide film defects than elongation.

Langmuir Aggregation of Thionin in Nucleic Acids and Its Application

The microsurface adsorption-spectral correction (MSASC) technique has been described. The formation of the double electrostatic films in nucleic acids causes the monolayer aggregation of stain molecules. The interaction of thionin (TN) with nucleic acids, ctD-NA, sDNA and yRNA, has been investigated at pH 7.8. Results show that the binding ratios of TN to ctDNA-P, sDNA-P and yR-NA-P are 1.27, 1.30 and 1.40, respectively, the binding constants of the aggregates are 2.8 · 104, 9.10 · 104 and 6.49 · 103 and their molar absorptivities are 1.04 · 104, 1.25 · 104 and · 104 L· mol?1, cm?1 at 630 nm. The aggregation may be applied to the spectrophotometric detection of nucleic acids samples.