The application of electric current pulse(ECP) to a solidification process refers to the immersion of electrodes into the liquid metal and the employment of thermal insulators on the upper surface of metal.In order ...The application of electric current pulse(ECP) to a solidification process refers to the immersion of electrodes into the liquid metal and the employment of thermal insulators on the upper surface of metal.In order to ascertain the effects of these two factors on the structure refinement by the ECP technique,three groups of experiments were performed with different types of electrodes or various thermal insulators.By the comparison between solidification structures under different conditions,it is followed that the electrode and the thermal insulator have an obvious influence on the grain refinement under an applied ECP,and further analysis demonstrates that the thermal conditions of the liquid surface play a vital role in the modification of solidification structure.Also,the results support the viewpoint that most of the equiaxed grains originate from the liquid surface subjected to an ECP.展开更多
A mathematical model considering free nuclei was developed to reveal the migration behavior of the free nuclei. Numerical simulation results show that most of the nuclei on the top surface of the melt move downwards a...A mathematical model considering free nuclei was developed to reveal the migration behavior of the free nuclei. Numerical simulation results show that most of the nuclei on the top surface of the melt move downwards and distribute randomly inside the Al melt, which induces more nucleation sites resulting in grain refinement. At the same time, the effect of nuclei size on the nuclei distribution and refinement employing electric current pulse (ECP) was also investigated. The smaller nuclei migrate a short distance with the Al melt at lower speed. But for the larger nuclei, the migration downwards with higher speed benefits the refinement of interior grains of the melt. The research results help to better understand the refinement process and provide a more reasonable explanation of the grain refinement mechanism using ECP.展开更多
Three kinds of AI-Si piston alloys were prepared and subjected to pulse electric current treatment (PECT) at different pouring temperatures. Some aspects of the solidification microstructures were examined including...Three kinds of AI-Si piston alloys were prepared and subjected to pulse electric current treatment (PECT) at different pouring temperatures. Some aspects of the solidification microstructures were examined including the morphology and the distribution of the matrix and the secondary phases by using of optical microscopy (OM), SEM and EDS methods. Results indicate that PECT can refine the grains of α-AI in the alloys as effectively as chemical modification by sodium salt. The processing parameters of PECT on the multi-component AI-Si alloys were then optimized through the testing of tensile strength, elongation and microhardness of the prepared alloys. A new theory was put forward to explain the mechanism of PECT.展开更多
Microstructure of reaction sintering of ZnAl2O4 at 1500℃ by hot-pressing(HP) and pulse electric current was investigated. The results indicated that the existed cracks in sintered body were caused by structure mismat...Microstructure of reaction sintering of ZnAl2O4 at 1500℃ by hot-pressing(HP) and pulse electric current was investigated. The results indicated that the existed cracks in sintered body were caused by structure mismatch. It is the evidence that periodical temperature field existed during pulse electric current sintering of nonconductive materials. The distance between high temperature areas was related to die diameter.展开更多
The superplastic deformation of aluminium alloy 7475 applied electric current pulse has been studied.The results presented that applying a high density current pulse raises both the elongation rate and the m value,and...The superplastic deformation of aluminium alloy 7475 applied electric current pulse has been studied.The results presented that applying a high density current pulse raises both the elongation rate and the m value,and makes supperior superplastic properties at high strain rate of 10^(-2)s^(-1),the optimum deformation temperature could move from 530℃to 480~510℃,TEM observation showed the superplastic deformation of the alloy is the results of grain boundary slips and dislocation slips in grains under function of the electron wind;the intergranular tear is a main behavior of fracture of the alloy.展开更多
Effects of the melt pulse electric current and thermal treatment on solidification structures of A356 alloy were investigated. In the experiments, the low temperature melt(953 K and 903 K) treated by pulse electric cu...Effects of the melt pulse electric current and thermal treatment on solidification structures of A356 alloy were investigated. In the experiments, the low temperature melt(953 K and 903 K) treated by pulse electric current was mixed with high temperature melt(1 223 K). By the control experiments, the results show that the solidification structure of A356 alloy is refined apparently by the pulse electric current together with melt thermal treatment process, and the mechanical properties, especially the elongation ratio of the specimen treated is improved greatly. The structure change of the melt by pulse electric current and melt thermal treatment is the main reason for the refinement of the solidification structure of A356 alloy.展开更多
The sintering resistance for conductive TiB2 and non-conductive A12O3 as well as empty die during pulse current sintering were investigated in this paper. Equivalent resistances were measured by current and valtage du...The sintering resistance for conductive TiB2 and non-conductive A12O3 as well as empty die during pulse current sintering were investigated in this paper. Equivalent resistances were measured by current and valtage during sintering the conductive and non-conductive materials in the same conditions. It is found that the current paths for conductive are different from those for non-conductive materials. For non-conductive materials, sintering resistances are influenced by powder sizes and heating rates, which indicates that pulse current has some interaction with non-conductive powders. For conductive TiB2 , sintering resistances are influenced by heating rates and ball-milling time, which indicates the effect of powders activated by spark.展开更多
Gain refinement in metal alloy can be achieved by applying an electric current pulse(ECP)in solidification process.Forced flow inside the melt has been proved to be a key role in grain refinement.In this paper,the flu...Gain refinement in metal alloy can be achieved by applying an electric current pulse(ECP)in solidification process.Forced flow inside the melt has been proved to be a key role in grain refinement.In this paper,the fluid flow inside Ga 20 wt%-In 12 wt%-Sn alloy induced by a damping sinusoidal ECP flowing through two parallel electrodes into the cylindrical melt was investigated by both experimental measurements and numerical simulations.Experimental results showed that a strong descending jet was induced beneath the bottom of electrodes under the application of ECP.Besides,it was found that flow intensity increases with the increase of amplitude,frequency,and pulse width,respectively.In order to unlock the formation mechanism of flow pattern and the relevance of flow intensity varied with electrical parameters,a three-dimensional numerical model under the application of ECP was established.Meanwhile,a comparative study was conducted by numerical simulations to reveal the distributions of electromagnetic fields and forced flow.Numerical results showed that the downward Lorentz force induced by ECP was concentrated beneath the bottom of electrodes.This downward Lorentz force induces a descending jet and provokes a global forced flow.According to numerical simulations,the evolution of flow intensity with electrical parameters under the application of ECP can be understood by the time averaged impulse of Lorentz force.展开更多
The effect of high density pulse electric current (HDPEC) on the solidification structure of the low temperature melt(LTM) of commercial A356 alloy was investigated. In the experiments, the HDPEC was discharged in the...The effect of high density pulse electric current (HDPEC) on the solidification structure of the low temperature melt(LTM) of commercial A356 alloy was investigated. In the experiments, the HDPEC was discharged in the LTM (953?K, 903?K and 873?K). By the control experiments, the results showed that the solidification structure of the LTM of A356 alloy is refined apparently when the HDPEC is discharged in low temperature melt. However, the holding time of melt treated has an adverse effect on the solidification structure. The longer the holding time of the melt treated with HDPEC, the coarser the microstructure. With the same discharge voltage, the lower the temperature of LTM, the more obscure the refinement of solidification structure. Finally, the mechanism of microstructure refining by HDPEC was analyzed.展开更多
The impurity iron in silicon material will seriously affect the photoelectric conversion efficiency of silicon solar cells.However,the traditional silicon purification method has the disadvantages of long cycle,high e...The impurity iron in silicon material will seriously affect the photoelectric conversion efficiency of silicon solar cells.However,the traditional silicon purification method has the disadvantages of long cycle,high energy consumption and serious pollution.In this study,an efficient and green pulsed electric current purification technology is proposed.The electromigration effect of iron elements,the current density gradient driving of iron phase,and the gravity of iron phase all affect the migration behavior of iron phase in silicon melt under pulsed electric current.Regardless of the depth of electrode insertion into the silicon melt,the solubility of iron in silicon decreases under the pulsed electric current,which helps to form the iron phase.At the same time,the iron phase tends to sink toward the bottom under the influence of gravity.When the electrode is shallowly inserted,a non-uniform electric field is formed in the silicon melt,and the iron phase is mainly driven by the current density gradient to accelerate sink toward the bottom.When the electrode is fully inserted,an approximately uniform electric field is formed in the silicon melt,and iron elements are preferentially migrated to the cathode by electromigration,forming iron phase sinking at the cathode.The study of impurity iron migration behavior in silicon melt under pulsed electric current provides a new approach for the purification of polycrystalline silicon.展开更多
Dielectric wall accelerator(DWA), towards high gradient acceleration field(30 MeV/m–100 MeV/m), is under development at Institute of Modern Physics. A prototype was designed and constructed to prove the principle. Th...Dielectric wall accelerator(DWA), towards high gradient acceleration field(30 MeV/m–100 MeV/m), is under development at Institute of Modern Physics. A prototype was designed and constructed to prove the principle. This needs a short pulse high current electron source to match the acceleration field generated by the Blumlein-type pulse forming lines(PFLs). In this paper, we report the design and test of a new type short pulse high current electron gun based on principle of vacuum arc discharge. Electron beams of 100 mA with pulse width of 10 ns were obtained.展开更多
Residual stress in high-carbon steel affects the dimensional accuracy, structural stability, and integrity of components. Although the evolution of residual stress under an electric field has received extensive attent...Residual stress in high-carbon steel affects the dimensional accuracy, structural stability, and integrity of components. Although the evolution of residual stress under an electric field has received extensive attention, its elimination mechanism has not been fully clarified. In this study, it was found that the residual stress of high-carbon steel could be effectively relieved within a few minutes through the application of a low density pulse current. The difference between the current pulse treatment and traditional heat treatment in reducing residual stress is that the electric pulse provides additional Gibbs free energy for the system, which promotes dislocation annihilation and carbon atom diffusion to form carbides, thus reducing the free energy of the system. The electroplastic and thermal effects of the pulse current promoted the movement of dislocations under the electric field, thus eliminating the internal stress caused by dislocation entanglement. The precipitation of carbides reduced the carbon content of the steel matrix and lattice shrinkage, thereby reducing the residual tensile stress. Considering that a pulsed current has the advantages of small size, small power requirement, continuous output, and continuously controllable parameters, it has broad application prospects for eliminating residual stress.展开更多
基金Project(2009AA03Z110) supported by the National High Technology Research and Development Program of ChinaProject (2011CB012902) supported by the National Basic Research Program of China
文摘The application of electric current pulse(ECP) to a solidification process refers to the immersion of electrodes into the liquid metal and the employment of thermal insulators on the upper surface of metal.In order to ascertain the effects of these two factors on the structure refinement by the ECP technique,three groups of experiments were performed with different types of electrodes or various thermal insulators.By the comparison between solidification structures under different conditions,it is followed that the electrode and the thermal insulator have an obvious influence on the grain refinement under an applied ECP,and further analysis demonstrates that the thermal conditions of the liquid surface play a vital role in the modification of solidification structure.Also,the results support the viewpoint that most of the equiaxed grains originate from the liquid surface subjected to an ECP.
基金Project(SELF-2011-01)supported by the Open Project of Shanghai Key Laboratory of Modern Metallurgy and Materials Processing,ChinaProjects(51204109,51035004)supported by the National Natural Science Foundation of China
文摘A mathematical model considering free nuclei was developed to reveal the migration behavior of the free nuclei. Numerical simulation results show that most of the nuclei on the top surface of the melt move downwards and distribute randomly inside the Al melt, which induces more nucleation sites resulting in grain refinement. At the same time, the effect of nuclei size on the nuclei distribution and refinement employing electric current pulse (ECP) was also investigated. The smaller nuclei migrate a short distance with the Al melt at lower speed. But for the larger nuclei, the migration downwards with higher speed benefits the refinement of interior grains of the melt. The research results help to better understand the refinement process and provide a more reasonable explanation of the grain refinement mechanism using ECP.
基金supported by Heilongjiang Provincial Natural Science Foundation(Grant No.E200504)in China and the Harbin Institute of Technology Inter-disciplines Foundation(Grant No.HIT.MD2002.14).
文摘Three kinds of AI-Si piston alloys were prepared and subjected to pulse electric current treatment (PECT) at different pouring temperatures. Some aspects of the solidification microstructures were examined including the morphology and the distribution of the matrix and the secondary phases by using of optical microscopy (OM), SEM and EDS methods. Results indicate that PECT can refine the grains of α-AI in the alloys as effectively as chemical modification by sodium salt. The processing parameters of PECT on the multi-component AI-Si alloys were then optimized through the testing of tensile strength, elongation and microhardness of the prepared alloys. A new theory was put forward to explain the mechanism of PECT.
基金This work was supported by the National Natural Science Foundation of China under grant No.50232020 and 50220160657.
文摘Microstructure of reaction sintering of ZnAl2O4 at 1500℃ by hot-pressing(HP) and pulse electric current was investigated. The results indicated that the existed cracks in sintered body were caused by structure mismatch. It is the evidence that periodical temperature field existed during pulse electric current sintering of nonconductive materials. The distance between high temperature areas was related to die diameter.
基金Supported by the National Natural Science Foundation of China(No 59201010)Hubei Province Natural Science Foundsation。
文摘The superplastic deformation of aluminium alloy 7475 applied electric current pulse has been studied.The results presented that applying a high density current pulse raises both the elongation rate and the m value,and makes supperior superplastic properties at high strain rate of 10^(-2)s^(-1),the optimum deformation temperature could move from 530℃to 480~510℃,TEM observation showed the superplastic deformation of the alloy is the results of grain boundary slips and dislocation slips in grains under function of the electron wind;the intergranular tear is a main behavior of fracture of the alloy.
文摘Effects of the melt pulse electric current and thermal treatment on solidification structures of A356 alloy were investigated. In the experiments, the low temperature melt(953 K and 903 K) treated by pulse electric current was mixed with high temperature melt(1 223 K). By the control experiments, the results show that the solidification structure of A356 alloy is refined apparently by the pulse electric current together with melt thermal treatment process, and the mechanical properties, especially the elongation ratio of the specimen treated is improved greatly. The structure change of the melt by pulse electric current and melt thermal treatment is the main reason for the refinement of the solidification structure of A356 alloy.
基金Supported by the Natural Science Foundation of China (59872024) Key Teacher Fund of National Education Ministry and Fund of State Key Lab of Plastic Forming Simulation and Die and Mould Technology(02 -11)
文摘The sintering resistance for conductive TiB2 and non-conductive A12O3 as well as empty die during pulse current sintering were investigated in this paper. Equivalent resistances were measured by current and valtage during sintering the conductive and non-conductive materials in the same conditions. It is found that the current paths for conductive are different from those for non-conductive materials. For non-conductive materials, sintering resistances are influenced by powder sizes and heating rates, which indicates that pulse current has some interaction with non-conductive powders. For conductive TiB2 , sintering resistances are influenced by heating rates and ball-milling time, which indicates the effect of powders activated by spark.
基金Project supported by the National Natural Science Foundation of China(Grant Nos.U1760204,51974183,52071194,and 52074180).
文摘Gain refinement in metal alloy can be achieved by applying an electric current pulse(ECP)in solidification process.Forced flow inside the melt has been proved to be a key role in grain refinement.In this paper,the fluid flow inside Ga 20 wt%-In 12 wt%-Sn alloy induced by a damping sinusoidal ECP flowing through two parallel electrodes into the cylindrical melt was investigated by both experimental measurements and numerical simulations.Experimental results showed that a strong descending jet was induced beneath the bottom of electrodes under the application of ECP.Besides,it was found that flow intensity increases with the increase of amplitude,frequency,and pulse width,respectively.In order to unlock the formation mechanism of flow pattern and the relevance of flow intensity varied with electrical parameters,a three-dimensional numerical model under the application of ECP was established.Meanwhile,a comparative study was conducted by numerical simulations to reveal the distributions of electromagnetic fields and forced flow.Numerical results showed that the downward Lorentz force induced by ECP was concentrated beneath the bottom of electrodes.This downward Lorentz force induces a descending jet and provokes a global forced flow.According to numerical simulations,the evolution of flow intensity with electrical parameters under the application of ECP can be understood by the time averaged impulse of Lorentz force.
文摘The effect of high density pulse electric current (HDPEC) on the solidification structure of the low temperature melt(LTM) of commercial A356 alloy was investigated. In the experiments, the HDPEC was discharged in the LTM (953?K, 903?K and 873?K). By the control experiments, the results showed that the solidification structure of the LTM of A356 alloy is refined apparently when the HDPEC is discharged in low temperature melt. However, the holding time of melt treated has an adverse effect on the solidification structure. The longer the holding time of the melt treated with HDPEC, the coarser the microstructure. With the same discharge voltage, the lower the temperature of LTM, the more obscure the refinement of solidification structure. Finally, the mechanism of microstructure refining by HDPEC was analyzed.
基金financially supported by the National Natural Science Foundation of China(No.U21B2082)Natural Science Foundation of Beijing Municipality(No.2222065)and Fundamental Research Funds for the Central Universities(No.FRF-TP-22-02C2).
文摘The impurity iron in silicon material will seriously affect the photoelectric conversion efficiency of silicon solar cells.However,the traditional silicon purification method has the disadvantages of long cycle,high energy consumption and serious pollution.In this study,an efficient and green pulsed electric current purification technology is proposed.The electromigration effect of iron elements,the current density gradient driving of iron phase,and the gravity of iron phase all affect the migration behavior of iron phase in silicon melt under pulsed electric current.Regardless of the depth of electrode insertion into the silicon melt,the solubility of iron in silicon decreases under the pulsed electric current,which helps to form the iron phase.At the same time,the iron phase tends to sink toward the bottom under the influence of gravity.When the electrode is shallowly inserted,a non-uniform electric field is formed in the silicon melt,and the iron phase is mainly driven by the current density gradient to accelerate sink toward the bottom.When the electrode is fully inserted,an approximately uniform electric field is formed in the silicon melt,and iron elements are preferentially migrated to the cathode by electromigration,forming iron phase sinking at the cathode.The study of impurity iron migration behavior in silicon melt under pulsed electric current provides a new approach for the purification of polycrystalline silicon.
基金Supported by knowledge innovation project of Chinese academy of sciences(No.Y115280YZD)the National Natural Science Foundation of China(No.11105195 and No.11105197)
文摘Dielectric wall accelerator(DWA), towards high gradient acceleration field(30 MeV/m–100 MeV/m), is under development at Institute of Modern Physics. A prototype was designed and constructed to prove the principle. This needs a short pulse high current electron source to match the acceleration field generated by the Blumlein-type pulse forming lines(PFLs). In this paper, we report the design and test of a new type short pulse high current electron gun based on principle of vacuum arc discharge. Electron beams of 100 mA with pulse width of 10 ns were obtained.
基金The work was financially supported by the Natural Science Foundation of Beijing Municipality(2222065)the National Natural Science Foundation of China(U21B2082)Fundamental Research Funds for the Central Universities(FRF-TP-22-02C2).
文摘Residual stress in high-carbon steel affects the dimensional accuracy, structural stability, and integrity of components. Although the evolution of residual stress under an electric field has received extensive attention, its elimination mechanism has not been fully clarified. In this study, it was found that the residual stress of high-carbon steel could be effectively relieved within a few minutes through the application of a low density pulse current. The difference between the current pulse treatment and traditional heat treatment in reducing residual stress is that the electric pulse provides additional Gibbs free energy for the system, which promotes dislocation annihilation and carbon atom diffusion to form carbides, thus reducing the free energy of the system. The electroplastic and thermal effects of the pulse current promoted the movement of dislocations under the electric field, thus eliminating the internal stress caused by dislocation entanglement. The precipitation of carbides reduced the carbon content of the steel matrix and lattice shrinkage, thereby reducing the residual tensile stress. Considering that a pulsed current has the advantages of small size, small power requirement, continuous output, and continuously controllable parameters, it has broad application prospects for eliminating residual stress.