The surface morphology of buffer layer yttrium-stabilized zirconia （YSZ） of YBa2CuaO7-σ （YBCO） high temperature superconducting films relies on a series of controllable experimental parameters. In this work, we f...The surface morphology of buffer layer yttrium-stabilized zirconia （YSZ） of YBa2CuaO7-σ （YBCO） high temperature superconducting films relies on a series of controllable experimental parameters. In this work, we focus on the influence of pulsed laser frequency and target crystalline type on surface morphology of YSZ films deposited by pulsed laser deposition （PLD） on rolling assisted biaxially textured substrate tapes. Usually two kinds of particles are observed in the YSZ layer： randomly distributed ones on the whole film and self-assembled ones along grain boundaries. SEM images are used to prove that particles can be partly removed when choosing dense targets of single crystalline. Lower frequency of pulsed laser also contributes to a smoother film surface. TEM images are used to view the crystalline structure of thin film. Thus we can obtain a basic understanding of how to prepare a particle-free YSZ buffer layer for YBCO in optimized conditions using PLD. The YBCO layer with nice structure and critical current density of around 5 MA/cm2 can be reached on smooth YSZ samples.展开更多
The yttria-stabilized zirconia(YSZ)film was fabricated on the La 0.8 Sr 0.2 MnO 3(LSM)substrate by electrochemical deposition.The effects of electrochemical deposition conditions on morphological structure of Y(OH) 3 ...The yttria-stabilized zirconia(YSZ)film was fabricated on the La 0.8 Sr 0.2 MnO 3(LSM)substrate by electrochemical deposition.The effects of electrochemical deposition conditions on morphological structure of Y(OH) 3 -Zr(OH) 4 film were studied.The optimal conditions for depositing homogeneous and compact hydroxide film were obtained.The experimental results show that the density of the electrophoretic deposition film is increased remarkably if electrochemical deposition is applied to fill in the pores.展开更多
基金Supported by the ITER Project of the Ministry of Science and Technology of China under Grant No 2011GB113004the Shanghai Commission of Science and Technology under Grant No 11DZ1100402the Youth Fund of the National Natural Science Foundation of China under Grant No 11204174
文摘The surface morphology of buffer layer yttrium-stabilized zirconia （YSZ） of YBa2CuaO7-σ （YBCO） high temperature superconducting films relies on a series of controllable experimental parameters. In this work, we focus on the influence of pulsed laser frequency and target crystalline type on surface morphology of YSZ films deposited by pulsed laser deposition （PLD） on rolling assisted biaxially textured substrate tapes. Usually two kinds of particles are observed in the YSZ layer： randomly distributed ones on the whole film and self-assembled ones along grain boundaries. SEM images are used to prove that particles can be partly removed when choosing dense targets of single crystalline. Lower frequency of pulsed laser also contributes to a smoother film surface. TEM images are used to view the crystalline structure of thin film. Thus we can obtain a basic understanding of how to prepare a particle-free YSZ buffer layer for YBCO in optimized conditions using PLD. The YBCO layer with nice structure and critical current density of around 5 MA/cm2 can be reached on smooth YSZ samples.
文摘The yttria-stabilized zirconia(YSZ)film was fabricated on the La 0.8 Sr 0.2 MnO 3(LSM)substrate by electrochemical deposition.The effects of electrochemical deposition conditions on morphological structure of Y(OH) 3 -Zr(OH) 4 film were studied.The optimal conditions for depositing homogeneous and compact hydroxide film were obtained.The experimental results show that the density of the electrophoretic deposition film is increased remarkably if electrochemical deposition is applied to fill in the pores.
