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Fabrication of fine-grained,high strength and toughness Mg alloy by extrusion−shearing process 被引量:15
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作者 Bo-ning WANG Feng WANG +2 位作者 Zhi WANG Zheng LIU Ping-li MAO 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2021年第3期666-678,共13页
A novel extrusion-shearing(ES) composite process was designed to fabricate fine-grained, high strength and tough magnesium alloy. The structural parameters of an ES die were optimized by conducting an orthogonal simul... A novel extrusion-shearing(ES) composite process was designed to fabricate fine-grained, high strength and tough magnesium alloy. The structural parameters of an ES die were optimized by conducting an orthogonal simulation experiment using finite element software Deform-3D, and Mg-3 Zn-0.6 Ca-0.6 Zr(ZXK310) alloy was processed using the ES die. The results show that the optimized structural parameters of ES die are extrusion angle(α) of 90°, extrusion section height(h) of 15 mm and inner fillet radius(r) of 10 mm. After ES at an extrusion temperature and a die temperature of 350 °C, ZXK310 alloy exhibited good ES forming ability, and obvious dynamic recrystallization occurred in the forming area. The grain size decreased from 1.42 μm of extrusion area to 0.85 μm of the forming area. Owing to the pinning of second phase and formation of ultrafine grains, the tensile strength, yield strength and elongation of alloy reached 362 MPa, 289 MPa and 21.7%, respectively. 展开更多
关键词 Mg−Zn−Ca−Zr alloy extrusion−shearing process die design dynamic recrystallization mechanical properties
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Anisotropic time-dependent behaviors of shale under direct shearing and associated empirical creep models 被引量:2
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作者 Yachen Xie Michael Z.Hou +1 位作者 Hejuan Liu Cunbao Li 《Journal of Rock Mechanics and Geotechnical Engineering》 SCIE CSCD 2024年第4期1262-1279,共18页
Understanding the anisotropic creep behaviors of shale under direct shearing is a challenging issue.In this context,we conducted shear-creep and steady-creep tests on shale with five bedding orientations (i.e.0°,... Understanding the anisotropic creep behaviors of shale under direct shearing is a challenging issue.In this context,we conducted shear-creep and steady-creep tests on shale with five bedding orientations (i.e.0°,30°,45°,60°,and 90°),under multiple levels of direct shearing for the first time.The results show that the anisotropic creep of shale exhibits a significant stress-dependent behavior.Under a low shear stress,the creep compliance of shale increases linearly with the logarithm of time at all bedding orientations,and the increase depends on the bedding orientation and creep time.Under high shear stress conditions,the creep compliance of shale is minimal when the bedding orientation is 0°,and the steady-creep rate of shale increases significantly with increasing bedding orientations of 30°,45°,60°,and 90°.The stress-strain values corresponding to the inception of the accelerated creep stage show an increasing and then decreasing trend with the bedding orientation.A semilogarithmic model that could reflect the stress dependence of the steady-creep rate while considering the hardening and damage process is proposed.The model minimizes the deviation of the calculated steady-state creep rate from the observed value and reveals the behavior of the bedding orientation's influence on the steady-creep rate.The applicability of the five classical empirical creep models is quantitatively evaluated.It shows that the logarithmic model can well explain the experimental creep strain and creep rate,and it can accurately predict long-term shear creep deformation.Based on an improved logarithmic model,the variations in creep parameters with shear stress and bedding orientations are discussed.With abovementioned findings,a mathematical method for constructing an anisotropic shear creep model of shale is proposed,which can characterize the nonlinear dependence of the anisotropic shear creep behavior of shale on the bedding orientation. 展开更多
关键词 Rock anisotropy Direct shear creep Creep compliance Steady-creep rate Empirical model Creep constitutive model
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Investigation of high rate mechanical flow followed by ignition for high-energy propellant under dynamic extrusion loading
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作者 Liying Dong Yanqing Wu +1 位作者 Kun Yang Xiao Hou 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2024年第2期336-347,共12页
Investigating the ignition response of nitrate ester plasticized polyether(NEPE) propellant under dynamic extrusion loading is of great significant at least for two cases. Firstly, it helps to understand the mechanism... Investigating the ignition response of nitrate ester plasticized polyether(NEPE) propellant under dynamic extrusion loading is of great significant at least for two cases. Firstly, it helps to understand the mechanism and conditions of unwanted ignition inside charged propellant under accident stimulus.Secondly, evaluates the risk of a shell crevice in a solid rocket motor(SRM) under a falling or overturning scene. In the present study, an innovative visual crevice extrusion experiment is designed using a dropweight apparatus. The dynamic responses of NEPE propellant during extrusion loading, including compaction and compression, rapid shear flow into the crevice, stress concentration, and ignition reaction, have been firstly observed using a high-performance high-speed camera. The ignition reaction is observed in the triangular region of the NEPE propellant sample above the crevice when the drop weight velocity was 1.90 m/s. Based on the user material subroutine interface UMAT provided by finite element software LS-DYNA, a viscoelastic-plastic model and dual ignition criterion related to plastic shear dissipation are developed and applied to the local ignition response analysis under crevice extrusion conditions. The stress concentration occurs in the crevice location of the propellant sample, the shear stress is relatively large, the effective plastic work is relatively large, and the ignition reaction is easy to occur. When the sample thickness decreases from 5 mm to 2.5 mm, the shear stress increases from 22.3 MPa to 28.6 MPa, the critical value of effective plastic work required for ignition is shortened from 1280 μs to 730 μs, and the triangular area is easily triggering an ignition reaction. The propellant sample with a small thickness is more likely to stress concentration, resulting in large shear stress and effective work, triggering an ignition reaction. 展开更多
关键词 NEPE propellant Crevice extrusion shear flow Sample thickness Ignition reaction
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Anisotropic shearing mechanism of Kangding slate:Experimental investigation and numerical analysis 被引量:1
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作者 Ping Liu Quansheng Liu +4 位作者 Penghai Deng Yucong Pan Yiming Lei Chenglei Du Xianqi Xie 《Journal of Rock Mechanics and Geotechnical Engineering》 SCIE CSCD 2024年第5期1487-1504,共18页
The shear mechanical behavior is regarded as an essential factor affecting the stability of the surrounding rocks in underground engineering.The shear strength and failure mechanisms of layered rock are significantly ... The shear mechanical behavior is regarded as an essential factor affecting the stability of the surrounding rocks in underground engineering.The shear strength and failure mechanisms of layered rock are significantly affected by the foliation angles.Direct shear tests were conducted on cubic slate samples with foliation angles of 0°,30°,45°,60°,and 90°.The effect of foliation angles on failure patterns,acoustic emission(AE)characteristics,and shear strength parameters was analyzed.Based on AE characteristics,the slate failure process could be divided into four stages:quiet period,step-like increasing period,dramatic increasing period,and remission period.A new empirical expression of cohesion for layered rock was proposed,which was compared with linear and sinusoidal cohesion expressions based on the results made by this paper and previous experiments.The comparative analysis demonstrated that the new expression has better prediction ability than other expressions.The proposed empirical equation was used for direct shear simulations with the combined finite-discrete element method(FDEM),and it was found to align well with the experimental results.Considering both computational efficiency and accuracy,it was recommended to use a shear rate of 0.01 m/s for FDEM to carry out direct shear simulations.To balance the relationship between the number of elements and the simulation results in the direct shear simulations,the recommended element size is 1 mm. 展开更多
关键词 ANISOTROPY Empirical expression of cohesion foliation angles Combined finite-discrete element method(FDEM) shear rate Element size
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Simple shear extrusion versus equal channel angular pressing:A comparative study on the microstructure and mechanical properties of an Mg alloy 被引量:2
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作者 A.Rezaei R.Mahmudi +1 位作者 C.Cayron R.E.Logé 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2023年第5期1769-1790,共22页
Two severe plastic deformation(SPD)techniques of simple shear extrusion(SSE)and equal channel angular pressing(ECAP)were employed to process an extruded Mg-6Gd-3Y-1.5Ag(wt%)alloy at 553 K for 1,2,4 and 6 passes.The mi... Two severe plastic deformation(SPD)techniques of simple shear extrusion(SSE)and equal channel angular pressing(ECAP)were employed to process an extruded Mg-6Gd-3Y-1.5Ag(wt%)alloy at 553 K for 1,2,4 and 6 passes.The microstructural evolutions were studied by electron back scattered diffraction(EBSD)analysis and transmission electron microscopy(TEM).The initial grain size of 7.5μm in the extruded alloy was reduced to about 1.3μm after 6 SPD passes.Discontinuous dynamic recrystallization was suggested to be operative in both SSE and ECAP,with also a potential contribution of continuous dynamic recrystallization at the early stages of deformation.The difference in the shear strain paths of the two SPD techniques caused different progression rate of dynamic recrystallization(DRX),so that the alloys processed by ECAP exhibited higher fractions of recrystallization and high angle grain boundaries(HAGBs).It was revealed that crystallographic texture was also significantly influenced by the difference in the strain paths of the two SPD methods,where dissimilar basal plane texture components were obtained.The compression tests,performed along extrusion direction(ED),indicated that the compressive yield stress(CYS)and ultimate compressive strength(UCS)of the alloys after both SEE and ECAP augmented continuously by increasing the number of passes.ECAP-processed alloys had lower values of CYS and UCS compared to their counterparts processed by SSE.This difference in the mechanical responses was attributed to the different configurations of basal planes with respect to the loading direction(ED)of each SPD technique. 展开更多
关键词 Mg-Gd-Y alloys Severe plastic deformation Simple shear extrusion Equal channel angular pressing Dynamic recrystallization Mechanical properties
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Extrusion 3D printing of carbon nanotube-assembled carbon aerogel nanocomposites with high electrical conductivity
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作者 Lukai Wang Jing Men +4 位作者 Junzong Feng Yonggang Jiang Liangjun Li Yijie Hu Jian Feng 《Nano Materials Science》 EI CAS CSCD 2024年第3期312-319,共8页
Carbon nanotubes(CNTs)with high aspect ratio and excellent electrical conduction offer huge functional improvements for current carbon aerogels.However,there remains a major challenge for achieving the on-demand shapi... Carbon nanotubes(CNTs)with high aspect ratio and excellent electrical conduction offer huge functional improvements for current carbon aerogels.However,there remains a major challenge for achieving the on-demand shaping of carbon aerogels with tailored micro-nano structural textures and geometric features.Herein,a facile extrusion 3D printing strategy has been proposed for fabricating CNT-assembled carbon(CNT/C)aerogel nanocomposites through the extrusion printing of pseudoplastic carbomer-based inks,in which the stable dispersion of CNT nanofibers has been achieved relying on the high viscosity of carbomer microgels.After extrusion printing,the chemical solidification through polymerizing RF sols enables 3D-printed aerogel nanocomposites to display high shape fidelity in macroscopic geometries.Benefiting from the micro-nano scale assembly of CNT nanofiber networks and carbon nanoparticle networks in composite phases,3D-printed CNT/C aerogels exhibit enhanced mechanical strength(fracture strength,0.79 MPa)and typical porous structure characteristics,including low density(0.220 g cm^(-3)),high surface area(298.4 m^(2)g^(-1)),and concentrated pore diameter distribution(~32.8nm).More importantly,CNT nanofibers provide an efficient electron transport pathway,imparting 3D-printed CNT/C aerogel composites with a high electrical conductivity of 1.49 S cm^(-1).Our work would offer feasible guidelines for the design and fabrication of shape-dominated functional materials by additive manufacturing. 展开更多
关键词 Carbon aerogel extrusion 3D printing Carbon nanotube Electrical conductivity RHEOLOGY
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Modeling of recrystallization behaviour of AA6xxx aluminum alloy during extrusion process
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作者 Marco NEGOZIO Antonio SEGATORI +3 位作者 Riccardo PELACCIA Barbara REGGIANI Sara Di DONATO Lorenzo DONATI 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2024年第10期3170-3184,共15页
An innovative approach was introduced for the development of a AA6063 recrystallization model.This method incorporated a regression-based technique for the determination of material constants and introduced novel equa... An innovative approach was introduced for the development of a AA6063 recrystallization model.This method incorporated a regression-based technique for the determination of material constants and introduced novel equations for assessing the grain size evolution.Calibration and validation of this methodology involved a combination of experimentally acquired microstructural data from the extrusion of three different AA6063 profiles and results from the simulation using the Qform Extrusion UK finite element code.The outcomes proved the agreement between experimental findings and numerical prediction of the microstructural evolution.The trend of the grain size variation based on different process parameters was accurately simulated,both after dynamic and static recrystallization,with an error of less than 25% in almost the whole sampling computations. 展开更多
关键词 recrystallization simulation aluminum alloy extrusion finite element method microstructure prediction
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Interface property of dissimilar Ti-6Al-4V/AA1050 composite laminate made by non-equal channel lateral co-extrusion and heat treatment
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作者 Juan Liao Mengmeng Tian Xin Xue 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2024年第3期197-208,共12页
The purpose of this paper is to examine the effect of processing parameters and subsequent heat treatments on the microstructures and bonding strengths of Ti-6Al-4V/AA1050 laminations formed via a non-equal channel la... The purpose of this paper is to examine the effect of processing parameters and subsequent heat treatments on the microstructures and bonding strengths of Ti-6Al-4V/AA1050 laminations formed via a non-equal channel lateral co-extrusion process.The microstructural evolution and growth mechanism in the diffusion layer were discussed further to optimize the bonding quality by appropriately adjusting process parameters.Scanning electron microscopes(SEM),energy dispersive spectrometer(EDS),and X-ray diffraction(XRD)were used to characterize interfacial diffusion layers.The shear test was used to determine the mechanical properties of the interfacial diffusion layer.The experimental results indicate that it is possible to co-extrusion Ti-6Al-4V/AA1050 compound profiles using non-equal channel lateral co-extrusion.Different heat treatment processes affect the thickness of the diffusion layer.When the temperature and time of heat treatment increase,the thickness of the reaction layers increases dramatically.Additionally,the shear strength of the Ti-6Al-4V/AA1050 composite interface is proportional to the diffusion layer thickness.It is observed that a medium interface thickness results in superior mechanical performance when compared to neither a greater nor a lesser interface thickness.Microstructural characterization of all heat treatments reveals that the only intermetallic compound observed in the diffusion layers is TiAl_(3).Due to the inter-diffusion of Ti and Al atoms,the TiAl_(3) layer grows primarily at AA1050/TiAl_(3) interfaces. 展开更多
关键词 shear strength CO-extrusion Heat treatment Microstructure Intermetallic compounds
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Method of fabricating artificial rock specimens based on extrusion free forming(EFF)3D printing
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作者 Xiaomeng Shi Tingbang Deng +2 位作者 Sen Lin Chunjiang Zou Baoguo Liu 《Journal of Rock Mechanics and Geotechnical Engineering》 SCIE CSCD 2024年第4期1455-1466,共12页
Three-dimensional(3D)printing technology has been widely used to create artificial rock samples in rock mechanics.While 3D printing can create complex fractures,the material still lacks sufficient similarity to natura... Three-dimensional(3D)printing technology has been widely used to create artificial rock samples in rock mechanics.While 3D printing can create complex fractures,the material still lacks sufficient similarity to natural rock.Extrusion free forming(EFF)is a 3D printing technique that uses clay as the printing material and cures the specimens through high-temperature sintering.In this study,we attempted to use the EFF technology to fabricate artificial rock specimens.The results show the physico-mechanical properties of the specimens are significantly affected by the sintering temperature,while the nozzle diameter and layer thickness also have a certain impact.The specimens are primarily composed of SiO_(2),with mineral compositions similar to that of natural rocks.The density,uniaxial compressive strength(UCS),elastic modulus,and tensile strength of the printed specimens fall in the range of 1.65–2.54 g/cm3,16.46–50.49 MPa,2.17–13.35 GPa,and 0.82–17.18 MPa,respectively.It is capable of simulating different types of rocks,especially mudstone,sandstone,limestone,and gneiss.However,the simulation of hard rocks with UCS exceeding 50 MPa still requires validation. 展开更多
关键词 Artificial rock 3D printing extrusion free forming(EFF) Similarity analysis Mechanical properties
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Roughness characterization and shearing dislocation failure for rock-backfill interface
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作者 Meifeng Cai Zhilou Feng +3 位作者 Qifeng Guo Xiong Yin Minghui Ma Xun Xi 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2024年第6期1167-1176,共10页
Shearing dislocation is a common failure type for rock–backfill interfaces because of backfill sedimentation and rock strata movement in backfill mining goaf.This paper designed a test method for rock–backfill shear... Shearing dislocation is a common failure type for rock–backfill interfaces because of backfill sedimentation and rock strata movement in backfill mining goaf.This paper designed a test method for rock–backfill shearing dislocation.Using digital image techno-logy and three-dimensional(3D)laser morphology scanning techniques,a set of 3D models with rough joint surfaces was established.Further,the mechanical behavior of rock–backfill shearing dislocation was investigated using a direct shear test.The effects of interface roughness on the shear–displacement curve and failure characteristics of rock–backfill specimens were considered.The 3D fractal dimen-sion,profile line joint roughness coefficient(JRC),profile line two-dimensional fractal dimension,and the surface curvature of the frac-tures were obtained.The correlation characterization of surface roughness was then analyzed,and the shear strength could be measured and calculated using JRC.The results showed the following:there were three failure threshold value points in rock–backfill shearing dis-location:30%–50%displacement before the peak,70%–90%displacement before the peak,and 100%displacement before the peak to post-peak,which could be a sign for rock–backfill shearing dislocation failure.The surface JRC could be used to judge the rock–backfill shearing dislocation failure,including post-peak sliding,uniform variations,and gradient change,corresponding to rock–backfill disloca-tion failure on the field site.The research reveals the damage mechanism for rock–backfill complexes based on the free joint surface,fills the gap of existing shearing theoretical systems for isomerism complexes,and provides a theoretical basis for the prevention and control of possible disasters in backfill mining. 展开更多
关键词 rock–backfill ROUGHNESS correlation characterization shearing dislocation interface failure
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A statistical damage-based constitutive model for shearing of rock joints in brittle drop mode
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作者 Xinrong Liu Peiyao Li +5 位作者 Xueyan Guo Xinyang Luo Xiaohan Zhou Luli Miao Fuchuan Zhou Hao Wang 《International Journal of Mining Science and Technology》 SCIE EI CAS CSCD 2024年第8期1041-1058,共18页
Some rock joints exhibit significant brittleness,characterized by a sharp decrease in shear stress upon reaching the peak strength.However,existing models often fail to accurately represent this behavior and are encum... Some rock joints exhibit significant brittleness,characterized by a sharp decrease in shear stress upon reaching the peak strength.However,existing models often fail to accurately represent this behavior and are encumbered by numerous parameters lacking clear mechanical significance.This study presents a new statistical damage constitutive model rooted in both damage mechanics and statistics,containing only three model parameters.The proposed model encompasses all stages of joint shearing,including the compaction stage,linear stage,plastic yielding stage,drop stage,strain softening stage,and residual strength stage.To derive the analytical expression of the constitutive model,three boundary conditions are introduced.Experimental data from both natural and artificial rock joints is utilized to validate the model,resulting in average absolute relative errors ranging from 3%to 8%.Moreover,a comparative analysis with established models illustrates that the proposed model captures stress drop and post-peak strain softening more effectively,with model parameters possessing clearer mechanical interpretations.Furthermore,parameter analysis is conducted to investigate the impacts of model parameters on the curves and unveil the relationship between these parameters and the mechanical properties of rock joints.Importantly,the proposed model is straightforward in form,and all model parameters can be obtained from direct shear tests,thus facilitating the utilization in numerical simulations. 展开更多
关键词 Rock joints Brittle rock Direct shear test Damage-based constitutive model Parameters analysis
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Engineering behaviour of in situ cored deep cement mixed marine deposits subjected to undrained and drained shearing
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作者 Wei Li Chung Yee Kwok 《Journal of Rock Mechanics and Geotechnical Engineering》 SCIE CSCD 2024年第5期1749-1760,共12页
The deep cement mixing(DCM)is used to improve the capacity and reduce the settlement of the soft ground by forming cemented clay columns.The investigation on the mechanical behaviour of the DCM samples is limited to e... The deep cement mixing(DCM)is used to improve the capacity and reduce the settlement of the soft ground by forming cemented clay columns.The investigation on the mechanical behaviour of the DCM samples is limited to either laboratory-prepared samples or in-situ samples under unconfined compression.In this study,a series of drained and undrained triaxial shearing tests was performed on the in-situ cored DCM samples with high cement content to assess their mechanical behaviours.It is found that the drainage condition affects significantly the stiffness,peak and residual strengths of the DCM samples,which is mainly due to the state of excess pore water pressure at different strain levels,i.e.being positive before the peak deviatoric stress and negative after the peak deviatoric stress,in the undrained tests.The slope of the failure envelope changes obviously with the confining pressures,being steeper at lower stress levels and flatter at higher stress levels.The strength parameters,effective cohesion and friction angle obtained from lower stress levels(c′0 andφ′0)are 400 kPa and 58°,respectively,which are deemed to be true for design in most DCM applications where the in-situ stress levels are normally at lower values of 50-200 kPa.Additionally,the computed tomography(CT)scanning system was adopted to visualize the internal structures of DCM samples.It is found that the clay pockets existing inside the DCM samples due to uneven mixing affect markedly their stress-strain behaviour,which is one of the main reasons for the high variability of the DCM samples. 展开更多
关键词 Deep cement mixing(DCM) In-situ cored sample Triaxial shearing Drainage condition Confining pressure Computed tomography(CT)
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Designing new low alloyed Mg-RE alloys with high strength and ductility via high-speed extrusion 被引量:6
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作者 Jinshu Xie Zhi Zhang +6 位作者 Shujuan Liu Jinghuai Zhang Jun Wang Yuying He Liwei Lu Yunlei Jiao Ruizhi Wu 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2023年第1期82-91,共10页
Two new low-alloyed Mg-2RE-0.8Mn-0.6Ca-0.5Zn(wt%,RE=Sm or Y)alloys are developed,which can be produced on an in-dustrial scale via relatively high-speed extrusion.These two alloys are not only comparable to commercial... Two new low-alloyed Mg-2RE-0.8Mn-0.6Ca-0.5Zn(wt%,RE=Sm or Y)alloys are developed,which can be produced on an in-dustrial scale via relatively high-speed extrusion.These two alloys are not only comparable to commercial AZ31 alloy in extrudability,but also have superior mechanical properties,especially in terms of yield strength(YS).The excellent extrudability is related to less coarse second-phase particles and high initial melting point of the two as-cast alloys.The high strength-ductility mainly comes from the formation of fine grains,nano-spaced submicron/nano precipitates,and weak texture.Moreover,it is worth noting that the YS of the two alloys can maintain above 160 MPa at elevated temperature of 250°C,significantly higher than that of AZ31 alloy(YS:45 MPa).The Zn/Ca solute segregation at grain boundaries,the improved heat resistance of matrix due to addition of RE,and the high melting points of strengthening particles(Mn,MgZn_(2),and Mg-Zn-RE/Mg-Zn-RE-Ca)are mainly responsible for the excellent high-temperature strength. 展开更多
关键词 magnesium alloys high-speed extrusion high strength high ductility solute segregation
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Role of extrusion rate on the microstructure and tensile properties evolution of ultrahigh-strength low-alloy Mg-1.0Al-1.0Ca-0.4Mn(wt.%)alloy 被引量:6
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作者 X.Q.Liu X.G.Qiao +3 位作者 R.S.Pei Y.Q.Chi L.Yuan M.Y.Zheng 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2023年第2期553-561,共9页
Mg-1.0Al-1.0Ca-0.4Mn(AXM1104, wt.%) low alloy was extruded at 200 ℃ with an extrusion ratio of 25 and different ram speeds from 1.0 to 7.0 mm/s. The influence of extrusion rate on microstructure and mechanical proper... Mg-1.0Al-1.0Ca-0.4Mn(AXM1104, wt.%) low alloy was extruded at 200 ℃ with an extrusion ratio of 25 and different ram speeds from 1.0 to 7.0 mm/s. The influence of extrusion rate on microstructure and mechanical properties of the AXM1104 alloy was systematically studied. With the increasing of extrusion rate, the mean dynamically recrystallized(DRXed) grain size of the low alloy and average particles diameter of precipitate second phases were increased, while the degree of grain boundary segregation and the intensity of the basal fiber texture were decreased. With the rising of extrusion rate from 1.0 to 7.0 mm/s, the tensile yield strength(TYS) of the as-extruded AXM1104 alloy was decreased from 445 MPa to 249 MPa, while the elongation to failure(EL) was increased from 5.0% to 17.6%. The TYS, ultimate tensile strength(UTS) and EL of the AXM1104 alloy extruded at the ram speed of 1.5 mm/s was 412 MPa, 419 MPa and 12.0%, respectively,exhibiting comprehensive tensile mechanical properties with ultra-high strength and excellent plasticity. The ultra-high TYS of 412 MPa was mainly due to the strengthening from ultra-fine DRXed grains with segregation of solute atoms at grain boundaries. The strain hardening rate is increase slightly with increasing extrusion speed, which may be ascribed to the increasing mean DRXed grain size with rising extrusion speed. The higher strain hardening rate contributes to the higher EL of these AXM1104 samples extruded at higher ram speed. 展开更多
关键词 Mg-Al-Ca-Mn alloy Ultrafine grain extrusion rate Grain boundary segregation MICROSTRUCTURE Ultrahigh strength
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Difference in extrusion temperature dependences of microstructure and mechanical properties between extruded AZ61 and AZ91 alloys 被引量:3
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作者 Dong Hee Lee Gyo Myeong Lee Sung Hyuk Park 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2023年第5期1683-1696,共14页
The effects of extrusion temperature on the microstructure and tensile properties of extruded AZ61 and AZ91 alloys are investigated by subjecting them to hot extrusion at 300 and 400℃.Although the average grain size ... The effects of extrusion temperature on the microstructure and tensile properties of extruded AZ61 and AZ91 alloys are investigated by subjecting them to hot extrusion at 300 and 400℃.Although the average grain size of the extruded AZ61 alloy slightly increases from 9.5 to 12.6μm with increasing extrusion temperature,its resultant microstructural variation is insignificant.In contrast,the average grain size of the extruded AZ91 alloy significantly increases from 5.7 to 22.5μm with increasing extrusion temperature,and the type of Mg17Al12 precipitates formed in it changes from fine dynamic precipitates with a spherical shape to coarse static precipitates with a lamellar structure.As the extrusion temperature increases,the tensile yield strength of the extruded AZ61 alloy increases from 183 to 197 MPa while that of the extruded AZ91 alloy decreases from 232 to 224 MPa.The tensile elongations of the extruded AZ61 and AZ91 alloys decrease with increasing extrusion temperature,but the degree of decrease is significant in the latter alloy.These different extrusion temperature dependences of the tensile properties of the extruded AZ61 and AZ91 alloys are discussed in terms of their microstructural characteristics,strengthening mechanisms,and crack initiation sites. 展开更多
关键词 Mg-Al-Zn alloys extrusion temperature PRECIPITATION Strengthening mechanism Tensile properties
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Mechanism of plasticity enhancement of AZ31B magnesium alloy sheet by accumulative alternating back extrusion 被引量:2
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作者 Ye Wang Feng Li +2 位作者 Nan Bian Hua Qiu Du Peng Da Huo 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2023年第5期1791-1801,共11页
Accumulative alternating back extrusion was a potential fine-grain modification method.In this paper,it was an innovative attempt to develop high-performance magnesium alloy sheet by this process.Under the condition o... Accumulative alternating back extrusion was a potential fine-grain modification method.In this paper,it was an innovative attempt to develop high-performance magnesium alloy sheet by this process.Under the condition of 350 K,commercial AZ31 magnesium alloy was made into billet by accumulative alternating back extrusion,and then extruded into fine-grain magnesium alloy sheet.Through a systematic study of its microstructure and mechanical properties,the results showed that the initial state had an important influence on the evolution of the structure during extrusion.After accumulative alternating back extrusion to produce the billet,the grain size of the sheet obtained by extrusion was significantly refined,which was related to the accumulation of deformation and grain refinement during the alternating loading process.Grain refinement caused the proportion of dynamic recrystallization inside the sheet with 2 cycles of accumulative alternating back extrusion to drop to 27%.With the increase of extrusion cycles from 2 to 4,the high density of dislocations led to an increase in the proportion of dynamic recrystallization and finer grains.The texture changed from strong basal texture to weak bimodal texture.The results of uniaxial tensile test show that due to grain refinement and texture change,the yield strength was significantly reduced,and the plasticity was significantly improved.It was verified that accumulative alternating back extrusion was meaningful for subsequent processing,and it also provided scientific guidance for the development of fine-grained magnesium alloy sheet. 展开更多
关键词 Magnesium alloy Alternating back extrusion Microstructure uniformity Bimodal texture Texture weakening Sheet anisotropy
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Variations in dynamic recrystallization behavior and mechanical properties of AZ31 alloy with extrusion temperature 被引量:1
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作者 Jae Won Cha Sung Hyuk Park 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2023年第7期2351-2365,共15页
This study investigates the effects of extrusion temperature on the dynamic recrystallization(DRX)behavior of a Mg-3Al-1Zn-0.3Mn(AZ31,wt%)alloy during hot extrusion and on the microstructural characteristics and mecha... This study investigates the effects of extrusion temperature on the dynamic recrystallization(DRX)behavior of a Mg-3Al-1Zn-0.3Mn(AZ31,wt%)alloy during hot extrusion and on the microstructural characteristics and mechanical properties of materials extruded at 350 and 450℃.An increase in the extrusion temperature causes a decrease in the amount of strain energy accumulated in the material during extrusion,because of promoted activation of pyramidal<c+a>slip and dynamic recovery.This reduced strain energy weakens the DRX behavior during extrusion,which eventually results in a decrease in the area fraction of recrystallized grains of the extruded material.The material extruded at 450℃has coarser grains and a stronger basal fiber texture than that extruded at 350℃.As the extrusion temperature increases from 350 to 450℃,the tensile yield strength(TYS)of the extruded material increases from 191.8 to 201.5 MPa,whereas its compressive yield strength(CYS)decreases from 122.5 to 111.0 MPa;consequently,its tension-compression yield stress ratio(CYS/TYS)decreases from 0.64 to 0.55.The increase in the TYS is attributed mainly to the stronger texture hardening and strain hardening effects of the extruded material,and the decrease in the CYS is attributed to the reduced twinning stress resulting from grain coarsening and texture intensification.The microstructural and textural evolutions of the materials during extrusion and the deformation and hardening mechanisms of the extruded materials are discussed in detail. 展开更多
关键词 Mg-Al-Zn alloy extrusion Dynamic recrystallization Microstructure Yield asymmetry
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Advanced strategies in the application of gelatin-based bioink for extrusion bioprinting 被引量:1
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作者 Jirong Yang Huimin He +3 位作者 Duo Li Qian Zhang Lizhi Xu Changshun Ruan 《Bio-Design and Manufacturing》 SCIE EI CAS CSCD 2023年第5期586-608,共23页
The significance of bioink suitability for the extrusion bioprinting of tissue-like constructs cannot be overemphasized.Gelatin,derived from the hydrolysis of collagen,not only can mimic the extracellular matrix to imm... The significance of bioink suitability for the extrusion bioprinting of tissue-like constructs cannot be overemphasized.Gelatin,derived from the hydrolysis of collagen,not only can mimic the extracellular matrix to immensely support cell function,but also is suitable for extrusion under certain conditions.Thus,gelatin has been recognized as a promising bioink for extrusion bioprinting.However,the development of a gelatin-based bioink with satisfactory printability and bioactivity to fabricate complex tissue-like constructs with the desired physicochemical properties and biofunctions for a specific biomedical application is still in its infancy.Therefore,in this review,we aim to comprehensively summarize the state-of-the-art methods of gelatin-based bioink application for extrusion bioprinting.Wefirstly outline the properties and requirements of gelatin-based bioinks for extrusion bioprinting,highlighting the strategies to overcome their main limitations in terms of printability,structural stability and cell viability.Then,the challenges and prospects are further discussed regarding the development of ideal gelatin-based bioinks for extrusion bioprinting to create complex tissue-like constructs with preferable physicochemical properties and biofunctions. 展开更多
关键词 Gelatin-based bioink extrusion bioprinting Tissue-like construct
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Bimodal grain structure formation and strengthening mechanisms in Mg-Mn-Al-Ca extrusion alloys 被引量:1
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作者 Jianyue Zhang Peng Peng +1 位作者 Qingshan Yang Alan A.Luo 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2023年第12期4407-4419,共13页
The effects of small additions of calcium (0.1%and 0.5%~1) on the dynamic recrystallization behavior and mechanical properties of asextruded Mg-1Mn-0.5Al alloys were investigated.Calcium microalloying led to the forma... The effects of small additions of calcium (0.1%and 0.5%~1) on the dynamic recrystallization behavior and mechanical properties of asextruded Mg-1Mn-0.5Al alloys were investigated.Calcium microalloying led to the formation of Al_(2)Ca in as-cast Mg-1Mn-0.5Al-0.1Ca alloy and both Mg_(2)Ca and Al_(2)Ca phases in Mg-1Mn-0.5Al-0.5Ca alloy.The formed Al_(2)Ca particles were fractured during extrusion process and distributed at grain boundary along extrusion direction (ED).The Mg_(2)Ca phase was dynamically precipitated during extrusion process,hindering dislocation movement and reducing dislocation accumulation in low angle grain boundaries (LAGBs) and hindering the transformation of high density of LAGBs into high angle grain boundaries (HAGBs).Therefore,a bimodal structure composed of fine dynamically recrystallized (DRXed) grains and coarse un DRXed regions was formed in Ca-microalloyed Mg-1Mn-0.5Al alloys.The bimodal structure resulted in effective hetero-deformation-induced (HDI) strengthening.Additionally,the fine grains in DRXed regions and the coarse grains in un DRXed regions and the dynamically precipitated Mg_(2)Ca phase significantly enhanced the tensile yield strength from 224 MPa in Mg-1Mn-0.5Al to335 MPa and 352 MPa in Mg-1Mn-0.5Al-0.1Ca and Mg-1Mn-0.5Al-0.5Ca,respectively.Finally,a yield point phenomenon was observed in as-extruded Mg-1Mn-0.5Al-x Ca alloys,more profound with 0.5%Ca addition,which was due to the formation of (■) extension twins in un DRXed regions. 展开更多
关键词 Magnesium alloys extrusion Dynamic precipitation Dynamic recrystallization Bimodal grain structure Mechanical properties
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EXPERIMENTS AND SIMULATIONS OF A NEW DEVELOPED FORMING TECHNOLOGY-SHEAR-EXTRUSION PROCESS OF COMPONENTS WITH BRANCHES 被引量:6
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作者 H.L. Yang, D.C. Kang, Z.L. Zhang, X.H. Piao and Z.D. Shi (National Die and Mold CAD Engineering Research Center, Shanghai Jiaotong University, Shanghai 200030, China) (School of Materials Sci. & Eng., Harbin Institute of Technology, Harbin 150001, China) 《Acta Metallurgica Sinica(English Letters)》 SCIE EI CAS CSCD 2001年第3期212-218,共7页
Shear-extrusion process and its forming parameters are proposed, whilst its laborsaving characteristic is utilized to forge large-size shutoff valve bodies on the middle-due press. This new process is intended for the... Shear-extrusion process and its forming parameters are proposed, whilst its laborsaving characteristic is utilized to forge large-size shutoff valve bodies on the middle-due press. This new process is intended for the manufacture of large-size forged tubular components with branches on the middle-due press. Experiments are carried out and processing parameters are obtained regarding the shear- extrusion process of a large-size shutoff valve body. Deformation and metal flow in the shear- extrusion process are investigated. In order to verify the laborsaving characteristic of this new process, some contrast experiments of extrusion force are performed between shear-extrusion and upsetting-extrusion for forming tubular components with branches. Based on rigid-plastic FEM, a plane-strain model is established to analyze shear-extrusion process of tubular components with branches. The analysis results by 2-dimensions FEM are comparatively well consistent with experimental results. Both simulated and experimental results show that this new forming process is feasible for forging large-size tubular components with branches on the middle-due press. 展开更多
关键词 Metal extrusion shearing Simulation Tubular steel structures
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