Monitoring the hydrolyzation of aspirin during the dissolution testing for aspirin delayed-release tablets with a fiber-optic dissolution system

The purpose of this study was to investigate the hydrolyzation of aspirin during the process of dissolution testing for aspirin delayed-release tablets. Hydrolysis product of salicylic acid can result in adverse effects and affect the determination of dissolution rate assaying. In this study, the technique of differential spectra was employed, which made it possible to monitor the dissolution testing in situ. The results showed that the hydrolyzation of aspirin made the percentage of salicylic acid exceed the limit of free salicylic acid （4.0）, and the hydrolyzation may affect the quality detection of aspirin delayed-release tablets.

Improving the Interfacial Mechanical Property of Fiber Reinforced Cement with Dielectric Barrier Discharge 1:The Pul - out Test

The effect of dielectric barrier discharge(DBD)on the interfacial mechanical property of polypropylene fiber reinforced cement is investigated with the aid of single fiber pull out test.The result shows that the DBD treatment improved the adhesion between the PP fiber and the surrounding cement matrix considerably without serious aging.Keywords:dielectric barrier discharge,single fiber pull-out test.

Characterization of Oxygen Plasma Modified Polyimide Fibers Interfacial Adhesion Performance by Single Fiber Fragmentation Test

The application of polyimide( PI) fibers in the field of composite materials has been limited because of their smooth surface and chemical inertness. In order to overcome these problems,oxygen plasma was used to modify the surface of fibers. The single fiber fragmentation test( SFFT) was used to characterize the interfacial adhesion performance of PI fiber as a simple and accurate analysis method. It was found that the interfacial shear strength between the fiber and resin after oxygen plasma modification was increased by 54% compared to the untreated fiber. Meanwhile, the surface micromorphology,chemical composition, wettability of fibers and the interface morphology at the fiber fracture were analyzed by field emission scanning electron microscope( FESEM), X-ray photoelectron spectroscopy( XPS),contact angle measurement and polarizing microscope,respectively. All of these results demonstrated that the single fiber fragmentation test for analyzing the interfacial adhesion of PI fibers was effective.

Testing of Cotton Fiber Length

To understand the influences of actual sampling conditions on cotton fiber length testing, this article presents a theoretic study on the distributions and fibrogram of the sample taken out by sampler from ideal sliver at a certain angle. From the distributions expression it can be found that the size of the sampler and the sampling angle are important factors which affect sampling, but if the sampling width is narrow enough, the influence of the sampling angle on the distributions and fibrogram is small enough to be omitted. This is an important conclusion for sampling, in light of this, some suggestions for designing new type sampler are put forward.

Monitoring of polymeric membrane fouling in hollow fiber module using ultrasonic nondestructive testing

This study describes the development of novel protocols extending the real-time ultrasonic reflectometry(UTDR) for the detection of membrane fouling in hollow fiber module during ultrafiltration(UF) of oily water treatment. A specially designed acoustic sensor with a frequency of 2.5 MHz was used. The hollow fiber membranes used were polysulphone(PSf) UF membranes with MWCO 40 kDa. The wastewaters with three different oily concentrations of 100, 500 and 1 000 mg/L were investigated. Diesel oil was utilized as the primary foulant. The results show that the permeate flux declines with operation time and its value becomes lower with the increase of the oily concentration in wastewater. It is found that ultrasonic measurement can detect the fouling and cleaning processes. A new signal analysis protocol-ultrasonic reflected energy was developed. Ultrasonic reflected energy obtained indicates the deposition of oily layer as a function of operation time and its removal after cleaning. The overall flux decline is reasonably correlated with the changes in ultrasonic reflected energy. This research provides the evidence that the ultrasonic reflectometry technique is capable of monitoring membrane fouling and cleaning in hollow fiber modules.

Effectiveness of Fiber Bragg Grating monitoring in the centrifugal model test of soil slope under rainfall conditions

Centrifugal model testsare playing an increasingly importantrolein investigating slope characteristics under rainfall conditions. However, conventional electronic transducers usually fail during centrifugal model tests because of the impacts of limitedtest space, high centrifugal force, and presence of water, with the result that limited valid data is obtained. In this study, Fiber Bragg Grating(FBG) sensing technology is employed in the design and development of displacement gauge, an anchor force gauge and an anti-slide pile moment gauge for use on centrifugal model slopes with and without a retaining structure. The two model slopes were installed and monitored at a centrifugal acceleration of 100 g. The test results show that the sensors developed succeed in capturing the deformation and retaining structure mechanical response of the model slopes during and after rainfall. The deformation curvefor the slope without retaining structure shows a steepresponse that turns gradualfor the slope with retaining structure. Importantly, for the slope with the retaining structure, results suggest that more attention be paid to increase of anchor force and antislide pile moment during rainfall. This study verifies the effectiveness of FBG sensing technology in centrifuge research and presents a new and innovative method for slope model testing under rainfall conditions.

Influence of Sugarcane Bagasse Fibers on the Mechanical Strength and Porosity of Concrete Made with Forspak 42.5 N Cement in the Republic of Congo

The concrete mixed to sugarcane bagasse fibers and polypropylene fibers prepared with varied conditions were presented. The aim of our study is to formulate a concrete mixed with sugarcane bagasse fibers, which will gradually replace the conventional polypropylene fibers often used. We formulated all our concretes using the dreux gorisse method. We used an oven calibrated at 105˚C to dry the washed fibers. We also carried out tensile splitting and compression tests, at 28 and 112 days of age. The reinforcement mechanisms of sugarcane bagasse fibers and polypropylene fibers concretes were subjected to tensile splitting and compression tests after total immersion of the specimens in tap water at 28 and 112 days. Porosity at 28 days, mass loss and drying shrinkage at 80 days were also studied. The curing processes of concretes containing 0.10, 0.15, 0.17, 0.23 and 0.25% bagasse fibers were compared with those of ordinary concretes containing no fiber. The results showed that the addition of bagasse fibers reduces mechanical strength and porosity. In summary, specimens SBC-0.15 and SBC-0.17 showed the best results for all fibers. We plan to do the same work, but this time with raffia or palm nut fibers.

Application Research of the Non-Destructive Testing Using Optical Fiber Sensor

In this paper, an optical fiber sensor is designed by using optical Faraday effect. It is composed of fiber collimator, polarizer, magneto-optical crystal and mirror. Based on the magnetic flux leakage (MFL) theory, The optical fiber sensor was placed between two permanent magnets with the N-pole. Therefore, the optical fiber sensing system was built to detect the defective ferromagnetic objects. Theoretical and experimental studies shown that the system can identify a little defects, such as irons’ blind hole (diameter φ =?3mm , depth t = 4mm?), irons’ grooves (length l= 30mm , width?ω = 10mm ), hole (φ?=?3mm ) and crackle etc. The system has the characteristics of small size, high sensitivity, fast signal response and high resolution. In terms of the defective oil and gas pipelines detection, The optical fiber sensing system is used in non-destructive testing, which will be valuable and meaningful.

纤维加筋黏土Ⅰ型、Ⅱ型宏细观断裂特性试验研究

探究掺入纤维对黏土抗裂性能的影响,引入直裂缝半圆弯曲试样(NSCB)和斜裂缝半圆弯曲试样(CNSCB),开展纤维加筋黏土的Ⅰ型、Ⅱ型断裂试验,从宏细观角度分析纤维掺量对加筋黏土Ⅰ型、Ⅱ型断裂特性的影响机制。结果表明:掺玻璃纤维加筋黏土试样的Ⅰ型、Ⅱ型断裂韧度KⅠC、KⅡC值和峰值荷载均高于纯黏土试样;KⅠC、KⅡC都随纤维掺量的增加呈先增加后减小的规律,0.2%掺量时最大;通过数字图像相关技术(DIC)法测得的断裂过程区(FPZ)长度与最大切向应力断裂准则(MTS)预测的较为吻合,随着试样纤维掺量的增加,NSCB试样和CNSCB试样的FPZ长度先减小后略微增大,最后趋于平缓。

基于声学参数的纤维复合材料机械强度无损检测技术研究

纤维复合材料在使用过程中可能会出现各种缺陷,如裂纹、分层、脱粘等。这些缺陷会导致材料的性能下降,甚至引发失效。为预测和评估纤维复合材料的长期使用性能,本文开展了基于声学参数的纤维复合材料机械强度无损检测技术研究,通过数值模拟和超声实验研究,建立了基于超声无损检测技术的纤维复合材料检测信息特征提取和性能评价方法,开发了纤维复合材料的超声检测装置。实验结果表明在玻璃纤维复合管刚度矩阵测量精度验证最大误差1.15%,在钢管上对检测装置验证得出杨氏模量精度最大误差9.3%,泊松比精度最大误差-8.27%。

文献《Validation of commercial fiber optic components for aerospace environments》点评

文章是对一篇SPIE会议文献《用于太空环境的商业光纤器件地面验证方法》的点评。介绍了商业光纤部件从市场采购到准备作为太空飞行部件使用前,在空间环境作用(包括真空、热、振动、辐射)下的地面工艺性合格鉴定试验技术。这项技术由NASA哥达德空间飞行中心(GSFC)创立并命名为"工艺技术有效性保证法",该项技术还包括如何建立商用光纤产品制造工艺性合格鉴定试验验收标准或准则方面的内容。"点评"还针对文献中3个实例之一"水星激光高度仪"试验件的热与振动环境试验规范、试验夹具等重要试验技术信息进行详细介绍。

木质素-稻草改良土的力学特性与修正Duncan-Chang模型

木质素具有胶结土体的作用,稻草纤维也具备提高土体抗剪强度的能力,而采用木质素和稻草共同改良红黏土的研究相对较少。本文通过固结不排水三轴试验,获得了木质素-稻草改良土在不同围压和不同木质素掺量下的应力-应变曲线,并据此研究该改良土的力学特性;同时通过建立修正Duncan-Chang模型,来分析木质素掺量对模型参数的影响。研究结果表明:改良土主应力差随木质素掺量的增加先增大后减小,当木质素的掺量为0.7%时,其到达最大值;改良土初始变形模量Ei、极限偏应力(σ1-σ3)ult、黏聚力c、内摩擦角φ及参数K均随木质素掺量的增加先增大后减小,参数n随木质素掺量的增加而增大,而破坏比Rf受木质素掺量的影响较小。

Effect of neat and reinforced polyacrylonitrile nanofibers incorporation on interlaminar fracture toughness of carbon/epoxy composite

This paper presents an experimental investigation on fracture behavior of epoxy resin-carbon fibers composites interleaved with both neat polyacrylonitrile （PAN） nanofibers and A1203-PAN nanofibers. In particular, the paper focuses on the effect of adding Al2O3 nanopartiles in PAN nanofibers, which were incorporated in unidirectional （UD） laminates. The effectiveness of adding a thin film made of Al2O3-PAN on the fracture behavior of the carbon fiber reinforced polymer （CFRP） has been addressed by comparing the energy release rates, obtained by testing double cantilever beam （DCB） samples under mode I loading condition. A general improvement in interlaminar fracture energy of the CFRP is observed when the both neat PAN nanofibers and Al2O3-PAN nanofibers are interleaved. However, higher interlaminar strength has been observed for the samples with a thin film of Al2O3-PAN nanofibers, suggesting a better stress distribution and stress transformation from resin-rich area to reinforcement phase of hybrid composites.

A Fiber Pull-Out Based Model for Synthetic Fiber Reinforced Concrete Beams under a Flexural Load

This work is intended to be a simple contribution to building a model able to implement theoretical results related to the random oriented fiber reinforced concrete in a procedure that could be used in structures analysis and design involving fiber reinforced elements. Here follows a short outline: In the introduction chapter the problem is presented together the work done. Section 2 develops some ancillary concepts of this material and its mechanical properties, while in Section 3, following the path of other researchers, the assumptions made to solve the problem are presented, together with the most relevant results related to presence of 3D randomly oriented fiber. In the following section a review of the mechanical process of fiber pull-out is done, and the results, mostly due to Victor Li researches, of a 3D randomly oriented synthetic fiber stress vs crack opening in a pull-out process from a cement matrix. In Section 5 the author, after making some assumptions about the configuration of the strain and crack geometry in the cross section where failure is assume to occur under flexural bending moment, the resultant stress is integrated to find the resultant internal moment vs increasing strain and crack width. In this analysis, the crack bridging law for synthetic fiber in FRC presented in the previous section is taken into account. In Section 6, a procedure to find a cross section configuration in equilibrium under external bending moment has been built. Under the assumption of a perfectly plastic collapse mechanism a numerical simulation is conducted on a specimen that undergoes a four-point bending test. A comparison with the trend of a similar test on a synthetic FRC sample has been done. The work is completed by the conclusions that could be inferred from this work.

Seismic response of continuous span bridges through fiber-based finite element analysis

It is widely recognized that nonlinear time-history analysis constitutes the most accurate way to simulate the response of structures subjected to strong levels of seismic excitation. This analytical method is based on sound underlying principles and has the capability to reproduce the intrinsic inelastic dynamic behavior of structures. Nonetheless, comparisons with experimental results from large-scale testing of structures are still needed, in order to ensure adequate levels of confidence in this numerical methodology. The fiber modelling approach employed in the current endeavor inherently accounts for geometric nonlinearities and material inelasticity, without a need for calibration of plastic hinges mechanisms, typical in concentrated plasticity models. The resulting combination of analysis accuracy and modelling simplicity, allows thus to overcome the perhaps not fully justifiable sense of complexity associated to nonlinear dynamic analysis. The fiber-based modelling approach is employed in the framework of a finite element program downloaded from the Intemet for seismic response analysis of framed structures. The reliability and accuracy of the program are demonstrated by numerically reproducing pseudo-dynamic tests on a four span continuous deck concrete bridge. Modelling assumptions are discussed, together with their implications on numerical results of the nonlinear time-history analyses, which were found to be in good agreement with experimental results.

Effectiveness of Metanx Prescription Medical Food on Small Nerve Fibers and Monofilament Sensation in Patients with Diabetic Peripheral Polyneuropathy

Purpose: Diabetic peripheral neuropathy (DPN) is prevalent among the population with type 2 diabetes, and treatment approaches are limited. The combination of L-methylfolate-methylcobalamin-pyridoxal-5-phospate (LMF-MC-PP, Metanx?) is a prescription medical food that has demonstrated significant improvements in sensory perception and quality of life as well as reduced neuropathic pain in patients with DPN. The present study examined the effects of LMF-MC-PP on sensory perception and epidermal nerve fiber density (ENFD) among patients with confirmed DPN. Methods: Patients with type 2 diabetes and diagnosed with diabetic peripheral polyneuropathy, based on loss of vibratory perception, warm-cold discrimination or monofilament sensation, underwent bilateral lower extremity ENFD assessments via skin punch biopsy and were started on LMF-MC-PP. ENFD and monofilament testing were repeated at 6 months. Findings: Of 123 patients evaluated, all had monofilament testing at baseline and 6 months and 122 had assessments at both time points. A significant (p < 0.05) improvement in ENFD from baseline to 6 months was observed. A significant (p = 0.0001) improvement in monofilament testing also was observed. Overall, more patients had intact sensation after 6 months, with 60 (48.8%) of 123 patients having positive monofilament test at baseline as compared to 95 (77.2%) positive after 6 months. An analysis of the association between improvements in ENFD and monofilament testing found that the two tended to occur together, and this was significant (p < 0.05) for the right limb. Implications: Clinically important and statistically significant improvements in ENFD and monofilament sensation were associated with LMF-MC-PP in patients with DPN. When compared to the decrease in ENFD expected among DPN patients, the improvements are even more clinically significant. These findings should be validated in a larger, placebo-controlled study.

钢纤维喷射砂浆力学性能与流动度多因素正交试验分析

为探究基体因素对钢纤维喷射砂浆力学性能和流动度的影响,基于正交试验方法对砂浆试件进行了力学性能和流动度测试。结果表明:砂胶比(A)对劈裂抗拉强度的影响较大,对7 d抗压强度有一定的影响,对后期抗折强度影响特别显著;钢纤维掺量(B)对劈裂抗拉强度、前期抗折强度和前中期抗压强度的影响分别为特别显著、显著和不显著;速凝剂掺量(C)对7 d前抗压强度、中后期劈裂抗拉强度影响显著;粉煤灰掺量(D)仅对后期抗压强度的影响显著;前述四种因素掺量对流动度的影响均不显著。由层次分析法得到对抗压强度、抗折强度、劈裂抗拉强度和流动度改善效果最佳的配合比分别为A1B3C3D1、A3B3C1D2、A3B3C3D1、A2B1C1D3,由功效系数法得到综合最佳配合比为A2B3C1D2。钢纤维在基体中起桥接与锚固加强的作用,速凝剂在水化过程中消耗大量的Ca(OH)_(2)并生成钙矾石,促使喷射砂浆早期强度迅速提升。

Influence of differential settlement on pavement structure of widened roads based on large-scale model test

This study introduced at first the background of numerous highway widening projects that have been developed in recent years in China.Using a large ground settlement simulator and a fiber Bragg grating (FBG) strain sensor network system,a large-scale model test,with a similarity ratio of 1:2,was performed to analyze the influence of differential settlement between new and old subgrades on pavement structure under loading condition.The result shows that excessive differential settlement can cause considerable tensile strain in the pavement structure of a widened road,for which a maximum value (S) of 6 cm is recommended.Under the repetitive load,the top layers of pavement structure are subjected to the alternate action of tensile and compressive strains,which would eventually lead to a fatigue failure of the pavement.However,application of geogrid to the splice between the new and the old roads can reduce differential settlement to a limited extent.The new subgrade of a widened road is vulnerable to the influence of dynamic load transferred from the above pavement structures.While for the old subgrade,due to its comparatively high stiffness,it can well spread the load on the pavement statically or dynamically.The test also shows that application of geogrid can effectively prevent or defer the failure of pavement structure.With geogrid,the modulus of resilience of the subgrade is increased and inhomogeneous deformation can be reduced;therefore,the stress/strain distribution in pavement structure under loading condition becomes uniform.The results obtained in this context are expected to provide a helpful reference for structural design and maintenance strategy for future highway widening projects.

Debonding Patch Detection in FRP-Strengthened Materials with Fiber-Optic Interferometer

The interfacial debonding in fiber-reinforced plastic(FRP)strengthened repair material will affect the bonding strength and lead to failure of the repair without warning.Unfortunately the interfacial damage is normally invisible and often in the form of a patch rather than a through-width crack.Therefore,a debonding patch detection technique based on fiber optic interferometry is proposed.A quasi-impulse loading is applied with a rubberhead hammer and the total elongation of a surface-mounted optical fiber along the length of the repair material is measured as a function of load position.When a debonding patch is present,the induced sudden slope or sign change on the plot of fiber integral strain v.s.load position will reveal the extent and the location of the debonded area.The results of the study indicate that the proposed technique is applicable for debonding patch detection in repaired members under various support conditions.

Rheological Behavior of Basalt Fiber Reinforced Asphalt Mastic

The characters of basalt fiber are analyzed and compared with commonly used fibers. The rheological behaviors of the basalt fiber reinforced asphalt mastic are investigated by the dynamic shear rheological tests and the repeated creep tests. The results show that basalt fiber has excellent reinforced performances, such as high asphalt absorption ratio, low water absorption ratio, high tensile strength, high elastic modulus and high temperature stability. The rutting factor of the fiber reinforced asphalt mastic is higher than the plain asphalt mastic and the reinforced effects are more remarkable under high temperature. The rheological performances of the asphalt mastic demonstrate a good linear relationship between different temperature and loading frequency. The creep stiffness modulus of the asphalt mastic at different loading time can be expressed by power function. Improved Burgers model is used to represent the rheological behaviors of the asphalt mastic with basalt fiber and the model parameters are estimated.