The study of liquid film characteristics in multiphase flow is a very important research topic, however,the characteristics of the liquid film around Taylor bubble structure in gas, oil and water three-phase flow are ...The study of liquid film characteristics in multiphase flow is a very important research topic, however,the characteristics of the liquid film around Taylor bubble structure in gas, oil and water three-phase flow are not clear. In the present study, a novel liquid film sensor is applied to measure the distributed signals of the liquid film in three-phase flow. Based on the liquid film signals, the liquid film characteristics including the structural characteristics and the nonlinear dynamics characteristics in three-phase flows are investigated for the first time. The structural characteristics including the proportion, the appearance frequency and the thickness of the liquid film are obtained and the influences of the liquid and gas superficial velocities and the oil content on them are investigated. To investigate the nonlinear dynamics characteristics of the liquid film with the changing flow conditions, the entropy analysis is introduced to successfully uncover and quantify the dynamic complexity of the liquid film behavior.展开更多
It is of a vital importance to reduce the frictional losses in marine diesel engines. Advanced surface textures have provided an e ective solution to friction performance of rubbing pairs due to the rapid development ...It is of a vital importance to reduce the frictional losses in marine diesel engines. Advanced surface textures have provided an e ective solution to friction performance of rubbing pairs due to the rapid development of surface engineering techniques. However,the mechanisms through which textured patterns and texturing methods prove beneficial remains unclear. To address this issue,the tribological system of the cylinder liner?piston ring(CLPR) is investigated in this work. Two types of surface textures(Micro concave,Micro V?groove) are processed on the cylinder specimen using di erent processing methods. Comparative study on the friction coe cients,worn surface texture features and oil film characteristics are performed. The results demonstrate that the processing method of surface texture a ect the performance of the CLPR pairs under the specific testing conditions. In addition the micro V?groove processed by CNCPM is more favorable for improving the wear performances at the low load,while the micro?con?cave processed by CE is more favorable for improving the wear performances at the high load. These findings are in helping to understand the e ect of surface texture on wear performance of CLPR.展开更多
The research on the oil film characteristic of piston pair is beneficial to the design and optimization of friction pair,which can improve the performance of piston pump.The fluid pressure of piston cavity is accurate...The research on the oil film characteristic of piston pair is beneficial to the design and optimization of friction pair,which can improve the performance of piston pump.The fluid pressure of piston cavity is accurately obtained by AMEsim simulation.Oil film thickness field model of piston pair under the slanting state of piston is established,and the distribution law is numerically analyzed under different speed and pressure by Matlab.The experiment model pump for oil film characteristic of piston pair is designed to measure oil film thickness under the pressure of 18 MPa.The experiment results show that oil film thickness varies greatly under high pressure,and oil film thickness fluctuates sharply under low speed.The minimum oil film thickness increases with spindle speed increasing and oil film characteristic of piston pair based on the numerical analysis method is verified.This method lays a foundation for studying the friction performance of piston pair in the axial piston pump.展开更多
Herein,a hot cracking initiation criterion based on the characteristics of solidification liquid film and the microstructure was proposed,which integrated both the mechanical and non-mechanical factors during solidifi...Herein,a hot cracking initiation criterion based on the characteristics of solidification liquid film and the microstructure was proposed,which integrated both the mechanical and non-mechanical factors during solidification.The criterion also took the effect of the shrinkage volume of the solid-liquid two-phase in the mushy zone,the flow behavior of the liquid film and the microstructure on the feeding behavior into account.Meanwhile,the effect factors of hot cracking initiation such as alloy composition,microstructure,mold design and process condition were included in this criterion,and it could quantitatively calculate whether hot cracks occurred under a certain state or not during solidification.The criterion was utilized to predict whether hot cracks occurred in Al-4.0 wt%Cu alloy in different initial solidification states or not,which was consistent with the experimental results and verified its reliability.According to the criterion expression,Vfeeding*was related with five effect factors includingη,ΔP*,l*,r*and n,in which r*and n were in positive correlation with Vfeeding*whileη,ΔP*and l*were in negative correlation with that,which provided a good instructive significance for mold design,process optimization and composition and microstructure regulation of alloys and simultaneously further enriched the mechanism and influencing factors of hot cracking initiation.Furthermore,a multiscale simulation method for calculating the characteristic parameters of hot tearing behavior during solidification was also provided in this study.展开更多
The process of producing high viscosity polyester by transesterification polycondensation needs to adjust the operating conditions and equipment structure of pre-polycondensation kettle and final polycondensation kett...The process of producing high viscosity polyester by transesterification polycondensation needs to adjust the operating conditions and equipment structure of pre-polycondensation kettle and final polycondensation kettle to realize process intensification.In view of this,the fluid volume function method of computational fluid dynamics numerical simulation was used to investigate the film formation and surface renewal characteristics of horizontal polycondensation kettle under different operating conditions,including viscosity,rotating speed and liquid height.The results show that the viscosity and rotating speed were positively correlated with the film area and surface renewal in the pre-polycondensation stage.However,increasing the viscosity by several orders of magnitude in the final polycondensation kettle,the larger the film area and film thickness,but the overall surface renewal of the disk decreased.Therefore,a hexagonal hole disk is designed.By comparison,it is found that the film is more uniform,the surface update frequency is higher,and the power consumption can be reduced by more than 20%.展开更多
Based on the theory of unsteady hydrodynamic lubrication and relevant mathematic and physical methods, a basic model was developed to analyze the unsteady lubrication film thickness, pressure stress and friction stres...Based on the theory of unsteady hydrodynamic lubrication and relevant mathematic and physical methods, a basic model was developed to analyze the unsteady lubrication film thickness, pressure stress and friction stress in the work zone in strip rolling. The distribution of pressure stress and friction stress in the work zone was obtained. A numerical simulation was made on a 1850 cold rolling mill. The influence of back tension stress and reduction on the distribution of pressure stress and friction stress between the roll gaps was qualitatively analyzed by numerical simulation. The calculated results indicate that the higher the back tension, the lower the pressure stress and the friction stress in the work zone, and the largest friction stresses are obtained at the inlet and outlet edges. The pressure and friction gradients are rather small at high back tension. The pressure-sensitive lubricant viscosity increases exponentially with the increase of pressure. The unsteady lubrication phenomenon in the roll bite is successfully demonstrated.展开更多
Recur to multi-hole and better elastic characteristics of metal rubber (MR), a new squeezed film damper with MR (SFD/MR) throttle ring installed on the end of MR and MR damping ring installed on the radial directi...Recur to multi-hole and better elastic characteristics of metal rubber (MR), a new squeezed film damper with MR (SFD/MR) throttle ring installed on the end of MR and MR damping ring installed on the radial direction of MR is implemented. Based on the D'alembert principle, a locomotion equation and the mathematical model of stationary response of SFD/MR system is put forward. It proves that the SFD/MR has better ability to resist unbalance loads than the traditional SFD after the stationary dynamic characteristics of the traditional SFD and the new SFD/MR are researched.展开更多
The Research Center of Superconducting Materials of GRINM prepared a YBaCuOsuperconducting film with thickness of 500 nm, the microwave characterization of which was car-ried out at Microwave Center, Chengdu Electroni...The Research Center of Superconducting Materials of GRINM prepared a YBaCuOsuperconducting film with thickness of 500 nm, the microwave characterization of which was car-ried out at Microwave Center, Chengdu Electronics Science-technological University. The com-prehensive Microwave characteristics for large-area superconducting film is obtained firstly inChina. Using this film Microwave Center prepared a cavity, the quality factor Q of which attainedto the-state-of the-art (Q= 13100, at 79 K and 3.04 GHz).展开更多
Gamma irradiation is employed for in situ preparation of PVA-PANI-ZnS nanocomposite. The irradiation dose is varied from 10 to 40 kGy at 10 kGy intervals. The XRD result confirms the formation of crystalline phases co...Gamma irradiation is employed for in situ preparation of PVA-PANI-ZnS nanocomposite. The irradiation dose is varied from 10 to 40 kGy at 10 kGy intervals. The XRD result confirms the formation of crystalline phases corresponding to ZnS nanoparticles, PVA and PANI. Field emission scanning electron microscopy shows the formation of agglomerated PANI along the PVA backbone, within which the ZnS nanoparticles are dispersed.UV-visible spectroscopy is conducted to measure the transmittance spectra of samples revealing the electronic absorption characteristics of ZnS and PANI nanoparticles. Photo-acoustic(PA) setup is installed to investigate the thermal properties of samples. The PA spectroscopy indicates a high value of thermal diffusivity for samples due to the presence of ZnS and PANI nanoparticles. Moreover, at higher doses, the more polymerization and formation of PANI and ZnS nanoparticles result in enhancement of thermal diffusivity.展开更多
The ultrathin aluminum films with thickness in the range of 2~60 nm have been deposited by dc magnetron sputtering apparatus. Reflectance and transmittance of the obtained samples were measured with a WFZ-900-D4 UV/V...The ultrathin aluminum films with thickness in the range of 2~60 nm have been deposited by dc magnetron sputtering apparatus. Reflectance and transmittance of the obtained samples were measured with a WFZ-900-D4 UV/VIS spectrophotometer. The optical constant (n, k) and permittivity (ε', ε') were determined by applying Newton-Simpson recurrent substitution method. The results indicate that the electromagnetic constitutive characteristic of ultrathin aluminum films is a function of thickness and has obvious size effect.展开更多
The transfer characteristics of amorphous indium-zinc-oxide thin film transistors are measured in the temperature range of 10-400K. The variation of electrical parameters (threshold voltage, field effect mobility, su...The transfer characteristics of amorphous indium-zinc-oxide thin film transistors are measured in the temperature range of 10-400K. The variation of electrical parameters (threshold voltage, field effect mobility, sub-threshold swing, and leafage current) with decreasing temperature are then extracted and analyzed. Moreover, the dom- inated carrier transport mechanisms at different temperature regions are investigated. The experimental data show that the carrier transport mechanism may change from trap-limited conduction to variable range hopping conduction at lower temperature. Moreover, the field effect mobilities are also extracted and simulated at various temperatures.展开更多
Cu/HfOx/n^+Si devices are fabricated to investigate the influence of technological parameters including film thickness and Ar/02 ratio on the resistive switching (RS) characteristics of HfOx films, in terms of swit...Cu/HfOx/n^+Si devices are fabricated to investigate the influence of technological parameters including film thickness and Ar/02 ratio on the resistive switching (RS) characteristics of HfOx films, in terms of switch ratio, endurance properties, retention time and multilevel storage. It is revealed that the RS characteristics show strong dependence on technological parameters mainly by altering the defects (oxygen vacancies) in the film. The sample with thickness of 2Onto and Ar/O2 ratio of 12:3 exhibits the best RS behavior with the potential of multilevel storage. The conduction mechanism of all the films is interpreted based on the filamentary model.展开更多
TiO2 thin films were prepared by DC magnetron sputtering with the oxygen flow rate higher than the threshold. The film deposited for 5 h was of anatase phase with a preferred orientation along the <220> directio...TiO2 thin films were prepared by DC magnetron sputtering with the oxygen flow rate higher than the threshold. The film deposited for 5 h was of anatase phase with a preferred orientation along the <220> direction, but the films deposited for 2 and 3 h were amorphous. The transmittance and photocatalytic activity of the TiO2 films increased constantly with increasing film thickness. When the annealing temperature was lower than 700℃, only anatase grew in the TiO2 film. TiO2 phase changed from anatase to rutile when the annealing temperature was above 800℃. The photocatalytic activity decreased with increasing annealing temperature.展开更多
An experimental investigation was performed to study the heat transfer in an eight-nozzle spray cooling system with de-ionized water as the working fluid. Visualization of the liquid-solid contact area and the flow ne...An experimental investigation was performed to study the heat transfer in an eight-nozzle spray cooling system with de-ionized water as the working fluid. Visualization of the liquid-solid contact area and the flow near the heated surface was made using a microscopic lens system in conjunction with an advanced high-speed camera. The film thickness and film wavelike characteristics under liquid volume flow rates ranged from 2.78×10 -6 m 3 /s to 1.39×10 -5 m 3 /s and surface temperatures between 22℃ and 78.2℃ were examined respectively. The development process of the liquid film on the heated surface was observed. The local mean film thickness, the film wavelike characteristics and the behavior of the bubbles appeared in the liquid film were captured using an image processing technique. It is discovered that there exists a climax of local mean film thickness during the starting process of spray cooling. When the liquid film reaches the dynamic stable state, the dimensionless mean film thickness decreases with the increase of the liquid volume flow rate, and increases with the increase of surface temperature generally. Besides, the volume flow rate has a more significant impact on the wavelength and amplitude of the liquid film compared to the surface temperature.展开更多
In this work, we focus on the optical super-resolution effect induced by strong nonlinear saturation absorption(NSA) of graphene oxide(GO) membranes. The third-order optical nonlinearities are characterized by the can...In this work, we focus on the optical super-resolution effect induced by strong nonlinear saturation absorption(NSA) of graphene oxide(GO) membranes. The third-order optical nonlinearities are characterized by the canonical Z-scan technique under femtosecond laser(wavelength: 800 nm, pulse width: 100 fs) excitation. Through controlling the applied femtosecond laser energy, NSA of the GO films can be tuned continuously. The GO film is placed at the focal plane as a unique amplitude filter to improve the resolution of the focused field. A multi-layer system model is proposed to present the generation of a deep sub-wavelength spot associated with the nonlinearity of GO films. Moreover, the parameter conditions to achieve the best resolution(~λ/6) are determined entirely. The demonstrated results here are useful for high density optical recoding and storage, nanolithography, and super-resolution optical imaging.展开更多
Polyaniline,ZnO and polyaniline/ZnO nanocomposite thin films are coated on glass substrates using the spray pyrolysis technique.The samples are characterized by the XRD,SEM,EDAX,UV-Vis and I-V characteristics. The XRD...Polyaniline,ZnO and polyaniline/ZnO nanocomposite thin films are coated on glass substrates using the spray pyrolysis technique.The samples are characterized by the XRD,SEM,EDAX,UV-Vis and I-V characteristics. The XRD analyses confirm that the spray-coated polyaniline and ZnO thin films have orthorhombic and hexagonal structures,respectively,and optical bandgap energy decreases from 3.81 to 3.41 eV with the addition of a Zn atom.SEM analysis of the polyaniline/ZnO nanocomposite thin films shows that there is an agglomeration of ZnO particles with uniform distribution in the polyaniline matrix,and the diode characteristics of the polyaniline /ZnO nanocomposite show weak rectification behavior.Parameters such as the ideality factor,reverse saturation current and barrier height are calculated from the I-V characteristics.展开更多
基金supported by the National Natural Science Foundation of China (42074142, 51527805, 41974139)China Postdoctoral Science Foundation (2020M680969, 2021T140099)the Fundamental Research Funds for the Central Universities (N2104013)。
文摘The study of liquid film characteristics in multiphase flow is a very important research topic, however,the characteristics of the liquid film around Taylor bubble structure in gas, oil and water three-phase flow are not clear. In the present study, a novel liquid film sensor is applied to measure the distributed signals of the liquid film in three-phase flow. Based on the liquid film signals, the liquid film characteristics including the structural characteristics and the nonlinear dynamics characteristics in three-phase flows are investigated for the first time. The structural characteristics including the proportion, the appearance frequency and the thickness of the liquid film are obtained and the influences of the liquid and gas superficial velocities and the oil content on them are investigated. To investigate the nonlinear dynamics characteristics of the liquid film with the changing flow conditions, the entropy analysis is introduced to successfully uncover and quantify the dynamic complexity of the liquid film behavior.
基金Supported by National Natural Science Foundation of China(Grant No.51422507)Hubei Provincial Natural Science Foundation of China(Grant No.2015CFB372)+1 种基金Fundamental Research Funds for the Central Universities of China(Grant No.2015IVA010)Tribology Science Fund of State Key Laboratory of Tribology of China(Grant No.SKLTKF14B03)
文摘It is of a vital importance to reduce the frictional losses in marine diesel engines. Advanced surface textures have provided an e ective solution to friction performance of rubbing pairs due to the rapid development of surface engineering techniques. However,the mechanisms through which textured patterns and texturing methods prove beneficial remains unclear. To address this issue,the tribological system of the cylinder liner?piston ring(CLPR) is investigated in this work. Two types of surface textures(Micro concave,Micro V?groove) are processed on the cylinder specimen using di erent processing methods. Comparative study on the friction coe cients,worn surface texture features and oil film characteristics are performed. The results demonstrate that the processing method of surface texture a ect the performance of the CLPR pairs under the specific testing conditions. In addition the micro V?groove processed by CNCPM is more favorable for improving the wear performances at the low load,while the micro?con?cave processed by CE is more favorable for improving the wear performances at the high load. These findings are in helping to understand the e ect of surface texture on wear performance of CLPR.
基金Supported by the National Natural Science Foundation of China(No.51975164)the Fundamental Research Foundation for Universities of Heilongjiang Province.
文摘The research on the oil film characteristic of piston pair is beneficial to the design and optimization of friction pair,which can improve the performance of piston pump.The fluid pressure of piston cavity is accurately obtained by AMEsim simulation.Oil film thickness field model of piston pair under the slanting state of piston is established,and the distribution law is numerically analyzed under different speed and pressure by Matlab.The experiment model pump for oil film characteristic of piston pair is designed to measure oil film thickness under the pressure of 18 MPa.The experiment results show that oil film thickness varies greatly under high pressure,and oil film thickness fluctuates sharply under low speed.The minimum oil film thickness increases with spindle speed increasing and oil film characteristic of piston pair based on the numerical analysis method is verified.This method lays a foundation for studying the friction performance of piston pair in the axial piston pump.
基金the National Natural Science Foundation of China(No.51875365).
文摘Herein,a hot cracking initiation criterion based on the characteristics of solidification liquid film and the microstructure was proposed,which integrated both the mechanical and non-mechanical factors during solidification.The criterion also took the effect of the shrinkage volume of the solid-liquid two-phase in the mushy zone,the flow behavior of the liquid film and the microstructure on the feeding behavior into account.Meanwhile,the effect factors of hot cracking initiation such as alloy composition,microstructure,mold design and process condition were included in this criterion,and it could quantitatively calculate whether hot cracks occurred under a certain state or not during solidification.The criterion was utilized to predict whether hot cracks occurred in Al-4.0 wt%Cu alloy in different initial solidification states or not,which was consistent with the experimental results and verified its reliability.According to the criterion expression,Vfeeding*was related with five effect factors includingη,ΔP*,l*,r*and n,in which r*and n were in positive correlation with Vfeeding*whileη,ΔP*and l*were in negative correlation with that,which provided a good instructive significance for mold design,process optimization and composition and microstructure regulation of alloys and simultaneously further enriched the mechanism and influencing factors of hot cracking initiation.Furthermore,a multiscale simulation method for calculating the characteristic parameters of hot tearing behavior during solidification was also provided in this study.
基金the financial support of the National Key Research and Development Program of China(2020YFA0710202,2018YFC0808805)。
文摘The process of producing high viscosity polyester by transesterification polycondensation needs to adjust the operating conditions and equipment structure of pre-polycondensation kettle and final polycondensation kettle to realize process intensification.In view of this,the fluid volume function method of computational fluid dynamics numerical simulation was used to investigate the film formation and surface renewal characteristics of horizontal polycondensation kettle under different operating conditions,including viscosity,rotating speed and liquid height.The results show that the viscosity and rotating speed were positively correlated with the film area and surface renewal in the pre-polycondensation stage.However,increasing the viscosity by several orders of magnitude in the final polycondensation kettle,the larger the film area and film thickness,but the overall surface renewal of the disk decreased.Therefore,a hexagonal hole disk is designed.By comparison,it is found that the film is more uniform,the surface update frequency is higher,and the power consumption can be reduced by more than 20%.
基金Project(51175133)supported by the National Natural Science Foundation of China
文摘Based on the theory of unsteady hydrodynamic lubrication and relevant mathematic and physical methods, a basic model was developed to analyze the unsteady lubrication film thickness, pressure stress and friction stress in the work zone in strip rolling. The distribution of pressure stress and friction stress in the work zone was obtained. A numerical simulation was made on a 1850 cold rolling mill. The influence of back tension stress and reduction on the distribution of pressure stress and friction stress between the roll gaps was qualitatively analyzed by numerical simulation. The calculated results indicate that the higher the back tension, the lower the pressure stress and the friction stress in the work zone, and the largest friction stresses are obtained at the inlet and outlet edges. The pressure and friction gradients are rather small at high back tension. The pressure-sensitive lubricant viscosity increases exponentially with the increase of pressure. The unsteady lubrication phenomenon in the roll bite is successfully demonstrated.
基金This project is supported by National Natural Science Foundation of China (No.50075017)
文摘Recur to multi-hole and better elastic characteristics of metal rubber (MR), a new squeezed film damper with MR (SFD/MR) throttle ring installed on the end of MR and MR damping ring installed on the radial direction of MR is implemented. Based on the D'alembert principle, a locomotion equation and the mathematical model of stationary response of SFD/MR system is put forward. It proves that the SFD/MR has better ability to resist unbalance loads than the traditional SFD after the stationary dynamic characteristics of the traditional SFD and the new SFD/MR are researched.
文摘The Research Center of Superconducting Materials of GRINM prepared a YBaCuOsuperconducting film with thickness of 500 nm, the microwave characterization of which was car-ried out at Microwave Center, Chengdu Electronics Science-technological University. The com-prehensive Microwave characteristics for large-area superconducting film is obtained firstly inChina. Using this film Microwave Center prepared a cavity, the quality factor Q of which attainedto the-state-of the-art (Q= 13100, at 79 K and 3.04 GHz).
文摘Gamma irradiation is employed for in situ preparation of PVA-PANI-ZnS nanocomposite. The irradiation dose is varied from 10 to 40 kGy at 10 kGy intervals. The XRD result confirms the formation of crystalline phases corresponding to ZnS nanoparticles, PVA and PANI. Field emission scanning electron microscopy shows the formation of agglomerated PANI along the PVA backbone, within which the ZnS nanoparticles are dispersed.UV-visible spectroscopy is conducted to measure the transmittance spectra of samples revealing the electronic absorption characteristics of ZnS and PANI nanoparticles. Photo-acoustic(PA) setup is installed to investigate the thermal properties of samples. The PA spectroscopy indicates a high value of thermal diffusivity for samples due to the presence of ZnS and PANI nanoparticles. Moreover, at higher doses, the more polymerization and formation of PANI and ZnS nanoparticles result in enhancement of thermal diffusivity.
基金the Advance FOundation of National Defense is greatly appreciated.
文摘The ultrathin aluminum films with thickness in the range of 2~60 nm have been deposited by dc magnetron sputtering apparatus. Reflectance and transmittance of the obtained samples were measured with a WFZ-900-D4 UV/VIS spectrophotometer. The optical constant (n, k) and permittivity (ε', ε') were determined by applying Newton-Simpson recurrent substitution method. The results indicate that the electromagnetic constitutive characteristic of ultrathin aluminum films is a function of thickness and has obvious size effect.
基金Supported by the National Natural Science Foundation of China under Grant No 61574048the Pearl River S&T Nova Program of Guangzhou under Grant No 201710010172+1 种基金the International Science and Technology Cooperation Program of Guangzhou under Grant No 201807010006the Opening Fund of Key Laboratory of Silicon Device Technology under Grant No KLSDTJJ2018-6
文摘The transfer characteristics of amorphous indium-zinc-oxide thin film transistors are measured in the temperature range of 10-400K. The variation of electrical parameters (threshold voltage, field effect mobility, sub-threshold swing, and leafage current) with decreasing temperature are then extracted and analyzed. Moreover, the dom- inated carrier transport mechanisms at different temperature regions are investigated. The experimental data show that the carrier transport mechanism may change from trap-limited conduction to variable range hopping conduction at lower temperature. Moreover, the field effect mobilities are also extracted and simulated at various temperatures.
基金Supported by the National Natural Science Foundation of China under Grant No 51202196the National Aerospace Science Foundation of China under Grant No 2013ZF53067+2 种基金the Natural Science Basic Research Plan in Shaanxi Province of China under Grant No 2014JQ6204the Fundamental Research Funds for the Central Universities under Grant No 3102014JCQ01032the 111 Project under Grant No B08040
文摘Cu/HfOx/n^+Si devices are fabricated to investigate the influence of technological parameters including film thickness and Ar/02 ratio on the resistive switching (RS) characteristics of HfOx films, in terms of switch ratio, endurance properties, retention time and multilevel storage. It is revealed that the RS characteristics show strong dependence on technological parameters mainly by altering the defects (oxygen vacancies) in the film. The sample with thickness of 2Onto and Ar/O2 ratio of 12:3 exhibits the best RS behavior with the potential of multilevel storage. The conduction mechanism of all the films is interpreted based on the filamentary model.
基金supported by the National Natural Science Foundation of China(No.50001013)Hundred-Talent Project of CAS and the NSFC for Outstanding Young Scientists(No.59625103).
文摘TiO2 thin films were prepared by DC magnetron sputtering with the oxygen flow rate higher than the threshold. The film deposited for 5 h was of anatase phase with a preferred orientation along the <220> direction, but the films deposited for 2 and 3 h were amorphous. The transmittance and photocatalytic activity of the TiO2 films increased constantly with increasing film thickness. When the annealing temperature was lower than 700℃, only anatase grew in the TiO2 film. TiO2 phase changed from anatase to rutile when the annealing temperature was above 800℃. The photocatalytic activity decreased with increasing annealing temperature.
基金supported by the National Natural Science Foundation of China under Grant No.50906083National Basic Research Program of China under Grant No.2011CB710705
文摘An experimental investigation was performed to study the heat transfer in an eight-nozzle spray cooling system with de-ionized water as the working fluid. Visualization of the liquid-solid contact area and the flow near the heated surface was made using a microscopic lens system in conjunction with an advanced high-speed camera. The film thickness and film wavelike characteristics under liquid volume flow rates ranged from 2.78×10 -6 m 3 /s to 1.39×10 -5 m 3 /s and surface temperatures between 22℃ and 78.2℃ were examined respectively. The development process of the liquid film on the heated surface was observed. The local mean film thickness, the film wavelike characteristics and the behavior of the bubbles appeared in the liquid film were captured using an image processing technique. It is discovered that there exists a climax of local mean film thickness during the starting process of spray cooling. When the liquid film reaches the dynamic stable state, the dimensionless mean film thickness decreases with the increase of the liquid volume flow rate, and increases with the increase of surface temperature generally. Besides, the volume flow rate has a more significant impact on the wavelength and amplitude of the liquid film compared to the surface temperature.
基金supported by the National Natural Science Foundation of China(Nos.61575139,51602213 and 11604236)the Young Science Foundation of Taiyuan University of Technology(No.2015QN066)
文摘In this work, we focus on the optical super-resolution effect induced by strong nonlinear saturation absorption(NSA) of graphene oxide(GO) membranes. The third-order optical nonlinearities are characterized by the canonical Z-scan technique under femtosecond laser(wavelength: 800 nm, pulse width: 100 fs) excitation. Through controlling the applied femtosecond laser energy, NSA of the GO films can be tuned continuously. The GO film is placed at the focal plane as a unique amplitude filter to improve the resolution of the focused field. A multi-layer system model is proposed to present the generation of a deep sub-wavelength spot associated with the nonlinearity of GO films. Moreover, the parameter conditions to achieve the best resolution(~λ/6) are determined entirely. The demonstrated results here are useful for high density optical recoding and storage, nanolithography, and super-resolution optical imaging.
文摘Polyaniline,ZnO and polyaniline/ZnO nanocomposite thin films are coated on glass substrates using the spray pyrolysis technique.The samples are characterized by the XRD,SEM,EDAX,UV-Vis and I-V characteristics. The XRD analyses confirm that the spray-coated polyaniline and ZnO thin films have orthorhombic and hexagonal structures,respectively,and optical bandgap energy decreases from 3.81 to 3.41 eV with the addition of a Zn atom.SEM analysis of the polyaniline/ZnO nanocomposite thin films shows that there is an agglomeration of ZnO particles with uniform distribution in the polyaniline matrix,and the diode characteristics of the polyaniline /ZnO nanocomposite show weak rectification behavior.Parameters such as the ideality factor,reverse saturation current and barrier height are calculated from the I-V characteristics.