Processing,microstructure,and properties of porous ceramic composites with directional channels

Porous ceramic composites with directional microchannels from micrometer to dozens of micrometer levels have attracted more and more attention in various fields including aerospace,biomedicines,and thermal insulation due to their excellent fluid permeability,mechanical properties,etc.In this article,we summarize the recent directional porous ceramics developments including their main processing routes and respective properties.Meanwhile,the properties get from different processing routes have been com-pared and analyzed in terms of microstructures,mechanical properties,and permeability.Emphasis has been given to the deeper understanding which can allow one to control the microstructural features of these porous ceramic composites to obtain the desired characteristics.This work can provide a useful reference for the development and application of porous ceramic composites with directional microchan-nels.

Direct data domain approach to space-time adaptive processing

In non-homogeneous environment, traditional space-time adaptive processing doesn＇t effectively suppress interference and detect target, because the secondary data don＇ t exactly reflect the statistical characteristic of the range cell under test. A ravel methodology utilizing the direct data domain approach to space-time adaptive processing （ STAP ） in airbome radar non-homogeneous environments is presented. The deterministic least squares adaptive signal processing technique operates on a ＂snapshot-by-snapshot＂ basis to dethrone the adaptive adaptive weights for nulling interferences and estimating signal of interest （SOI）. Furthermore, this approach eliminates the requirement for estimating the covariance through the data of neighboring range cell, which eliminates calculating the inverse of covariance, and can be implemented to operate in real-time. Simulation results illustrate the efficiency of interference suppression in non-homogeneous environment.

Defects of (Tb_(0.3)Dy_(0.7))Fe_(1.95) Alloys with "One-Step" Directional Solidification Process

The main types of defect in the (Tb_(0.3)Dy_(0.7))Fe_(1.95) alloys with the 'one-step' directional solidification process were investigated. The effect of the dendrite, grain boundaries, twin boundaries, and REFe_3 precipitates on the magnetostrictive response of the (Tb_(0.3)Dy_(0.7))Fe_(1.95) alloys was analyzed respectively. The experiment results demonstrate that the dendrite, twin boundaries, and REFe_3 precipitates can be avoided by modifying alloying ingredient, solidification parameters and annealing technique. The dendritic growth front often leads to dendrite sheet, rare earth-rich phase, and twin boundaries. The lower proportion of rare earth, or slow solidification rate, results in the occurrence of REFe_3 precipitatates. It is vital for diminishing the defects to control the undercooling of solid-liquid interface at (2.4～5.1)×10~4 K·s·cm^(-2) so that the crystal grows in cellular growth front.

A NOVEL UNIVERSAL PREPROCESSING APPROACH FOR HIGH-RESOLUTION DIRECTION-OF-ARRIVAL ESTIMATION

A novel universal preprocessing method is proposed to estimate angles of arrival,which is applicable to one-or two-dimensional high resolution processing based on arbitrarycenter-symmetric arrays (such as uniform linear arrays, equal-spaced rectangular planar arraysand symmetric circular arrays). By mapping the complex signal space into the real one, the newmethod can effectively reduce the computation needed by the signal subspace direction findingtechniques without any performance degradation. In addition, the new preprocessing scheme itselfcan decorrelate the coherent signals received on the array. For regular array geometry such asuniform linear arrays and equal-spaced rectangular planar arrays, the popular spatial smoothingpreprocessing technique can be combined with the novel approach to improve the decorrelatingability. Simulation results confirm the above conclusions.

Rejection of Direct Blast Interference Based on Signal Phase-Matching Array Processing

In bistaic acoustic testing, there will be strong direct blast interference. An algorithm based on signal phase-matching array processing that rejects direct blast interference in bistatic acoustic testing has been studied, through which the object scattering signal is accurately extracted. Characteristics of bistatic acoustic testing and signal phase matching processing principle are fully integrated in this algorithm. Firstly, the direct blast interference is calculated from the receiving signal based on three subarrays signal phase matching processing. Secondly, the direct blast is rejected by subtraction from the receiving signal. In this way the limitations of the high signal to noise ratio that signal phase matching processing required for direct calculating the object scattering signal can be avoided. Simulation and sea trial results show that, when the ratio of signal to interference is greater than -20 dB, this algorithm of direct blast interference rejection based phase matching signal processing can accurately extract the object scattering signal.

Heat Transfer Analysis During "One-Step" Directional Solidification Process for Giant Magnetostrictive Materials

By theoretical analysis of heat transfer during the "one-step" directional solidification process, the functional relation between the temperature in solid-liquid interface and its effect factor was studied. The thermal gradient in solid liquid interface and heat transfer coefficient between the samples and surroundings were also calculated. On the basis of the above analysis, some suggestions for improving the thermal gradient in solid-liquid interface were put forward. It will provide a theoretical instruction for preparing high performance giant magnetostrictive materials (GMM).

Numerical simulation of direct shear tests on mechanical properties of talus deposits based on self-adaptive PCNN digital image processing

The macro mechanical properties of materials with characteristics of large scale and complicated structural composition can be analyzed through its reconstructed meso-structures.In this work,the meso-structures of talus deposits that widely exist in the hydro-power engineering in the southwest of China were first reconstructed by small particles according to the in-situ photographs based on the self-adaptive PCNN digital image processing,and then numerical direct shear tests were carried out for studying the mechanical properties of talus deposits.Results indicate that the reconstructed meso-structures of talus deposits are more consistent with the actual situation because the self-adaptive PCNN digital image processing has a higher discrimination in the details of soil-rock segmentation.The existence and random distribution of rock blocks make the initial shear stiffness,the peak strength and the residual strength higher than those of the "pure soil" with particle size less than 1.25 cm apparently,but reduce the displacements required for the talus deposits reaching its peak shear strength.The increase of rock proportion causes a significant improvement in the internal friction angle of talus deposit,which to a certain degree leads to the characteristics of shear stress-displacement curves having a changing trend from the plastic strain softening deformation to the nonlinear strain hardening deformation,while an unconspicuous increase in cohesion.The uncertainty and heterogeneity of rock distributions cause the differences of rock proportion within shear zone,leading to a relatively strong fluctuation in peak strengths during the shear process,while movement features of rock blocks,such as translation,rotation and crossing,expand the scope of shear zone,increase the required shear force,and also directly lead to the misjudgment that the lower shear strength is obtained from the samples with high rock proportion.That,however,just explains the reason why the shear strength gained from a small amount of indoor test data is not consistent with engineering practice.

Solute Redistribution in Directional Melting Process

The solute redistribution in directional melting process is theoretically studied. Based on quantitative evaluations, uniform.solute distribution in liquid and a quasi-steady solute distribution in solid are supposed. The discussion on the solute balance comes to a simple model for the solute redistribution in directional melting process. As an example, the variation of liquid composition during melting process of carbon steel is quantitatively evaluated using the model. Results show that the melting of an alloy starts at solidus temperature, but approaches the liquidus temperature after a very short transient process.

Identification of Kinematic Errors of Five-axis Machine Tool Trunnion Axis from Finished Test Piece

Compared with the traditional non-cutting measurement,machining tests can more accurately reflect the kinematic errors of five-axis machine tools in the actual machining process for the users.However,measurement and calculation of the machining tests in the literature are quite difficult and time-consuming.A new method of the machining tests for the trunnion axis of five-axis machine tool is proposed.Firstly,a simple mathematical model of the cradle-type five-axis machine tool was established by optimizing the coordinate system settings based on robot kinematics.Then,the machining tests based on error-sensitive directions were proposed to identify the kinematic errors of the trunnion axis of cradle-type five-axis machine tool.By adopting the error-sensitive vectors in the matrix calculation,the functional relationship equations between the machining errors of the test piece in the error-sensitive directions and the kinematic errors of C-axis and A-axis of five-axis machine tool rotary table was established based on the model of the kinematic errors.According to our previous work,the kinematic errors of C-axis can be treated as the known quantities,and the kinematic errors of A-axis can be obtained from the equations.This method was tested in Mikron UCP600 vertical machining center.The machining errors in the error-sensitive directions can be obtained by CMM inspection from the finished test piece to identify the kinematic errors of five-axis machine tool trunnion axis.Experimental results demonstrated that the proposed method can reduce the complexity,cost,and the time consumed substantially,and has a wider applicability.This paper proposes a new method of the machining tests for the trunnion axis of five-axis machine tool.

Recovery of iron from copper tailings via low-temperature direct reduction and magnetic separation: process optimization and mineralogical study

Currently, the majority of copper tailings are not effectively developed. Worldwide, large amounts of copper tailings generated from copper production are continuously dumped, posing a potential environmental threat. Herein, the recovery of iron from copper tailings via low-temperature direct reduction and magnetic separation was conducted; process optimization was carried out, and the corresponding mineralogy was investigated. The reduction time, reduction temperature, reducing agent (coal), calcium chloride additive, grinding time, and magnetic field intensity were examined for process optimization. Mineralogical analyses of the sample, reduced pellets, and magnetic concentrate under various conditions were performed by X-ray diffraction, optical microscopy, and scanning electron microscopy-energy-dispersive X-ray spectrometry to elucidate the iron reduction and growth mechanisms. The results indicated that the optimum parameters of iron recovery include a reduction temperature of 1150A degrees C, a reduction time of 120 min, a coal dosage of 25%, a calcium chloride dosage of 2.5%, a magnetic field intensity of 100 mT, and a grinding time of 1 min. Under these conditions, the iron grade in the magnetic concentrate was greater than 90%, with an iron recovery ratio greater than 95%.

Mathematical simulation of direct reduction process in zinc-bearing pellets

A one-dimensional unsteady mathematical model was established to describe direct reduction in a composite pellet made of metallurgical dust. The model considered heat transfer, mass transfer, and chemical reactions including iron oxide reductions, zinc oxide reduction and carbon gasification, and it was numerically solved by the tridiagonal matrix algorithm （TDMA）. In order to verify the model, an experiment was performed, in which the profiles of temperature and zinc removal rate were measured during the reduction process. Results calculated by the mathematical model were in fairly good agreement with experimental data. Finally, the effects of furnace temperature, pellet size, and carbon content were investigated by model calculations. It is found that the pellet temperature curve can be divided into four parts according to heating rate. Also, the zinc removal rate increases with the increase of furnace temperature and the decrease of pellet size, and carbon content in the pellet has little influence on the zinc removal rate.

RESEARCH ON LASER DIRECT DEPOSITION PROCESS OF Ti-6Al-4V ALLOY

Laser direct deposition （LDD） of metallic components is an advanced technology of combining CAD/CAM （computer aided design/computer aided manufacturing）, high power laser, and rapid prototyping. This technology uses laser beam to melt the powders fed coaxiaUy into the molten pool by the laser beam to fabricate fuUy dense metallic components. The present article mainly studies the LDD of Ti-6Al-4V alloy, which can be used to fabricate aircraft components. The mechanical properties of the Ti-6Al-4V alloy, fabricated by LDD, are obtained using the tension test, and the oxygen content of used powders and deposited specimens are measured. In the present article, it can be seen that the mechanical properties obtained using this method are higher than the ones obtained by casting, and equal to those got by wrought anneal. One aircraft part has been made using the LDD process. Because of this aircraft part, with sophisticated shape, the effect of the laser scanning track on the internal soundness of the deposited part was discussed.

A consistency improving method in the analytic hierarchy process based on directed circuit analysis

Test of consistency is critical for the analytic hierarchy process(AHP) methodology. When a pairwise comparison matrix(PCM) fails the consistency test, the decision maker(DM) needs to make revisions. The state of the art focuses on changing a single entry or creating a new matrix based on the original inconsistent matrix so that the modified matrix can satisfy the consistency requirement. However, we have noticed that the reason that causes inconsistency is not only numerical inconsistency, but also logical inconsistency, which may play a more important role in the whole inconsistency. Therefore, to realize satisfactory consistency, first of all, we should change some entries that form a directed circuit to make the matrix logically consistent, and then adjust other entries within acceptable deviations to make the matrix numerically consistent while preserving most of the original comparison information. In this paper, we firstly present some definitions and theories, based on which two effective methods are provided to identify directed circuits. Four optimization models are proposed to adjust the original inconsistent matrix. Finally, illustrative examples and comparison studies show the effectiveness and feasibility of our method.

Explosion limits estimation and process optimization of direct propylene epoxidation with H2 and O2

Direct propylene epoxidation with H2 and O2,an attractive process to produce propylene oxide(PO),has a potential explosion danger due to the coexistence of flammable gases(i.e.,C3 H6 and H2)and oxidizer(i.e.,O2).The unknown explosion limits of the multi-component feed gas mixture make it difficult to optimize the reaction process under safe operation conditions.In this work,a distribution method is proposed and verified to be effective by comparing estimated and experimental explosion limits of more than 200 kinds of flammable gas mixture.Then,it is employed to estimate the explosion limits of the feed gas mixture,some results of which are also validated by the classic Le Chatelier’s Rule and flammable resistance method.Based on the estimated explosion limits,process optimization is carried out using commercially high and inherently safe reactant concentrations to enhance reaction performance.The promising results are directly obtained through the interface called gOPT in gPROMS only by using a simple,easy-constructed and mature packed-bed reactor,such as the PO yield of 13.3%,PO selectivity of 85.1%and outlet PO fraction of 1.8%.These results can be rationalized by indepth analyses and discussion about the effects of the decision variables on the operation safety and reaction performance.The insights revealed here could shed new light on the process development of the PO production based on the estimation of the explosion limits of the multi-component feed gas mixture containing flammable gase s,inert gas and O2,followed by process optimization.

Structural Interpretation of Lineaments Uses Satellite Images Processing: A Case Study in North-Eastern Tunisia

This paper presents a lineament detection method using multi-band remote sensing images. The main objective of this work is to design an automatic image processing tool for lineament mapping from Landsat-7 ETM + satellite data. Five procedures were involved: 1) The Principal Component Analysis;2) image enhancement using histogram equalization technique 3) directional Sobel filters of the original data;4) histogram segmentation and 5) binary image generation. The applied methodology was contributed in identifying several known large-scale faults in the Northeast of Tunisia. The statistical and spatial analyses of lineament map indicate a difference of morphological appearance of lineaments in the satellite image. Indeed, all the lineaments present a specific organization. Five groups were classified based on three orientations: NE-SW, E-W and NW-SE. The overlapping of lineament map with the geologic map confirms that these lineaments of diverse directions can be identified and recognized on the field as a fault. The identified lineaments were linked to a deep faults caused by tectonic movements in Tunisia. This study shows the performance of the satellite image processing in the analysis and mapping of the accidents in the northern Atlas.

Direct Observation of Carrier Transportation Process in InGaAs/GaAs Multiple Quantum Wells Used for Solar Cells and Photodetectors

The resonant excitation is used to generate photo-excited carriers in quantum wells to observe the process of the carriers transportation by comparing the photoluminescence results between quantum wells with and without a p-n junction. It is observed directly in experiment that most of the photo-excited carriers in quantum wells with a p-n junction escape from quantum wells and form photoeurrent rather than relax to the ground state of the quantum wells. The photo absorption coei^cient of multiple quantum wells is also enhanced by a p-n junction. The results pave a novel way for solar cells and photodetectors making use of low-dimensional structure.

Direct Urca Processes with Hyperon-Hyperon Interactions

与相互作用从潜力的新试验性的数据推出了的一个弱重核子重核子( YY )，这篇论文在包括的相对论的吝啬的领域理论( RMFT )的框架执行了直接 Urca ( DURCA )进程的计算*并且介子，与与强壮的 YY 相互作用并且没有计算的结果比较(*，)介子包括了。在中子星物质，当强壮的 YY 相互作用供应吸引人的时，弱 YY 相互作用供应在重核子之间的另外的排斥相互作用。与弱 YY 相互作用，当比那些小时，重核子的有效群众比有强壮的 YY 相互作用的那些大(* ，) 包括的介子。阀值星为包含核子的 DURCA 过程集中， A 不对 YY 相互作用的力量敏感。弱 YY 相互作用为包含的 DURCA 过程导致更大的阀值群众吗？并且 0 比另外的二个盒子。仅仅当弱 YY 相互作用被使用时，包含 0 的过程能发生在中子星。弱 YY 相互作用能引进与更大的质量并且比强壮的 YY 相互作用的更快的冷却的与中子星的观察的协议。

A New View on Processing Gain of DSSS Systems under CW Interference

Differing from the general analysis,the process of continuous wave(CW) interference being despreaded in a direct sequence spread spectrum(DSSS) system is reanalyzed. It is proved that the result sequence of continuous wave interference being despreaded varies according to sinusoid in time.Its frequency and amplitude are derived.The processing gain is discussed under 3 cases in comparison with traditional analysis.Results show that the processing gain varies according to the frequency offset of CW to DSSS signal carrier.

Influence of A Hyperons ^1S0 Superfluidity on the Direct Urca Processes with Hyperons

In the framework of the relativistic mean field theory （RMFT）,the relativistic energy losses of the directUrca processes with hyperons （Y-DURCA） for reactions A → p+e + ve and （?） → A + e + ve are studied in neutron stars.We calculate the energy gap of A hyperons and investigate the effects of the 1S0 superfluidity （SF） of A hyperons on theY-DURCA processes.The calculated results are in line with the recent experimental data ABaa ～ 1.01±0.20-0.11+0.18 MeV.The results indicate that the 1S0 SF of A hyperons exists in most density ranges of happening the two reactions.Thetheoretical cooling curves are in agreement with observation data.

Processing of Liaohe Highly Sour Crude

In order to solve the problems related with processing low-quality Liaohe highly sour crude, the Liaohe Petrochemical Company has explored the possibility in optimizing the processing of highly sour crude by adopting different process schemes depending upon the properties of the highly sour crude. The Liaohe naphthenic-base crude oil with low freezing point is earmarked for manufacture of naphthenic lube oils and heavy traffic paving asphalt, while the extra-heavy Liaohe crude with high acid number is routed directly to delayed coking unit coupled with corresponding corrosion preventing measures, resulting in tackling the problem of equipment corrosion arising from refining of Liaohe highly sour crude to obtain light distillates from Liaohe heavy crude through a short process scheme.