Large crystal growth of Cr-doped h-YMnO3has been investigated by using a high pressure optical floatingzone method. The size of the grown crystals is typically 60–70 mm in length and 4–5 mm in diameter. The structur...Large crystal growth of Cr-doped h-YMnO3has been investigated by using a high pressure optical floatingzone method. The size of the grown crystals is typically 60–70 mm in length and 4–5 mm in diameter. The structure of the grown crystals is analyzed by powder X-ray diffraction and scanning electron microscopy.The defects in the as-grown crystals, including low-angle grain boundary and inclusions are studied. An off-stoichiometric phenomenon is found with a slight Cr deficiency in different parts. The relationship between defects and growth conditions during crystal growth is also discussed. The magnetic properties show spin-glass phase features with weak ferromagnetic behavior below 30 K.展开更多
One improved mixing-extruding machine was introduced as the second-generation product of the mixing-molding integrated technology. In the extruding system,the conventional single screw extruder was substituted by a sp...One improved mixing-extruding machine was introduced as the second-generation product of the mixing-molding integrated technology. In the extruding system,the conventional single screw extruder was substituted by a special conical twin-screw extruder,resulting in stronger feeding ability,more stable extrusion pressure,and better quality of products. The integrated mathematical model of mixing-extruding process was also established by theoretical derivation and optimization according to the experimental results.Then its accuracy was verified by the influences of the pressure of floating weight and the cooling water temperature of extruder on the mixing-extruding integrated process. The results showed that the changes of both parameters could give rise to the fluctuation of the temperature and apparent viscosity of polyblends, thus further influencing the screw rotation speed.展开更多
基金financial support of the National Natural Science Foundation of China (Nos. 51471135 and 51301133)the National Key Research and Development Program (No. 2016YFB1100101)Shaanxi International Cooperation Program
文摘Large crystal growth of Cr-doped h-YMnO3has been investigated by using a high pressure optical floatingzone method. The size of the grown crystals is typically 60–70 mm in length and 4–5 mm in diameter. The structure of the grown crystals is analyzed by powder X-ray diffraction and scanning electron microscopy.The defects in the as-grown crystals, including low-angle grain boundary and inclusions are studied. An off-stoichiometric phenomenon is found with a slight Cr deficiency in different parts. The relationship between defects and growth conditions during crystal growth is also discussed. The magnetic properties show spin-glass phase features with weak ferromagnetic behavior below 30 K.
基金National Natural Science Foundation of China(No.51345006)Specialized Research Fund for the Doctoral Program of Higher Education,China(No.20123719120004)
文摘One improved mixing-extruding machine was introduced as the second-generation product of the mixing-molding integrated technology. In the extruding system,the conventional single screw extruder was substituted by a special conical twin-screw extruder,resulting in stronger feeding ability,more stable extrusion pressure,and better quality of products. The integrated mathematical model of mixing-extruding process was also established by theoretical derivation and optimization according to the experimental results.Then its accuracy was verified by the influences of the pressure of floating weight and the cooling water temperature of extruder on the mixing-extruding integrated process. The results showed that the changes of both parameters could give rise to the fluctuation of the temperature and apparent viscosity of polyblends, thus further influencing the screw rotation speed.
