In the process of riveting an MB15 forging die,cracks were discovered emerging along the longitudinal direction and near the riveting hole.Through fracture analysis,microscopic observation,energy spectrum analysis,met...In the process of riveting an MB15 forging die,cracks were discovered emerging along the longitudinal direction and near the riveting hole.Through fracture analysis,microscopic observation,energy spectrum analysis,metallographic examination,and hardness test,the properties and causes of the cracks are discussed.The results indicate that the cracking type is intergranular brittle cracking,occurring during the forging stage.Furthermore,the recrystallization at the crack site is found to be incomplete,which is attributed to the low deformation temperature.展开更多
Multidirectional forging(MDF)was successfully applied to fabricate large-size Mg-Gd-Y-Zn-Zr-Ag alloy in this work and effects of T4,T5 and T6 treatments on the microstructure and mechanical properties of the as-forged...Multidirectional forging(MDF)was successfully applied to fabricate large-size Mg-Gd-Y-Zn-Zr-Ag alloy in this work and effects of T4,T5 and T6 treatments on the microstructure and mechanical properties of the as-forged alloy were analyzed.Results show that dynamic recrystallization(DRX)occurs and second phase particles precipitate along the grain boundary during the MDF process.After annealing treatment(T4),the volume fraction and size of dynamic precipitates slightly increase at a lower temperature(430℃)compared with those of MDFed sample,while they are dissolved into theα-Mg matrix at a higher temperature(450℃).At the meantime,short plate-shaped long-period stacking ordered(LPSO)phases are observed in the DRX grains of the MDFed sample and then dissolved into theα-Mg matrix during annealing at both temperatures.Typical basal texture is identified in the MDFed sample,but the basal pole tilts away from final forging direction and rare-earth texture component with<1121>orientation parallel to penultimate forging direction becomes visible after annealing.The T6 sample annealing at 430℃for 4 h and ageing at 200℃for 34 h exhibits the superior strength and ductility in this study.The ultimate tensile strength,tensile yield strength and elongation to failure,which is 455 MPa,308 MPa and 7.7%,respectively,are overall improved compared with the directly-aged(T5)sample.This paper provides a superior heat treatment schedule to manufacture high-performance large-scale Mg-Gd-Y-Zn-Zr-Ag components for industrial production.展开更多
Ti-47Al-2Nb-2Cr-0.4(W, Mo) (mole fraction, %) alloy ingot fabricated using vacuum consumable melting was containerless near-isothermally forged, and the high temperature forgeability, microstructure and tensile pr...Ti-47Al-2Nb-2Cr-0.4(W, Mo) (mole fraction, %) alloy ingot fabricated using vacuum consumable melting was containerless near-isothermally forged, and the high temperature forgeability, microstructure and tensile properties were investigated. The results show that the TiAl ingot exhibits good heat workability during containerless near-isothermally forging process, and there are not evident cracks on the surface of as-forged TiAl pancake with a total deformation degree of 60%. The microstructure of the TiAl ingot appears to be typical nearly-lamellar(NL), comprising a great amount of lamellar colonies (α2+γ) and a few equiaxed γ grains. After near-isothermally forging, the as-forged pancake shows primarily fine equiaxed γ grains with an average grain size of 20 μm and some broken lamellar pieces, and some bent lamellas still exist in the hard-deformation zone. Tensile tests at room temperature show that ultimate tensile strength increases from 433 MPa to 573 MPa after forging due to grain refinement effect.展开更多
The effect of forging on the microstructure and texture evolution of a high Nb containing Ti-45Al-7Nb-0.3W(at.%)alloy was investigated by X-ray diffractometer(XRD),scanning electron microscopy(SEM),and transmission el...The effect of forging on the microstructure and texture evolution of a high Nb containing Ti-45Al-7Nb-0.3W(at.%)alloy was investigated by X-ray diffractometer(XRD),scanning electron microscopy(SEM),and transmission electron microscopy(TEM).The results show that the as-cast alloy is mainly composed of α_(2)/γ lamellar colonies with a mean size of 70μm,but the hot-forged pancake displays a near duplex microstructure(DP).Kinking and bending of lamellar colonies,deformation twinning and dynamic recrystallization(DRX)occur during hot forging.Meanwhile,dense dislocations in theβphase after forging suggest that the high-temperature β phase with a disordered structure is favorable for improving the hot-workability of the alloy.Unlike the common TiAl casting texture,the solidification process of the investigated as-cast alloy with high Nb content is completely via the β phase region,resulting in the formation of a<110>γ fiber texture where the<110>γ aligns parallel to the heat-flow direction.In comparison,the relatively strong<001>and weak<302>texture components in the as-forged alloy are attributed to the deformation twinning.After annealing,static recrystallization occurs at the twin boundary and intersections,which weakens the deformation texture.展开更多
Forging spur gears are widely used in the driving system of mining machinery and equipment due to their higher strength and dimensional accuracy.For the purpose of precisely calculating the volume of cylindrical spur ...Forging spur gears are widely used in the driving system of mining machinery and equipment due to their higher strength and dimensional accuracy.For the purpose of precisely calculating the volume of cylindrical spur gear billet in cold precision forging,a new theoretical method named average circle method was put forward.With this method,a series of gear billet volumes were calculated.Comparing with the accurate three-dimensional modeling method,the accuracy of average circle method by theoretical calculation was estimated and the maximum relative error of average circle method was less than 1.5%,which was in good agreement with the experimental results.Relative errors of the calculated and the experimental for obtaining the gear billet volumes with reference circle method are larger than those of the average circle method.It shows that average circle method possesses a higher calculation accuracy than reference circle method(traditional method),which should be worth popularizing widely in calculation of spur gear billet volume.展开更多
Effect of multi-directional forging(MDF)on wear properties of Mg-Zn alloys(with 2,4,and 6wt%Zn)is investigated.Dry sliding wear test was performed using pin on disk machine on MDF processed and homogenized samples.Wea...Effect of multi-directional forging(MDF)on wear properties of Mg-Zn alloys(with 2,4,and 6wt%Zn)is investigated.Dry sliding wear test was performed using pin on disk machine on MDF processed and homogenized samples.Wear behavior of samples was analyzed at loads of ION and 20 N,with sliding distances of 2000m and 4000m,at a sliding velocity of 3m/s.Microstructures of worn samples were observed under scanning electron microscopy(SEM),energy dispersive spectroscopy(EDS),and x-ray diffraction(XRD)and the results were analyzed.Mechanical properties were evaluated using microhardness test.After 5 passes of MDF,the average grain size was found to be 30±4p m,22±3 pm,and 18±3 pm,in Mg-2%Zn,Mg-4%Zn,and Mg-6%Zn alloys,respectively,with significant improvement in hardness in all cases.Wear resistance was improved after MDF processing,as well as,with increment in Zn content in Mg alloy.However,it decreased when the load and the sliding distance increased.Worn surface exhibited ploughing,delamination,plastic deformation,and wear debris along sliding direction,and abrasive wear was found to be the main mechanism.展开更多
Elemental titanium(Ti)and nickel(Ni)powders were consolidated by spark plasma sintering(SPS)to fabricate Ti-51%Ni(mole fraction)shape-memory alloys(SMAs).The objective of this study is to enhance the superelasticity o...Elemental titanium(Ti)and nickel(Ni)powders were consolidated by spark plasma sintering(SPS)to fabricate Ti-51%Ni(mole fraction)shape-memory alloys(SMAs).The objective of this study is to enhance the superelasticity of SPS produced Ti-Ni alloy using free forging as a secondary process.Products from two processes(with and without free forging)were compared in terms of microstructure,transformation temperature and superelasticity.The results showed that,free forging effectively improved the tensile and shape-memory properties.Ductility increased from 6.8%to 9.2%after forging.The maximum strain during superelasticity increased from 5%to 7.5%and the strain recovery rate increased from 72%to 92%.The microstructure of produced Ti-51%Ni SMA consists of the cubic austenite(B2)matrix,monoclinic martensite(B19′),secondary phases(Ti3Ni4,Ti2Ni and TiNi3)and oxides(Ti4Ni2O and Ti3O5).There was a shift towards higher temperatures in the martensitic transformation of free forged specimen(aged at 500°C)due to the decrease in Ni content of B2 matrix.This is related to the presence of Ti3Ni4 precipitates,which were observed using transmission electron microscope(TEM).In conclusion,free forging could improve superelasticity and mechanical properties of Ti-51%Ni SMA.展开更多
Transmission electron microscopy(TEM),scanning electron microscopy(SEM),hardness tests and tensile tests were performed to investigate the effect of aging on microstructure and mechanical properties of forged Al-4.4Cu...Transmission electron microscopy(TEM),scanning electron microscopy(SEM),hardness tests and tensile tests were performed to investigate the effect of aging on microstructure and mechanical properties of forged Al-4.4Cu-0.7Mg-0.6Si alloy.The results show that the alloy exhibits splendid mechanical properties with an ultimate tensile strength of504MPa and an elongation of10.1%after aging at170°C for16h.With tensile testing temperature increasing to150°C,the strength of the alloy declines slightly to483MPa.Then,the strength drops quickly when temperature reaches over200°C.The high strength of the alloy in peak-aged condition is caused by a considerable amount ofθ'and AlMgSiCu(Q)precipitates.The relatively stable mechanical properties tested below150°C are mainly ascribed to the stability ofθ'precipitates.The growth ofθ'and Q precipitates and the generation ofθphase lead to a rapid drop of the strength when temperature is over150°C.展开更多
NiTi-Al-based alloys are promising high-tem- perature structural materials for aerospace and astronautics applications. A new NiTi-Al-based alloy Ni--43Ti-4AI- 2Nb-2Hf (at%) was processed via isothermal forging. The...NiTi-Al-based alloys are promising high-tem- perature structural materials for aerospace and astronautics applications. A new NiTi-Al-based alloy Ni--43Ti-4AI- 2Nb-2Hf (at%) was processed via isothermal forging. The microstructure and mechanical properties at room temperature and high temperature were investigated through scanning electron microscope (SEM), X-ray diffraction (XRD), and tensile tests. Results show that the micro- structure of as-forged Ni-43Ti--4AI-2Nb-2Hf alloy con- sists of NiTi matrix, Ti2Ni phase, and Hf-rich phase. The simultaneous addition of Nb and Hf, which have strong affinities for Ti sites, promotes the precipitation of Hf-rich phases along the grain boundaries. The tensile strengths of Ni-43Ti-4A1-2Nb-2Hf alloy are dramatically increased compared with the ternary Ni-46Ti-4A1 alloy. At room temperature and 650℃, the yield stress of Ni--43Ti-4Al- 2Nb-2Hf alloy reaches 1,070 and 610 MPa, respectively, which are 30 % and 150 % higher than those of Ni--46Ti- 4Al alloy. The improved tensile property results from the solid solution strengthening by Nb and Hf, as well as the dispersion hardening of the Ti2Ni and Hf-rich phases.展开更多
Cold closed-die forging is a suitable process to produce spur-bevel gears due to its advantages, such as saving materials and time, reducing costs, increasing die life and improving the quality of the product. The hom...Cold closed-die forging is a suitable process to produce spur-bevel gears due to its advantages, such as saving materials and time, reducing costs, increasing die life and improving the quality of the product. The homogeneity of microstructure of cold closed-die forged gears can highly affect their service performance. The homogeneity of microstructure and Vickers hardness in cold closed-die forged gear of 20 Cr Mn Ti alloy is comprehensively studied by using optical microscopy and Vickers hardness tester. The results show that the distribution homogeneity of the aspect ratio of grain and Vickers hardness is the same. In the circumferential direction of the gear tooth, the distribution of the aspect ratio of grain and Vickers hardness is inhomogeneous and they gradually decrease from the surface to the center of the tooth. In the radial direction, the distribution of the aspect ratio of grain and Vickers hardness is inhomogeneous on the surface of the gear tooth; while it is relatively homogeneous in the center of the gear tooth. In the axial direction of the gear tooth, the distribution of the aspect ratio of grain and Vickers hardness is relatively homogeneous from the small-end to the large-end of the gear tooth.展开更多
In this study, AA2519 alloy was initially processed by multi axial forging (MAF) at room and cryogenic temperatures. Subsequently, the microstructure and the mechanical behavior of the processed samples under quasi-st...In this study, AA2519 alloy was initially processed by multi axial forging (MAF) at room and cryogenic temperatures. Subsequently, the microstructure and the mechanical behavior of the processed samples under quasi-static loading were investigated to determine the influence of cryogenic forging on alloys’ subgrains dimensions, grain boundaries interactions, strength, ductility and toughness. In addition, the failure mechanisms at the tensile rupture surfaces were characterized using scanning electron micro-scope (SEM). The results show significant improvements in the strength, ductility and toughness of the alloy as a result of the cryogenic MAF process. The formation of nanoscale crystallite microstructure, heavily deformed grains with high density of grain boundaries and second phase breakage to finer particles were characterized as the main reasons for the increase in the mechanical properties of the cryogenic forged samples. The cryogenic processing of the alloy resulted in the formation of an ultrafine grained material with tensile strength and toughness that are ~41% and ~80% higher respectively after 2 cycles MAF when compared with the materials processed at ambient temperature. The fractography analysis on the tested materials shows a substantial ductility improvement in the cryoforged (CF) samples when compared to the room temperature forged (RTF) samples which is in alignment with their stress-strain profiles. However, extended forging at higher cycles than 2 cycles led only to increase in strength at the expense of ductility for both the CF and RTF samples.展开更多
This paper investigated the high cycle fatigue behavior of a forged Mg-7Gd-5Y-1Nd-0.5Zr alloy with different stress concentration factor(Kt),under different stress ratio(R),and along different loading direction.The sm...This paper investigated the high cycle fatigue behavior of a forged Mg-7Gd-5Y-1Nd-0.5Zr alloy with different stress concentration factor(Kt),under different stress ratio(R),and along different loading direction.The smooth specimen(Kt=1),under R=0.1 and along longitude direction,shows a high fatigue strength of 162 MPa at 107 cycles.The fatigue behavior of the forged Mg-7Gd-5Y-1Nd-0.5Zr alloy exhibits a high sensitive to the notch.Moreover,change of stress ratio from 0.1 to−1 may also result in a bad fatigue property.The flux inclusions were elongated along longitude direction and/or transverse direction during the forging process of the Mg-7Gd-5Y-1Nd-0.5Zr alloy.The interface between the flux inclusion and the matrix may debond and serve as the crack initiation site during the fatigue loading process,leading to the deterioration of the fatigue property along thickness direction and a high anisotropic fatigue behavior between longitude direction and thickness direction.展开更多
The microstructural evolution and tensile properties of a forged Ti−42Al−5Mn alloy subjected to different heat treatments were studied.The results showed that,when the forged alloy was aged at 800℃ for 24 h,the inter...The microstructural evolution and tensile properties of a forged Ti−42Al−5Mn alloy subjected to different heat treatments were studied.The results showed that,when the forged alloy was aged at 800℃ for 24 h,the interlamellar spacing(λ)andγgrain size at colony boundaries are generally coarsened.Whereas,when the alloy was first annealed at 1300℃ and then aged at 800℃ for 24 h,this coarsening of related microstructures appears less pronounced.The suggested annealing temperatures for the forged Ti−42Al−5Mn alloy are in the range of 1250−1300℃.It was found that,on the condition of the same annealing system,both the strength and ductility were improved as the aging temperature changed from 1000 to 800℃.The secondary precipitatedβo(β_(o,sec))at colony boundaries could be responsible for improving the strength,and theγphase at colony boundaries with the grain size about 6μm might be one of the main reasons for the better ductility.展开更多
With a focus on the backup roll, a rolling-contact-fatigue experiment was performed on samples of 5% Cr forged steel. The P-S-N fatigue curves were determined and the fatigue strength was calculated. The emergence of ...With a focus on the backup roll, a rolling-contact-fatigue experiment was performed on samples of 5% Cr forged steel. The P-S-N fatigue curves were determined and the fatigue strength was calculated. The emergence of cracks on the test-sample surfaces was observed at different fatigue cycles. A micro-hardness tester was used to measure the hardness of the subsurface fatigue layer. The microstructures were analyzed at various magnifications with an optical microscope, scanning electron microscope, and transmission electron microscope. Based on these tests, the rolling-contact-fatigue mechanism of the large forged steel backup roll was also considered. The results showed that the contact-fatigue strength of the tested backup roll steel was 1 249 MPa;the surface fatigue crack lengthened continuously as the number of cycles increased and followed an S-shaped curve; the subsurface fatigue hardness reached its highest value at about 90 (HV) increment from the matrix hardness of 540 (HV) in the backup roll; the subsurface martensite/bainite microstructure was crushed and the dislocation density was greatly increased. Under alternating contact stresses,the surface/subsurface material was damaged and exhibited many microdefects. At the least, the surface fatigue layer on backup rolls should be fully removed before the microcracks enter a period of rapid propagation.展开更多
A round 60% of useful energy is wasted in industry, homes, or transportation. Therefore, there has been increasing attention on thermoelectric materials for their ability to harvest waste heat into useful energy. The ...A round 60% of useful energy is wasted in industry, homes, or transportation. Therefore, there has been increasing attention on thermoelectric materials for their ability to harvest waste heat into useful energy. The efficiency of a thermoelectric material depends on its electrical conductivity, Seebeck coefficient, and thermal conductivity in a conflicting manner which results in efficiency optimization challenges. Single crystals and polycrystalline layered materials have comparatively better thermoelectric and mechanical properties in a certain direction. Texture engineering is a special strategy that allows the exploitation of superior material properties in a specific direction. Texturing could be achieved by various sintering and deformation methods, which yield defects improving thermoelectric and mechanical properties. The results show that for(Bi,Sb)_(2)Te_(3), Bi_(2)(Se,Te)_(3), C uSbSe_(2), and SnSe, significant enhancement in the thermoelectric figure of merit is achieved by enhancing the preferred orientation. Texture engineering provides a wide range of strategies to elevate the zT of anisotropic materials to values comparable to those of their single crystalline counterparts.展开更多
The microstructure and mechanical properties of titanium(Ti)-bearing medium-carbon nonquenched and tempered steel with different nitrogen content before and after hot forging were investigated through smelting,forging...The microstructure and mechanical properties of titanium(Ti)-bearing medium-carbon nonquenched and tempered steel with different nitrogen content before and after hot forging were investigated through smelting,forging,and laboratory tests.The results show that the grain size of nonquenched and tempered steel was gradually refined,and the ferrite content gradually increased with an increase in nitrogen content.The grain size of the material with low nitrogen content increased abnormally,and its impact properties significantly decreased after hot forging.The grain size of nonquenched and tempered steel with higher nitrogen content was slightly larger than that before forging,and the tensile and yield strength increased,but the impact toughness was not significantly reduced.The Ti-bearing nonquenched and tempered steel showed better strength and toughness after hot forging with the addition of 0.010%0.015%nitrogen.展开更多
Blockchain has proven to be an emerging technology in the digital world, changing the way everyone thinks about data security and bringing efficiency to several industries. It has already been applied to a wide range ...Blockchain has proven to be an emerging technology in the digital world, changing the way everyone thinks about data security and bringing efficiency to several industries. It has already been applied to a wide range of applications, from financial services and supply chain management to voting systems and identity verification. An organization must verify its candidates before selecting them. Choosing an unqualified candidate can ruin an organization’s reputation. In this paper, a blockchain-based academic certificate authentication system will be used to ensure authenticity and make the assertion of the decentralized system secure. However, the system will generate, authenticate and make corrections on academic certificates. Ultimately, some blockchain-based authentication systems already exist, they can’t correct any errors that occur during generation. A blockchain-based certificate authentication system was built using blockchain technology. Where admin could generate, authenticate and correct the certificate if necessary. The admin can also check how many times a certificate has been modified. Other users can only check the authenticity of the certificates. We’re using two blockchains to enable corrections. Blockchain technology can successfully implement a certificate authentication system. This system will eliminate doubts about the authenticity of certificates, provide fast responses, and ensure reliable and secure storage. The proposed system will help in many ways, such as providing a user-friendly university admission, and smooth job hiring process, etc. In conclusion, our proposed system can permanently eradicate certificate forgeries and create and promote trust in society.展开更多
The promotion of the national common language and writing system stands as a cornerstone in cultivating a sense of community among the Chinese nation.The national common language and writing system,serving as a potent...The promotion of the national common language and writing system stands as a cornerstone in cultivating a sense of community among the Chinese nation.The national common language and writing system,serving as a potent vehicle for cultural dissemination and linguistic communication,acts as a crucial bridge fostering unity,mutual support,cultural exchange,and cohesion among diverse ethnic groups.Its widespread promotion not only reinforces the cohesion of the Chinese nation but also plays a pivotal role in fortifying national and cultural identity.The advocacy and dissemination of the national common language and writing system contribute significantly to enhancing the sense of community within the Chinese nation.This concerted effort serves as an internal driving force,creating a positive feedback loop that strengthens both national identity and the cultural bonds shared by the Chinese people.The reciprocal relationship between the promotion and popularization of the national common language and writing system reinforces a mutual sense of assistance and reciprocity.This bidirectional dynamic propels a synergistic interplay,fostering a beneficial cycle in the promotion and widespread adoption of the national common language and writing system.In essence,the promotion and popularization of the national common language and writing system not only contribute to its advancement but also serve to deepen the sense of community within the Chinese nation.This reciprocal interaction between the two elements establishes a robust foundation for nurturing a strong and cohesive Chinese community.展开更多
基金Key R&D Plan Projects in Hubei Province(Grant No.2021BID001)the Research on Multiple Regression and Fitting Technology of Simulation Data for Dynamic Umbrella Opening of Lifesaving Umbrella(Grant No.HX2021157)。
文摘In the process of riveting an MB15 forging die,cracks were discovered emerging along the longitudinal direction and near the riveting hole.Through fracture analysis,microscopic observation,energy spectrum analysis,metallographic examination,and hardness test,the properties and causes of the cracks are discussed.The results indicate that the cracking type is intergranular brittle cracking,occurring during the forging stage.Furthermore,the recrystallization at the crack site is found to be incomplete,which is attributed to the low deformation temperature.
基金supported by National Natural Science Foundation of China(Grant No.51874367 and 51574291)。
文摘Multidirectional forging(MDF)was successfully applied to fabricate large-size Mg-Gd-Y-Zn-Zr-Ag alloy in this work and effects of T4,T5 and T6 treatments on the microstructure and mechanical properties of the as-forged alloy were analyzed.Results show that dynamic recrystallization(DRX)occurs and second phase particles precipitate along the grain boundary during the MDF process.After annealing treatment(T4),the volume fraction and size of dynamic precipitates slightly increase at a lower temperature(430℃)compared with those of MDFed sample,while they are dissolved into theα-Mg matrix at a higher temperature(450℃).At the meantime,short plate-shaped long-period stacking ordered(LPSO)phases are observed in the DRX grains of the MDFed sample and then dissolved into theα-Mg matrix during annealing at both temperatures.Typical basal texture is identified in the MDFed sample,but the basal pole tilts away from final forging direction and rare-earth texture component with<1121>orientation parallel to penultimate forging direction becomes visible after annealing.The T6 sample annealing at 430℃for 4 h and ageing at 200℃for 34 h exhibits the superior strength and ductility in this study.The ultimate tensile strength,tensile yield strength and elongation to failure,which is 455 MPa,308 MPa and 7.7%,respectively,are overall improved compared with the directly-aged(T5)sample.This paper provides a superior heat treatment schedule to manufacture high-performance large-scale Mg-Gd-Y-Zn-Zr-Ag components for industrial production.
基金Project (2011CB605505) supported by the National Basic Research Program of ChinaProject (2008AA03A233) supported by the National High-Tech Research and Development Program of China
文摘Ti-47Al-2Nb-2Cr-0.4(W, Mo) (mole fraction, %) alloy ingot fabricated using vacuum consumable melting was containerless near-isothermally forged, and the high temperature forgeability, microstructure and tensile properties were investigated. The results show that the TiAl ingot exhibits good heat workability during containerless near-isothermally forging process, and there are not evident cracks on the surface of as-forged TiAl pancake with a total deformation degree of 60%. The microstructure of the TiAl ingot appears to be typical nearly-lamellar(NL), comprising a great amount of lamellar colonies (α2+γ) and a few equiaxed γ grains. After near-isothermally forging, the as-forged pancake shows primarily fine equiaxed γ grains with an average grain size of 20 μm and some broken lamellar pieces, and some bent lamellas still exist in the hard-deformation zone. Tensile tests at room temperature show that ultimate tensile strength increases from 433 MPa to 573 MPa after forging due to grain refinement effect.
基金Projects(52274402,52174381)supported by the National Natural Science Foundation of China。
文摘The effect of forging on the microstructure and texture evolution of a high Nb containing Ti-45Al-7Nb-0.3W(at.%)alloy was investigated by X-ray diffractometer(XRD),scanning electron microscopy(SEM),and transmission electron microscopy(TEM).The results show that the as-cast alloy is mainly composed of α_(2)/γ lamellar colonies with a mean size of 70μm,but the hot-forged pancake displays a near duplex microstructure(DP).Kinking and bending of lamellar colonies,deformation twinning and dynamic recrystallization(DRX)occur during hot forging.Meanwhile,dense dislocations in theβphase after forging suggest that the high-temperature β phase with a disordered structure is favorable for improving the hot-workability of the alloy.Unlike the common TiAl casting texture,the solidification process of the investigated as-cast alloy with high Nb content is completely via the β phase region,resulting in the formation of a<110>γ fiber texture where the<110>γ aligns parallel to the heat-flow direction.In comparison,the relatively strong<001>and weak<302>texture components in the as-forged alloy are attributed to the deformation twinning.After annealing,static recrystallization occurs at the twin boundary and intersections,which weakens the deformation texture.
文摘Forging spur gears are widely used in the driving system of mining machinery and equipment due to their higher strength and dimensional accuracy.For the purpose of precisely calculating the volume of cylindrical spur gear billet in cold precision forging,a new theoretical method named average circle method was put forward.With this method,a series of gear billet volumes were calculated.Comparing with the accurate three-dimensional modeling method,the accuracy of average circle method by theoretical calculation was estimated and the maximum relative error of average circle method was less than 1.5%,which was in good agreement with the experimental results.Relative errors of the calculated and the experimental for obtaining the gear billet volumes with reference circle method are larger than those of the average circle method.It shows that average circle method possesses a higher calculation accuracy than reference circle method(traditional method),which should be worth popularizing widely in calculation of spur gear billet volume.
文摘Effect of multi-directional forging(MDF)on wear properties of Mg-Zn alloys(with 2,4,and 6wt%Zn)is investigated.Dry sliding wear test was performed using pin on disk machine on MDF processed and homogenized samples.Wear behavior of samples was analyzed at loads of ION and 20 N,with sliding distances of 2000m and 4000m,at a sliding velocity of 3m/s.Microstructures of worn samples were observed under scanning electron microscopy(SEM),energy dispersive spectroscopy(EDS),and x-ray diffraction(XRD)and the results were analyzed.Mechanical properties were evaluated using microhardness test.After 5 passes of MDF,the average grain size was found to be 30±4p m,22±3 pm,and 18±3 pm,in Mg-2%Zn,Mg-4%Zn,and Mg-6%Zn alloys,respectively,with significant improvement in hardness in all cases.Wear resistance was improved after MDF processing,as well as,with increment in Zn content in Mg alloy.However,it decreased when the load and the sliding distance increased.Worn surface exhibited ploughing,delamination,plastic deformation,and wear debris along sliding direction,and abrasive wear was found to be the main mechanism.
基金the Ministry of Higher Education of Malaysia for the Malaysian International Scholarship and research funding under FRGS vote No. R.J13000.7824.4F810
文摘Elemental titanium(Ti)and nickel(Ni)powders were consolidated by spark plasma sintering(SPS)to fabricate Ti-51%Ni(mole fraction)shape-memory alloys(SMAs).The objective of this study is to enhance the superelasticity of SPS produced Ti-Ni alloy using free forging as a secondary process.Products from two processes(with and without free forging)were compared in terms of microstructure,transformation temperature and superelasticity.The results showed that,free forging effectively improved the tensile and shape-memory properties.Ductility increased from 6.8%to 9.2%after forging.The maximum strain during superelasticity increased from 5%to 7.5%and the strain recovery rate increased from 72%to 92%.The microstructure of produced Ti-51%Ni SMA consists of the cubic austenite(B2)matrix,monoclinic martensite(B19′),secondary phases(Ti3Ni4,Ti2Ni and TiNi3)and oxides(Ti4Ni2O and Ti3O5).There was a shift towards higher temperatures in the martensitic transformation of free forged specimen(aged at 500°C)due to the decrease in Ni content of B2 matrix.This is related to the presence of Ti3Ni4 precipitates,which were observed using transmission electron microscope(TEM).In conclusion,free forging could improve superelasticity and mechanical properties of Ti-51%Ni SMA.
基金Project(51301209)supported by the National Natural Science Foundation of China
文摘Transmission electron microscopy(TEM),scanning electron microscopy(SEM),hardness tests and tensile tests were performed to investigate the effect of aging on microstructure and mechanical properties of forged Al-4.4Cu-0.7Mg-0.6Si alloy.The results show that the alloy exhibits splendid mechanical properties with an ultimate tensile strength of504MPa and an elongation of10.1%after aging at170°C for16h.With tensile testing temperature increasing to150°C,the strength of the alloy declines slightly to483MPa.Then,the strength drops quickly when temperature reaches over200°C.The high strength of the alloy in peak-aged condition is caused by a considerable amount ofθ'and AlMgSiCu(Q)precipitates.The relatively stable mechanical properties tested below150°C are mainly ascribed to the stability ofθ'precipitates.The growth ofθ'and Q precipitates and the generation ofθphase lead to a rapid drop of the strength when temperature is over150°C.
基金supported by the National Natural Science Foundation of China (No. 51201016)
文摘NiTi-Al-based alloys are promising high-tem- perature structural materials for aerospace and astronautics applications. A new NiTi-Al-based alloy Ni--43Ti-4AI- 2Nb-2Hf (at%) was processed via isothermal forging. The microstructure and mechanical properties at room temperature and high temperature were investigated through scanning electron microscope (SEM), X-ray diffraction (XRD), and tensile tests. Results show that the micro- structure of as-forged Ni-43Ti--4AI-2Nb-2Hf alloy con- sists of NiTi matrix, Ti2Ni phase, and Hf-rich phase. The simultaneous addition of Nb and Hf, which have strong affinities for Ti sites, promotes the precipitation of Hf-rich phases along the grain boundaries. The tensile strengths of Ni-43Ti-4A1-2Nb-2Hf alloy are dramatically increased compared with the ternary Ni-46Ti-4A1 alloy. At room temperature and 650℃, the yield stress of Ni--43Ti-4Al- 2Nb-2Hf alloy reaches 1,070 and 610 MPa, respectively, which are 30 % and 150 % higher than those of Ni--46Ti- 4Al alloy. The improved tensile property results from the solid solution strengthening by Nb and Hf, as well as the dispersion hardening of the Ti2Ni and Hf-rich phases.
基金Project(51105287)supported by the National Natural Science Foundation of ChinaProject(2013M531750)supported by China Postdoctoral Science Foundation
文摘Cold closed-die forging is a suitable process to produce spur-bevel gears due to its advantages, such as saving materials and time, reducing costs, increasing die life and improving the quality of the product. The homogeneity of microstructure of cold closed-die forged gears can highly affect their service performance. The homogeneity of microstructure and Vickers hardness in cold closed-die forged gear of 20 Cr Mn Ti alloy is comprehensively studied by using optical microscopy and Vickers hardness tester. The results show that the distribution homogeneity of the aspect ratio of grain and Vickers hardness is the same. In the circumferential direction of the gear tooth, the distribution of the aspect ratio of grain and Vickers hardness is inhomogeneous and they gradually decrease from the surface to the center of the tooth. In the radial direction, the distribution of the aspect ratio of grain and Vickers hardness is inhomogeneous on the surface of the gear tooth; while it is relatively homogeneous in the center of the gear tooth. In the axial direction of the gear tooth, the distribution of the aspect ratio of grain and Vickers hardness is relatively homogeneous from the small-end to the large-end of the gear tooth.
文摘In this study, AA2519 alloy was initially processed by multi axial forging (MAF) at room and cryogenic temperatures. Subsequently, the microstructure and the mechanical behavior of the processed samples under quasi-static loading were investigated to determine the influence of cryogenic forging on alloys’ subgrains dimensions, grain boundaries interactions, strength, ductility and toughness. In addition, the failure mechanisms at the tensile rupture surfaces were characterized using scanning electron micro-scope (SEM). The results show significant improvements in the strength, ductility and toughness of the alloy as a result of the cryogenic MAF process. The formation of nanoscale crystallite microstructure, heavily deformed grains with high density of grain boundaries and second phase breakage to finer particles were characterized as the main reasons for the increase in the mechanical properties of the cryogenic forged samples. The cryogenic processing of the alloy resulted in the formation of an ultrafine grained material with tensile strength and toughness that are ~41% and ~80% higher respectively after 2 cycles MAF when compared with the materials processed at ambient temperature. The fractography analysis on the tested materials shows a substantial ductility improvement in the cryoforged (CF) samples when compared to the room temperature forged (RTF) samples which is in alignment with their stress-strain profiles. However, extended forging at higher cycles than 2 cycles led only to increase in strength at the expense of ductility for both the CF and RTF samples.
基金This work was funded by the National Basic Research Program of China(973 Program)through project No.2013CB632202National Natural Science Foundation of China(NSFC)through projects No.51105350 and No.51301173,respectively.
文摘This paper investigated the high cycle fatigue behavior of a forged Mg-7Gd-5Y-1Nd-0.5Zr alloy with different stress concentration factor(Kt),under different stress ratio(R),and along different loading direction.The smooth specimen(Kt=1),under R=0.1 and along longitude direction,shows a high fatigue strength of 162 MPa at 107 cycles.The fatigue behavior of the forged Mg-7Gd-5Y-1Nd-0.5Zr alloy exhibits a high sensitive to the notch.Moreover,change of stress ratio from 0.1 to−1 may also result in a bad fatigue property.The flux inclusions were elongated along longitude direction and/or transverse direction during the forging process of the Mg-7Gd-5Y-1Nd-0.5Zr alloy.The interface between the flux inclusion and the matrix may debond and serve as the crack initiation site during the fatigue loading process,leading to the deterioration of the fatigue property along thickness direction and a high anisotropic fatigue behavior between longitude direction and thickness direction.
基金the Jihua Laboratory Scientific Research Project,China (No.X210291TL210)the National Natural Science Foundation of China (No.51971215)the Natural Science Foundation of Liaoning Province of China (No.2019-MS-330)。
文摘The microstructural evolution and tensile properties of a forged Ti−42Al−5Mn alloy subjected to different heat treatments were studied.The results showed that,when the forged alloy was aged at 800℃ for 24 h,the interlamellar spacing(λ)andγgrain size at colony boundaries are generally coarsened.Whereas,when the alloy was first annealed at 1300℃ and then aged at 800℃ for 24 h,this coarsening of related microstructures appears less pronounced.The suggested annealing temperatures for the forged Ti−42Al−5Mn alloy are in the range of 1250−1300℃.It was found that,on the condition of the same annealing system,both the strength and ductility were improved as the aging temperature changed from 1000 to 800℃.The secondary precipitatedβo(β_(o,sec))at colony boundaries could be responsible for improving the strength,and theγphase at colony boundaries with the grain size about 6μm might be one of the main reasons for the better ductility.
文摘With a focus on the backup roll, a rolling-contact-fatigue experiment was performed on samples of 5% Cr forged steel. The P-S-N fatigue curves were determined and the fatigue strength was calculated. The emergence of cracks on the test-sample surfaces was observed at different fatigue cycles. A micro-hardness tester was used to measure the hardness of the subsurface fatigue layer. The microstructures were analyzed at various magnifications with an optical microscope, scanning electron microscope, and transmission electron microscope. Based on these tests, the rolling-contact-fatigue mechanism of the large forged steel backup roll was also considered. The results showed that the contact-fatigue strength of the tested backup roll steel was 1 249 MPa;the surface fatigue crack lengthened continuously as the number of cycles increased and followed an S-shaped curve; the subsurface fatigue hardness reached its highest value at about 90 (HV) increment from the matrix hardness of 540 (HV) in the backup roll; the subsurface martensite/bainite microstructure was crushed and the dislocation density was greatly increased. Under alternating contact stresses,the surface/subsurface material was damaged and exhibited many microdefects. At the least, the surface fatigue layer on backup rolls should be fully removed before the microcracks enter a period of rapid propagation.
基金support from the A*STAR’s Science and Engineering Research CouncilSustainable Hybrid Lighting System for Controlled Environment Agriculture Program: A19D9a0096+1 种基金Singapore MOE AcRF Tier 2 under Grant (No.2018-T2-1-010)funding from the A*STAR’s Career Development Award (No.C210112022)。
文摘A round 60% of useful energy is wasted in industry, homes, or transportation. Therefore, there has been increasing attention on thermoelectric materials for their ability to harvest waste heat into useful energy. The efficiency of a thermoelectric material depends on its electrical conductivity, Seebeck coefficient, and thermal conductivity in a conflicting manner which results in efficiency optimization challenges. Single crystals and polycrystalline layered materials have comparatively better thermoelectric and mechanical properties in a certain direction. Texture engineering is a special strategy that allows the exploitation of superior material properties in a specific direction. Texturing could be achieved by various sintering and deformation methods, which yield defects improving thermoelectric and mechanical properties. The results show that for(Bi,Sb)_(2)Te_(3), Bi_(2)(Se,Te)_(3), C uSbSe_(2), and SnSe, significant enhancement in the thermoelectric figure of merit is achieved by enhancing the preferred orientation. Texture engineering provides a wide range of strategies to elevate the zT of anisotropic materials to values comparable to those of their single crystalline counterparts.
文摘The microstructure and mechanical properties of titanium(Ti)-bearing medium-carbon nonquenched and tempered steel with different nitrogen content before and after hot forging were investigated through smelting,forging,and laboratory tests.The results show that the grain size of nonquenched and tempered steel was gradually refined,and the ferrite content gradually increased with an increase in nitrogen content.The grain size of the material with low nitrogen content increased abnormally,and its impact properties significantly decreased after hot forging.The grain size of nonquenched and tempered steel with higher nitrogen content was slightly larger than that before forging,and the tensile and yield strength increased,but the impact toughness was not significantly reduced.The Ti-bearing nonquenched and tempered steel showed better strength and toughness after hot forging with the addition of 0.010%0.015%nitrogen.
文摘Blockchain has proven to be an emerging technology in the digital world, changing the way everyone thinks about data security and bringing efficiency to several industries. It has already been applied to a wide range of applications, from financial services and supply chain management to voting systems and identity verification. An organization must verify its candidates before selecting them. Choosing an unqualified candidate can ruin an organization’s reputation. In this paper, a blockchain-based academic certificate authentication system will be used to ensure authenticity and make the assertion of the decentralized system secure. However, the system will generate, authenticate and make corrections on academic certificates. Ultimately, some blockchain-based authentication systems already exist, they can’t correct any errors that occur during generation. A blockchain-based certificate authentication system was built using blockchain technology. Where admin could generate, authenticate and correct the certificate if necessary. The admin can also check how many times a certificate has been modified. Other users can only check the authenticity of the certificates. We’re using two blockchains to enable corrections. Blockchain technology can successfully implement a certificate authentication system. This system will eliminate doubts about the authenticity of certificates, provide fast responses, and ensure reliable and secure storage. The proposed system will help in many ways, such as providing a user-friendly university admission, and smooth job hiring process, etc. In conclusion, our proposed system can permanently eradicate certificate forgeries and create and promote trust in society.
基金National Common Language Education Practice and Training Innovation Team(Science and Technology Leading Talents and Innovation Team BuildingProject Number:ZSLJ202201)。
文摘The promotion of the national common language and writing system stands as a cornerstone in cultivating a sense of community among the Chinese nation.The national common language and writing system,serving as a potent vehicle for cultural dissemination and linguistic communication,acts as a crucial bridge fostering unity,mutual support,cultural exchange,and cohesion among diverse ethnic groups.Its widespread promotion not only reinforces the cohesion of the Chinese nation but also plays a pivotal role in fortifying national and cultural identity.The advocacy and dissemination of the national common language and writing system contribute significantly to enhancing the sense of community within the Chinese nation.This concerted effort serves as an internal driving force,creating a positive feedback loop that strengthens both national identity and the cultural bonds shared by the Chinese people.The reciprocal relationship between the promotion and popularization of the national common language and writing system reinforces a mutual sense of assistance and reciprocity.This bidirectional dynamic propels a synergistic interplay,fostering a beneficial cycle in the promotion and widespread adoption of the national common language and writing system.In essence,the promotion and popularization of the national common language and writing system not only contribute to its advancement but also serve to deepen the sense of community within the Chinese nation.This reciprocal interaction between the two elements establishes a robust foundation for nurturing a strong and cohesive Chinese community.