Multidirectional forging(MDF)was successfully applied to fabricate large-size Mg-Gd-Y-Zn-Zr-Ag alloy in this work and effects of T4,T5 and T6 treatments on the microstructure and mechanical properties of the as-forged...Multidirectional forging(MDF)was successfully applied to fabricate large-size Mg-Gd-Y-Zn-Zr-Ag alloy in this work and effects of T4,T5 and T6 treatments on the microstructure and mechanical properties of the as-forged alloy were analyzed.Results show that dynamic recrystallization(DRX)occurs and second phase particles precipitate along the grain boundary during the MDF process.After annealing treatment(T4),the volume fraction and size of dynamic precipitates slightly increase at a lower temperature(430℃)compared with those of MDFed sample,while they are dissolved into theα-Mg matrix at a higher temperature(450℃).At the meantime,short plate-shaped long-period stacking ordered(LPSO)phases are observed in the DRX grains of the MDFed sample and then dissolved into theα-Mg matrix during annealing at both temperatures.Typical basal texture is identified in the MDFed sample,but the basal pole tilts away from final forging direction and rare-earth texture component with<1121>orientation parallel to penultimate forging direction becomes visible after annealing.The T6 sample annealing at 430℃for 4 h and ageing at 200℃for 34 h exhibits the superior strength and ductility in this study.The ultimate tensile strength,tensile yield strength and elongation to failure,which is 455 MPa,308 MPa and 7.7%,respectively,are overall improved compared with the directly-aged(T5)sample.This paper provides a superior heat treatment schedule to manufacture high-performance large-scale Mg-Gd-Y-Zn-Zr-Ag components for industrial production.展开更多
A method to simulate processes of forging and subsequent heat treatment of an axial symmetric rod is formulated in eulerian description and the feasibility is investigated. This method uses finite volume mushes for t...A method to simulate processes of forging and subsequent heat treatment of an axial symmetric rod is formulated in eulerian description and the feasibility is investigated. This method uses finite volume mushes for troching material deformation and an automatically refined facet surface to accurately trace the free surface of the deforming material.In the method,the deforming work piece flows through fixed finite volume meshes using eulerian formulation to describe the conservation laws,Fixed finite volume meshing is particularly suitable for large three-dimensional deformation such as forging because remeshing techniques are not required, which are commonly considered to be the main bottelencek in the ssimulations of large defromation by using the finite element method,By means of this finite volume method, an approach has been developed in the framework of 'metallo-thermo-mechanics' to simulate metallic structure, temperature and stress/strain coupled in the heat treatment process.In a first step of simulation, the heat treatment solver is limited in small deformation hypothesis,and un- coupled with forging. The material is considered as elastic-plastic and takes into account of strain, strain rate and temperature effects on the yield stress.Heat generation due to deformation,heat con- duction and thermal stress are considered.Temperature - dependent phase transformation,stress-in- duced phase transformation,latent heat,transformation stress and strain are included.These ap- proaches are implemented into the commerical commercial computer program MSC/SuperForge and a verification example with experimental date is given as comparison.展开更多
The hardness and residual stress in the forging for cold roller during low temperature tempering,and the relationship of residual stress and cooling temperature of high temperature tempering for heavy forgings were st...The hardness and residual stress in the forging for cold roller during low temperature tempering,and the relationship of residual stress and cooling temperature of high temperature tempering for heavy forgings were studied.The stress relaxation constant at low temperature tempering and the elasto-plastisity inversion temperature at high temperature tempering were found.The results are of great importance to determine rational tempering cooling process of heavy forgings.展开更多
The ＂soft canning＂ heat preservation technique is invented by Baoshan Iron ＆ Steel Co., Ltd. （Hereafter referred to Baosteel）, using the flexible insulation material which can be stuck on the surface of the heate...The ＂soft canning＂ heat preservation technique is invented by Baoshan Iron ＆ Steel Co., Ltd. （Hereafter referred to Baosteel）, using the flexible insulation material which can be stuck on the surface of the heated ingot or billet in the superalloy thermal process. This adhesive insulation material can reduce the temperature drop of the ingot or billet during the transferring or hot working process, and can deform with the billet without dropping. The surface temperature drop can be effectively reduced, so the products can be obtained a good surface quality and the structural uniformity can be improved. The technique is applied to hard-wrought superalloy forging of cogging, superalloy rods finished forging fire and superalloy hot die forging processing,and good results have been achieved.展开更多
The heat treatment, including two steps, was proposed to obtain Fine Fully Lamellar (FFL) microstructure on TiAl containing minor Ni. The first step was in (a+y) phase region to get Duplex (DP) microstructure, and the...The heat treatment, including two steps, was proposed to obtain Fine Fully Lamellar (FFL) microstructure on TiAl containing minor Ni. The first step was in (a+y) phase region to get Duplex (DP) microstructure, and the second step was in a phase region transforming DP microstructure into FFL microstructure. The effect of heat treatment on microstructures and properties was studied. The results showed that the static recrystallization kinetics in (a+y) phase region took the form of Avrami equitation, and the remnant lamellae in DP microstructure were detrimental to room temperature tensile properties. The FL microstructures were obtained after heat treatment in phase region using DP microstructure, the uniform FFL microstructure was beneficial to comprehensive properties.展开更多
In order to realize cold forging of magnesium alloys in practical application,some methods for ductility improvement of a commercial wrought AZ31B magnesium alloy(Mg-3%Al-1%Zn,mass fraction) at room temperature were s...In order to realize cold forging of magnesium alloys in practical application,some methods for ductility improvement of a commercial wrought AZ31B magnesium alloy(Mg-3%Al-1%Zn,mass fraction) at room temperature were suggested.The effects of heat treatment before forging and hydrostatic pressure during forging on the ductility were investigated in cold upsetting and cup forging.High-temperature annealing was effective to reduce the degree of the texture anisotropy of the specimen,and it was found that the forging limit of the annealed specimen was improved in cold forging.On the other hand,cold cup forging of the annealed specimen was carried out with applying counter pressure.By applying counter pressures of 100-200 MPa during forging,the critical punch stroke for forging limit of the specimen without crack was improved by 25%in punch stroke.展开更多
The paper introduced the 5 CrMnMo steel, including the chemical composition, the heat treatment technology, the forging die working condition, and the invalidation form （such as the cavity arris wear, the cavity subs...The paper introduced the 5 CrMnMo steel, including the chemical composition, the heat treatment technology, the forging die working condition, and the invalidation form （such as the cavity arris wear, the cavity subsidence, the cold and the heat fatigue crackle）. Then gave some precautions for prolonging the mould life by improving the heat treatment technology.展开更多
Nitrogen can increase the strength of steels without weakening the toughness and improve the corrosion resistance at the same time. Compared with conventional nitrogen-free die steels, a new type of nitrogen-containin...Nitrogen can increase the strength of steels without weakening the toughness and improve the corrosion resistance at the same time. Compared with conventional nitrogen-free die steels, a new type of nitrogen-containing die steel was developed with many superior properties, such as high strength, high hardness, and good toughness. This paper focused on the effects of heat treatment on the microstruc- tures and mechanical properties of the new type of nitrogen-containing die steel, which were investigated by the optimized deformation process and heat treatment. Isothermal spheroidal annealing and high-temperature quenching as well as high-temperature tempering were ap- plied in the experiment by means of an orthogonal method after the steel was multiply forged. The mechanical properties of nitro- gen-containing die steel forgings are better than the standard of NADCA #207-2003.展开更多
In this study, a new near-beta titanium alloy, Ti- 4Al-1 Sn-2Zr-5Mo-8V-2.5Cr, was prepared by induction skull melting (ISM) and multidirectional forging. The effect of aging heat treat me rn on microstructure and ten ...In this study, a new near-beta titanium alloy, Ti- 4Al-1 Sn-2Zr-5Mo-8V-2.5Cr, was prepared by induction skull melting (ISM) and multidirectional forging. The effect of aging heat treat me rn on microstructure and ten sile properties of the alloy after solution treatment in the twophase (α+β) region was investigated. The microstructure results show that the globular primary ot phase (cxp) and the needle-like secondary y. phase (ots) are precipitated in the P matrix. The size of ots increases with the increase in aging temperature, while the con tent of ots goes up to a peak value and then decreases. The tensile testing results show that the strength increases first and then decreases with the in crease in temperature. The variation of ductility presents the opposite way compared with the trend of strength level. When aged at 500℃, the alloy exhibits an excellebalance of tensile strength (1529 MPa) and elongation (9.22%). And the relative mechanism of sirengthening and toughening was analyzed and discussed.展开更多
基金supported by National Natural Science Foundation of China(Grant No.51874367 and 51574291)。
文摘Multidirectional forging(MDF)was successfully applied to fabricate large-size Mg-Gd-Y-Zn-Zr-Ag alloy in this work and effects of T4,T5 and T6 treatments on the microstructure and mechanical properties of the as-forged alloy were analyzed.Results show that dynamic recrystallization(DRX)occurs and second phase particles precipitate along the grain boundary during the MDF process.After annealing treatment(T4),the volume fraction and size of dynamic precipitates slightly increase at a lower temperature(430℃)compared with those of MDFed sample,while they are dissolved into theα-Mg matrix at a higher temperature(450℃).At the meantime,short plate-shaped long-period stacking ordered(LPSO)phases are observed in the DRX grains of the MDFed sample and then dissolved into theα-Mg matrix during annealing at both temperatures.Typical basal texture is identified in the MDFed sample,but the basal pole tilts away from final forging direction and rare-earth texture component with<1121>orientation parallel to penultimate forging direction becomes visible after annealing.The T6 sample annealing at 430℃for 4 h and ageing at 200℃for 34 h exhibits the superior strength and ductility in this study.The ultimate tensile strength,tensile yield strength and elongation to failure,which is 455 MPa,308 MPa and 7.7%,respectively,are overall improved compared with the directly-aged(T5)sample.This paper provides a superior heat treatment schedule to manufacture high-performance large-scale Mg-Gd-Y-Zn-Zr-Ag components for industrial production.
文摘A method to simulate processes of forging and subsequent heat treatment of an axial symmetric rod is formulated in eulerian description and the feasibility is investigated. This method uses finite volume mushes for troching material deformation and an automatically refined facet surface to accurately trace the free surface of the deforming material.In the method,the deforming work piece flows through fixed finite volume meshes using eulerian formulation to describe the conservation laws,Fixed finite volume meshing is particularly suitable for large three-dimensional deformation such as forging because remeshing techniques are not required, which are commonly considered to be the main bottelencek in the ssimulations of large defromation by using the finite element method,By means of this finite volume method, an approach has been developed in the framework of 'metallo-thermo-mechanics' to simulate metallic structure, temperature and stress/strain coupled in the heat treatment process.In a first step of simulation, the heat treatment solver is limited in small deformation hypothesis,and un- coupled with forging. The material is considered as elastic-plastic and takes into account of strain, strain rate and temperature effects on the yield stress.Heat generation due to deformation,heat con- duction and thermal stress are considered.Temperature - dependent phase transformation,stress-in- duced phase transformation,latent heat,transformation stress and strain are included.These ap- proaches are implemented into the commerical commercial computer program MSC/SuperForge and a verification example with experimental date is given as comparison.
文摘The hardness and residual stress in the forging for cold roller during low temperature tempering,and the relationship of residual stress and cooling temperature of high temperature tempering for heavy forgings were studied.The stress relaxation constant at low temperature tempering and the elasto-plastisity inversion temperature at high temperature tempering were found.The results are of great importance to determine rational tempering cooling process of heavy forgings.
文摘The ＂soft canning＂ heat preservation technique is invented by Baoshan Iron ＆ Steel Co., Ltd. （Hereafter referred to Baosteel）, using the flexible insulation material which can be stuck on the surface of the heated ingot or billet in the superalloy thermal process. This adhesive insulation material can reduce the temperature drop of the ingot or billet during the transferring or hot working process, and can deform with the billet without dropping. The surface temperature drop can be effectively reduced, so the products can be obtained a good surface quality and the structural uniformity can be improved. The technique is applied to hard-wrought superalloy forging of cogging, superalloy rods finished forging fire and superalloy hot die forging processing,and good results have been achieved.
基金National High-Tech Projects(863 program)supported this research under the contract number 2001AA301080 and 2002AA305209 respectively.
文摘The heat treatment, including two steps, was proposed to obtain Fine Fully Lamellar (FFL) microstructure on TiAl containing minor Ni. The first step was in (a+y) phase region to get Duplex (DP) microstructure, and the second step was in a phase region transforming DP microstructure into FFL microstructure. The effect of heat treatment on microstructures and properties was studied. The results showed that the static recrystallization kinetics in (a+y) phase region took the form of Avrami equitation, and the remnant lamellae in DP microstructure were detrimental to room temperature tensile properties. The FL microstructures were obtained after heat treatment in phase region using DP microstructure, the uniform FFL microstructure was beneficial to comprehensive properties.
基金supported in part by the Japan Ministry of Education,Culture,Sports,Science and Technology,with Grant-in-Aid for Young Scientists(B)
文摘In order to realize cold forging of magnesium alloys in practical application,some methods for ductility improvement of a commercial wrought AZ31B magnesium alloy(Mg-3%Al-1%Zn,mass fraction) at room temperature were suggested.The effects of heat treatment before forging and hydrostatic pressure during forging on the ductility were investigated in cold upsetting and cup forging.High-temperature annealing was effective to reduce the degree of the texture anisotropy of the specimen,and it was found that the forging limit of the annealed specimen was improved in cold forging.On the other hand,cold cup forging of the annealed specimen was carried out with applying counter pressure.By applying counter pressures of 100-200 MPa during forging,the critical punch stroke for forging limit of the specimen without crack was improved by 25%in punch stroke.
文摘The paper introduced the 5 CrMnMo steel, including the chemical composition, the heat treatment technology, the forging die working condition, and the invalidation form （such as the cavity arris wear, the cavity subsidence, the cold and the heat fatigue crackle）. Then gave some precautions for prolonging the mould life by improving the heat treatment technology.
基金supported by the National Natural Science Foundation of China (Nos.50974014 and 51174026)
文摘Nitrogen can increase the strength of steels without weakening the toughness and improve the corrosion resistance at the same time. Compared with conventional nitrogen-free die steels, a new type of nitrogen-containing die steel was developed with many superior properties, such as high strength, high hardness, and good toughness. This paper focused on the effects of heat treatment on the microstruc- tures and mechanical properties of the new type of nitrogen-containing die steel, which were investigated by the optimized deformation process and heat treatment. Isothermal spheroidal annealing and high-temperature quenching as well as high-temperature tempering were ap- plied in the experiment by means of an orthogonal method after the steel was multiply forged. The mechanical properties of nitro- gen-containing die steel forgings are better than the standard of NADCA #207-2003.
基金financially supported by the National Natural Science Foundation of China (Nos. 51504163, 51604191 and 51601099)
文摘In this study, a new near-beta titanium alloy, Ti- 4Al-1 Sn-2Zr-5Mo-8V-2.5Cr, was prepared by induction skull melting (ISM) and multidirectional forging. The effect of aging heat treat me rn on microstructure and ten sile properties of the alloy after solution treatment in the twophase (α+β) region was investigated. The microstructure results show that the globular primary ot phase (cxp) and the needle-like secondary y. phase (ots) are precipitated in the P matrix. The size of ots increases with the increase in aging temperature, while the con tent of ots goes up to a peak value and then decreases. The tensile testing results show that the strength increases first and then decreases with the in crease in temperature. The variation of ductility presents the opposite way compared with the trend of strength level. When aged at 500℃, the alloy exhibits an excellebalance of tensile strength (1529 MPa) and elongation (9.22%). And the relative mechanism of sirengthening and toughening was analyzed and discussed.
